Crystalline chalcogenido metalates – synthetic approaches for materials synthesis and transformation

References

[1] Y.-F. Song, R. Tsunashima. Recent advances on polyoxometalate-based molecular and composite materials. Chem. Soc. Rev.2012, 41, 7384.10.1039/c2cs35143aSuche in Google Scholar PubMed

[2] T. Irie, S. Endo, S. Kimura. Electrical properties of p- and n-type CuInSe₂ single crystals. J. Appl. Phys.1978, 18, 1303.10.1143/JJAP.18.1303Suche in Google Scholar

[3] H. Li, C. D. Malliakas, Z. Liu, J. A. Peters, M. Sebastian, L. Zhao, D. Y. Chung, B. W. Wessels, M. G. Kanatzidis. Investigation of semi-insulating Cs₂Hg₆S₇ and Cs₂Hg_6-xCd_xS₇ alloy for hard radiation detection. Cryst. Growth Des.2014, 14, 5949.10.1021/cg501151rSuche in Google Scholar

[4] W. S. Sheldrick, M. Wachhold. Solventothermal synthesis of solid-state chalcogenidometalates. Angew. Chem. Int. Ed. Engl.1997, 36, 206.10.1002/anie.199702061Suche in Google Scholar

[5] A. Stein, S. W. Keller, T. E. Mallouk. Turning down the heat: design and mechanism in solid-state syntesis. Science1993, 259, 1558.10.1126/science.259.5101.1558Suche in Google Scholar PubMed

[6] J. Androulakis, S. C. Peter, H. Li, C. D. Malliakas, J. A. Peters, Z. Liu, B. W. Wessels, J.-H. Song, H. Jin, A. J. Freeman, M. G. Kanatzidis. Dimensional reduction: a design tool for new radiation detection materials. Adv. Mater.2011, 23, 4163.10.1002/adma.201102450Suche in Google Scholar PubMed

[7] G. Thiele, L. Vondung, C. Donsbach, S. Pulz, S. Dehnen. Organic cation and complex cation-stabilized (Poly-)selenides, [Cation]_x(Se_y)_z: diversity in structures and properties. Z. Anorg. Allg. Chem. 2014, 640, 2684.10.1002/zaac.201400457Suche in Google Scholar

[8] G. Thiele, N. Lichtenberger, R. Tonner, S. Dehnen. Syntheses, structures and electronic properties of a new series of tellurides of the type [Sequestrated Cation]₂[Te_x] (x = 1–4). Z. Anorg. Allg. Chem.2013, 639, 2809.10.1002/zaac.201300303Suche in Google Scholar

[9] G. Thiele, L. Vondung, S. Dehnen. β-K₂Se₂ and K₂Se₄: missing links in the binary system K-Se. Z. Kristallogr. 2016, 231, 257.10.1515/zkri-2015-1921Suche in Google Scholar

[10] G. Thiele, S. Santner, C. Donsbach, M. Assmann, M. Müller, S. Dehnen. Solvothermal and ionothermal syntheses and structures of amine- and/or (Poly-)Chalcogenide coordinated metal complexes. Z. Kristallogr.2014, 229, 489.10.1515/zkri-2014-1746Suche in Google Scholar

[11] C. Donsbach, G. Thiele, L. H. Finger, J. Sundermeyer, S. Dehnen. Mercurates from a revised ionothermal synthesis route: the pseudo-flux approach. Inorg. Chem.2016, 55, 6725.10.1021/acs.inorgchem.6b00974Suche in Google Scholar PubMed

[12] K. O. Klepp. Darstellung und Kristallstruktur von K₂Sn₂S₅ und K₂Sn₂Se₅. Z. Naturforsch.1992, 47b, 197.10.1515/znb-1992-0209Suche in Google Scholar

[13] Y. Lin, D. Xie, W. Massa, L. Mayrhofer, S. Lippert, B. Evers, A. Chernikov, M. Koch, S. Dehnen. Reversible changes in structural dimensionality of selenostannates in ionic liquids: formation, structures, stability and photocunductivity. Chem. Eur. J.2013, 19, 8806.10.1002/chem.201300807Suche in Google Scholar PubMed

[14] G. Thiele, L. Vondung, S. Dehnen. About the syntheses of chalcogenidometalates by in-situ reduction with elemental alkali metals. Z. Anorg. Allg. Chem.2015, 641, 247.10.1002/zaac.201400462Suche in Google Scholar

[15] G. Thiele, C. Donsbach, R. Riedel, M. Marsch, K. Harms, S. Dehnen. Smallest molecular chalcogenidometalate anions of the heaviest metals: syntheses, structures, and their interconversion. Dalton Trans.2016, 45, 5958.10.1039/C5DT03996GSuche in Google Scholar PubMed

[16] G. Thiele, T. Krüger, S. Dehnen. K₄[PbSe₄]·en·NH₃: a non-oxide, non-halide inorganic lead(IV) compound. Angew. Chem. Int. Ed.2014, 53, 4704.10.1002/anie.201310455Suche in Google Scholar

[17] G. Thiele, S. Lippert, F. Fahrnbauer, P. Bron, O. Oeckler, A. Rahimi-Iman, M. Koch, B. Roling, S. Dehnen. K₂Hg₂Se₃: large-scale synthesis of a photoconductor material prototype with a columnar polyanionic substructure. Chem. Mater.2015, 27, 4114.10.1021/acs.chemmater.5b01198Suche in Google Scholar

[18] G. Thiele, C. Donsbach, I. Nußbruch, S. Dehnen. Combining solid state and solution based techniques: synthesis and reactivity of chalcogenidoplumbates(II or IV). J. Vis. Exp.2016, in press.10.3791/54789Suche in Google Scholar PubMed PubMed Central

[19] G. Thiele, M. Balmer, S. Dehnen. Synthesis, structure and electronic situation of [Rh₆Te₈(PPh₃)₆]·4C₆H₆. Z. Naturforsch.2016, 71b, 391.10.1515/znb-2015-0199Suche in Google Scholar

[20] G. Thiele, Z. You, S. Dehnen. Molecular CHEVREL-like clusters [(RhPPh₃)₆(μ-Se)₈] and [Pd₆(μ-Te)₈]^4–. Inorg. Chem.2015, 54, 2491.10.1021/ic502409rSuche in Google Scholar PubMed

[21] G. Thiele, Y. Franzke, F. Weigend, S. Dehnen. μ-PbSe: a heavy CO homologue as an unexpected ligand. Angew. Chem. Int. Ed.2015, 54, 11283.10.1002/anie.201504863Suche in Google Scholar PubMed

[22] S. Santner, J. Heine, S. Dehnen. Synthesis of crystalline chalcogenides in ionic liquids. Angew. Chem. Int. Ed.2016, 54, 886.10.1002/anie.201507736Suche in Google Scholar PubMed

[23] W.-W. Xiong, J.-R. Li, B. Hu, B. Tan, R.-F. Li, X.-Y. Huang. Largest discrete dupertetrahedral clusters synthesized in ionic liquids. Chem. Sci.2012, 3, 1200.10.1039/c2sc00824fSuche in Google Scholar

[24] Y. Lin, W. Massa, S. Dehnen. “Zeoball”: a molecular zeolite-related anion with spherical topology. J. Am. Chem. Soc.2012, 134, 4497.10.1021/ja2115635Suche in Google Scholar PubMed

[25] G. Thiele, B. Wagner, S. Dehnen. Solvothermal reactions in and with nitriles. Eur. J. Inorg. Chem.2015, 2015, 5322.10.1002/ejic.201501019Suche in Google Scholar

[26] S. Heimann, G. Thiele, S. Dehnen. Nitrile functionalized organogermane chalcogenide clusters with hetero-(nor-)adamantane cores. J. Organomet. Chem.2016, 813, 36.10.1016/j.jorganchem.2016.03.026Suche in Google Scholar