A solid-state approach for the low temperature synthesis of Cr3Si hollow particles

Liangbiao Wang; Zhe Chen; Yongjie Xie; Yuting Xiong; Qinglin Cheng; Ziyan Wang; Hengyuan Zhang; Ziming Zhou; Kailong Zhang; Tao Mei

doi:10.1515/ijmr-2021-8375

Artikel

A solid-state approach for the low temperature synthesis of Cr₃Si hollow particles

Liangbiao Wang , Zhe Chen , Yongjie Xie , Yuting Xiong , Qinglin Cheng , Ziyan Wang , Hengyuan Zhang , Ziming Zhou , Kailong Zhang und Tao Mei

Veröffentlicht/Copyright: 20. November 2021

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Aus der Zeitschrift International Journal of Materials Research Band 112 Heft 11

Abstract

In this paper, pure cubic chromium silicide (Cr₃Si) hollow particles have been successfully synthesized through the solid-state reaction of chromium sesquioxide, silicon powder and metallic lithium in an autoclave at 600 °C for 10 h. The as-prepared samples were characterized by means of X-ray diffraction, field emission scanning electron microscopy and transmission electron microscopy, which showed that the as-prepared samples were cubic phase Cr₃Si hollow particles. Furthermore, the oxidation resistance of the obtained Cr₃Si sample was also investigated.

Keywords: Chemical synthesis; Silicide; Particles; X-ray diffraction

Dr. Liangbiao Wang School of Chemistry and Environment Engineering Jiangsu University of Technology No. 1801 Zhongwu Road Changzhou 213001 P. R. China

Dr. Kailong Zhang Key Laboratory for Palygorskite Science and Applied Technology of Jiangsu School of Chemical Engineering Huaiyin Institute of Technology Huaian, China No. 1 Yuancheng Road Huai ’an 223003 P. R. China

Prof. Tao Mei School of Materials Science and Engineering Hubei University Wuhan China No. 368 Youyi Road Wuhan 430062 P. R. China

Funding statement: This work was supported by the National Natural Science Foundation of China (grant no. 52176185), the Changzhou Sci&Tech Program (grant no. CJ20200041) and the Open Project of Key Laboratory for Palygorskite Science and Applied Technology of Jiangsu (grant no. HPK202004).

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Received: 2021-05-22

Accepted: 2021-07-23

Published Online: 2021-11-20

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Artikel in diesem Heft

https://doi.org/10.1515/ijmr-2021-8375

Schlagwörter für diesen Artikel

Chemical synthesis; Silicide; Particles; X-ray diffraction