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Effect of ball milling time on the synthesis of nanocrystalline merwinite via mechanical activation and heat treatment

  • Masoud Hafezi , Ali Nadernezhad , Maryam Mohammadi , Hadi Barzegar and Hossein Mohammadi
Published/Copyright: May 8, 2014
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International Journal of Materials Research
From the journal International Journal of Materials Research Volume 105 Issue 5

Abstract

Nanocrystalline merwinite was successfully synthesized by mechanical activation of a mixture of magnesium hydroxide, calcium oxide and silica gel powders followed by heat treatment. The phase development and various physical properties were investigated as a function of milling time using X-ray diffraction, scanning electron microscopy, simultaneous thermal analysis, particle size analysis and transmission electron microscopy. The results showed that formation of merwinite in annealed powders was enhanced by increasing the milling time. Nanocrystalline merwinite powder with an average crystallite size of about 36 nm was obtained after 30 hours of ball milling and subsequent annealing in 900 °C for 1 hour.

Keywords: Merwinite; Mechanical activation; X-ray techniques; Phase development
* Correspondence address, Assistant Professor Masoud Hafezi, Biomaterials Group, Nanotechnology and Advanced Materials Department, Materials and Energy Research Center, P.O. Box 14155-4777, Tehran, Iran, Tel.: +98-2636280040-9, Fax: +98-2636201888, E-mail:

References

[1] C.Wu, J.Chang: J. Biomed. Mater. Res.83 (2007) 153. 10.1002/jbm.b.30779Search in Google Scholar

[2] T.Kokubo: J. Biomaterials12 (2) (1991) 155. 10.1016/0142-9612(91)90194-FSearch in Google Scholar

[3] L.Xu, G.Yu, E.Zhang, F.Pan, K.Yang: J. Biomed. Mater. Res.83 (2007) 703. 10.1002/jbm.a.31273Search in Google Scholar PubMed

[4] Z.Li, X.Gu, S.Lou, Y.Zheng: J. Biomaterials29 (2008) 1329. 10.1016/j.biomaterials.2007.12.021Search in Google Scholar PubMed

[5] M.Hafezi-Ardakani, F.Moztarzadeh, M.Rabiee, A.Talebi, M.Abasi-Shahni, F.Fesahat, F.Sadeghian: J. Ceram. Proc. Res.11 (2010) 765.Search in Google Scholar

[6] J.Ou, Y.Kang, Z.Huang, X.Chen, J.Wu, R.Xiao, G.Yin: Biomed. Mater.3 (2008) 015015. 10.1088/1748-6041/3/1/015015Search in Google Scholar PubMed

[7] J.Ou, G.F.Yin, D.L.Zhou, X.C.Chen, Y.D.Yao, W.Z.Yang, B.L.Wu, M.Xue, J.Cui, W.F.Zhu, Y.Q.Kang: Key Eng. Mater.330 (2007) 67. 10.4028/www.scientific.net/KEM.330-332.67Search in Google Scholar

[8] M.Hafezi-Ardakani, F.Moztarzadeh, M.Rabiee, A.Talebi: Ceram. Int.37 (2011) 175. 10.1016/j.ceramint.2010.08.034Search in Google Scholar

[9] M.Abbasi-Shahni, S.Hesaraki, A.Behnam-Ghader, M.Hafezi-Ardakani: Key Eng. Mater.493 (2012) 582.Search in Google Scholar

[10] M.Hafezi-Ardakani, F.Kavian, F.Moztarzadeh, M. BaghabanEslaminejad, A.Zamanian, F.Bagheri: Key Eng. Mater.493 (2012) 718.Search in Google Scholar

[11] T.D.Shen, C.C.Koch, T.L.McCormick, R.J.Nemanich, J.Y.Huang, J.G.Huang: J. Mater. Res.10 (1995) 139. 10.1557/JMR.1995.0139Search in Google Scholar

[12] E.Gaffet, L.Mazerolles, P.Berthet, D.Michel: Mater. Sci. Forum235 (1996) 103–108).10.4028/www.scientific.net/MSF.235-238.103Search in Google Scholar

[13] G.J.Fan, F.Q.Guo, Z.Q.Hu, M.X.Quan, K.Lu: Phys. Rev.55 (1997) 11010. 10.1103/PhysRevB.55.11010Search in Google Scholar

[14] G.Zhou, H.Bakker: Phys. Rev.49 (18) (1994) 12507. 10.1103/PhysRevB.49.12507Search in Google Scholar

[15] E.J.Mittemeijer, U.Welzel: Z. Kristallogr.223 (9) (2008) 552. 10.1524/zkri.2008.1213Search in Google Scholar

[16] G.K.Williamson, W.H.Hall: Acta Metall.1 (1953) 22. 10.1016/0001-6160(53)90006-6Search in Google Scholar

[17] F.Tavangarian, R.Emadi: Mater. Lett.65 (15–16) (2011) 2354.10.1016/j.matlet.2011.04.108Search in Google Scholar

[18] F.Tavangarian, R.Emadi: J. Alloys Compd.485 (1–2) (2009) 648.10.1016/j.jallcom.2009.06.051Search in Google Scholar

[19] P.J.Anderson, R.F.Horlock: Trans. Faraday Soc.58 (1962) 1993. 10.1039/tf9625801993Search in Google Scholar

[20] F.Tavangarian, R.Emadi: Powder Technol.203 (2010) 180. 10.1016/j.powtec.2010.05.007Search in Google Scholar

[21] F.Tavangarian, R.Emadi: J. Alloys Compd.489 (2) (2010) 600. 10.1016/j.jallcom.2009.09.120Search in Google Scholar

[22] F.Tavangarian, R.Emadi: Int. J. Mod. Phys. B24 (03) (2010) 343. 10.1142/S0217979210053987Search in Google Scholar

[23] F.Tavangarian, R.Emadi, A.Shafyei: Powder Technol.198 (3) (2010) 412. 10.1016/j.powtec.2009.12.007Search in Google Scholar

[24] F.Tavangarian, R.Emadi: Mater. Res. Bull.45 (4) (2010) 388. 10.1016/j.materresbull.2009.12.032Search in Google Scholar

[25] C.Suryanarayana: Prog. Mater. Sci.46 (1) (2001) 1. 10.1016/S0079-6425(99)00010-9Search in Google Scholar

Received: 2013-10-20
Accepted: 2013-11-27
Published Online: 2014-05-08
Published in Print: 2014-05-13

© 2014, Carl Hanser Verlag, München

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https://doi.org/10.3139/146.111048
Keywords for this article
Merwinite; Mechanical activation; X-ray techniques; Phase development

Articles in the same Issue

  1. Contents
  2. Contents
  3. Review
  4. Research trends in microwave dielectrics and factors affecting their properties: A review
  5. Original Contributions
  6. Efficiency and work performance of TiNi alloy undergoing B2 ↔ R martensitic transformation
  7. Fabrication of Gasar made from Cu-24 wt.% Mn alloy
  8. Effect of intermediate frequency electromagnetic field on the solidification structure and mechanical properties of direct chill cast Al-8 wt.%Si alloy
  9. Effect of Ni-based conversion coating and Ni–P electroless plating on the bonding process of pure Al and AZ31 alloy
  10. Effect of ball milling time on the synthesis of nanocrystalline merwinite via mechanical activation and heat treatment
  11. Structural and magnetic properties of Fe–Al2O3 soft magnetic composites prepared using the sol–gel method
  12. Improved dielectric performance of barium strontium titanate multilayered capacitor by means of pulsed laser deposition and slow injection sol–gel methods
  13. Effect of heat treatment on the slurry erosion resistance of high strength steel DP980
  14. Development of biomimetic gelatin–chitosan/hydroxyapatite nanocomposite via double diffusion method for biomedical applications
  15. Short Communications
  16. Effects of rolling rate on microstructure and mechanical properties of Mg sheets
  17. Effect of post-weld heat treatment on dissimilar friction stir welded AA6063 and A319 aluminium alloys
  18. Dielectric and magnetic properties of Ba0.8Sr0.2TiO3 – Y3Fe5O12 – YFeO3 composites
  19. Microwave-assisted modulated synthesis of zirconium-based metal–organic framework (Zr-MOF) for hydrogen storage applications
  20. DGM News
  21. DGM News
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