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Surface morphology and phase stability of titanium irradiated with 168 MeV 136Xe ions

Paper presented at the “XIII Scientific Conference on Titanium and Titanium Alloys 2017”, 24–27 September 2017, Janów Podlaski, Poland
  • Mariusz Kaminski , Piotr Budzynski , Zbigniew Surowiec , Marek Wiertel and Vladimir A. Skuratov
Published/Copyright: July 27, 2018
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International Journal of Materials Research
From the journal International Journal of Materials Research Volume 109 Issue 8

Abstract

A titanium sample was irradiated with Xe 168 MeV energy at fluences of 1 × 1014, 2.2 × 1014, and 5 × 1014 ions · m−2. Changes induced by the ions with irradiation were analysed with an atomic force microscope, scanning electron microscope, and X-ray diffractometer. The irradiation at a fluence of 1 × 1014 ions · cm−2 leads to formation of hillocks with a density of 9 × 106 hillocks · cm−2. An increase in the fluence value results in disappearance of the hillocks and formation of void–dislocation lines. The changes in the surface topography are accompanied by a change in the relative content of the hcp (α) and fcc phases. The substantial changes in the crystalline structure (increased content of the fcc phase, reduction of lattice constants, changes in stresses) resulted from irradiation at a fluence of 1 × 1014 ions · cm−2. Irradiation of massive titanium samples with xenon ions at a fluence of 168 MeV 1 × 1014 ions · cm−2 at room temperature leads to a transition of ∼10% of the hexagonally closed-packed phase – hcp (α) into a face centred cubic structure (the fcc phase). Higher Xe ion fluences contribute to further reduction of lattice constants and crystallite sizes as well as reduction of the phase fcc content and lower values of stresses. It has been found for the first time that irradiation at higher fluences leads to partial recovery of the hcp (α) phase. Irradiation changes the texture of∼50% of the fcc phase crystallites.

Keywords: High energy ion implantation; Phase stability; Titanium; X-ray diffraction; AFM
*Correspondence address, Kamiński Mariusz, MSc. Eng., Faculty of Mechanical Engineering, Lublin University of Technology, Nadbystrzycka str. 36, 20-618 Lublin, Poland, Tel.: +48517663623, E-mail:

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Received: 2017-08-07
Accepted: 2018-01-29
Published Online: 2018-07-27
Published in Print: 2018-08-10

© 2018, Carl Hanser Verlag, München

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https://doi.org/10.3139/146.111653
Keywords for this article
High energy ion implantation; Phase stability; Titanium; X-ray diffraction; AFM

Articles in the same Issue

  1. Contents
  2. Contents
  3. Original Contributions
  4. Dynamic fragmentation and spheroidization of α phase grains during hot deformation of Ti-6Al-4V alloy
  5. Formation and characterization of hot tearing in AZ series alloys
  6. The effect of quench-aging on the mechanical properties of Zn-27Al-1Cu alloy
  7. Microstructural and mechanical properties of novel β-type Ti–Nb–Ni alloys containing a second phase
  8. Microstructure evolution mechanisms of undercooled Ni80Cu20 alloys
  9. Microstructures and tensile properties of CuZrAlNb metallic glass composites under different cooling rates
  10. Influence of a rare-earth element on the solidification behaviour and mechanical properties of undercooled Al–Si alloys
  11. Microstructure of aluminide coatings on Ti6Al4V alloy produced by the slurry method with inorganic binder
  12. Ultrathin SnO2 nanorod/reduced graphene oxide nanosheet composites for electrochemical supercapacitor applications with excellent cyclic stability
  13. Combustion synthesis and formation mechanism of silver nanoparticles
  14. Phase relationship of the Ag–Zr–Cr system at 1000 and 750°C
  15. Thermal properties of carbonized composite materials based on carbon filled elastomeric matrices
  16. Short Communications
  17. Surface morphology and phase stability of titanium irradiated with 168 MeV 136Xe ions
  18. DGM News
  19. DGM News
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