Volume 227, Issue 4

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

Open Access
Crystal structure of Na₄Rb₂(V₁₀O₂₈)·10H₂O, H₂₀Na₄O₃₈Rb₂V₁₀

October 18, 2014

Hai-Xing Liu, Xiao-Yan Ren, Jing-Zhong Xiao, Hui-Juan Yue, Xi-Shi Tai

Page range: 429-430

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H 20 Na 4 O 38 Rb 2 V 10 , triclinic, P 1̄(no. 2), a = 8.5555(9) Å, b = 10.448(1) Å, c = 11.237(2) Å, α = 68.483(1)°, β = 87.170(2)°, γ = 67.291(1)°, V = 857.0 Å 3 , Z = 1, R gt (F) = 0.0611, wR ref (F 2 ) = 0.1679, T = 293 K.
Open Access
Crystal structure of calciumpermanganate tetrahydrate, Ca(MnO₄)₂·4H₂O, CaH₈Mn₂O₁₂

October 18, 2014

Florian Wächter, Michael Wörle, Serhiy Budnyk, Reinhard Nesper

Page range: 431-432

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CaH 8 Mn 2 O 12 , orthorhombic, Pccn (no. 56), a = 13.9791(19) Å, b = 5.5404(8) Å, c = 13.3908(18) Å, V = 1037.1(2) Å 3 , Z = 4, R gt (F) = 0.0318, wR ref (F 2 ) = 0.0659, T = 293 K.
Open Access
Crystal structure of lithium potassium yttrium pentafluoride LiKYF5 prepared from high-temperature melt, F₁₀K₂Li₂Y₂

October 18, 2014

Kazumasa Sugiyama, Yuki Furuya, Akira Yoshikawa

Page range: 433-434

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F 10 K 2 Li 2 Y 2 , monoclinic, P2 1 /c (no. 14), a = 6.3683(4) Å, b = 23.888(1) Å, c = 6.4310(4) Å, β = 113.545(2)°, V = 896.9 Å 3 , Z = 4, R gt (F) = 0.0312, wR ref (F 2 ) = 0.0784, T = 293 K
Open Access
Crystal structure of catena-(μ₂-hydroxo)-tris(μ₃-hydroxo)-(μ₆-sulfato)-tricopper( II), Cu₃H₄O₈S

October 18, 2014

Ling Huang, Duan Qiu, Bo Zhao

Page range: 435-436

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Cu 3 H 4 O 8 S, orthorhombic, Pnma (no. 62), a = 8.283(1) Å, b = 6.063(1) Å, c = 12.046(2) Å, V = 604.9 Å 3 , Z = 4, R gt (F) = 0.0234, wR ref (F 2 ) = 0.0649, T = 296 K.
Open Access
Crystal structure of [(1,4-di(1-imidazolyl)benzene-κ²N:N')(μ₂-5-iso nicotinamidoisophthalato-κ²O¹,O³)copper(II)], C₂₆H₁₈CuN₆O₅

October 18, 2014

Yi-Fang Deng, Xue Nie, Chun-Hua Zhang, Man-Sheng Chen

Page range: 437-438

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C 26 H 18 CuN 6 O 5 , triclinic, P1̄ (no. 2), a = 7.652(2) Å, b = 10.026(2) Å, c = 16.727(3) Å, α = 72.832(4)°, β = 78.101(3)°, γ = 79.010(4)°, V = 1188.2 Å 3 , Z = 2, R gt (F) = 0.0585, wR ref (F 2 ) = 0.1368, T = 291 K
Open Access
Crystal structure of 2-aminoethylammonium tris-(1,2-ethanediamine) zinc(II)tetraselenoantimonate(V), (C₂H₉N₂)[Zn(C₂H₈N₂)₃][SbSe₄], C₈H₃₃N₈SbSe₄Zn

October 18, 2014

Prashanth W. Menezes, Thomas F. Fässler

Page range: 439-440

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C 8 H 33 N 8 SbSe 4 Zn, triclinic, P 1̄ (no. 2), a = 8.8100(2) Å, b = 9.6324(2) Å, c = 14.2606(4) Å, α = 104.963(2)°, β = 92.574(2)°, γ = 109.713(3)°, V = 1089.0 Å 3 , Z = 2, R gt (F) = 0.0274, wR ref (F 2 ) = 0.0711, T = 150 K.
Open Access
Synthesis and crystal structure of a new mercury(II) chlorine complex with nitronyl nitroxides, C₁₅H₁₉Cl₄Hg₂N₄O₂

October 18, 2014

Guang-Jian Yang, Ling-Xian Luo

Page range: 441-442

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C 15 H 19 Cl 4 Hg 2 N 4 O 2 , triclinic, P1̄ (no. 2), a = 7.445(2) Å, b = 9.463(2) Å, c = 16.180(3) Å, α = 94.245(2)°, β = 100.747(2)°, γ = 102.523(2)°, V = 1085.5 Å 3 , Z = 2, R gt (F) = 0.0312, wR ref (F 2 ) = 0.0815, T = 291 K.
Open Access
Crystal structure of trans-N₃-(2-chlorobenzylidene)-5-bromopyridine-3,4- diamine, C₁₂H₉BrClN₃

October 18, 2014

Mingjian Cai, Xiuge Wang

Page range: 443-444

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C 12 H 9 BrClN 3 , monoclinic, P2 1 /n (no. 14), a = 3.8743(5) Å, b = 22.229(2) Å, c = 13.631(1) Å, β = 98.103(6)°, V = 1162.2 Å 3 , Z = 4, R gt (F) = 0.0287, wR ref (F 2 ) = 0.0831, T = 113 K.
Open Access
Synthesis and crystal structure of a new mercury(II) complex with imino nitroxide radical, C₃₀H₃₈Cl₆Hg₃N₈O₂

October 18, 2014

Chao-Jun He, En-Pu Zu, Xiao-Jun Zhou

Page range: 445-446

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C 30 H 38 Cl 6 Hg 3 N 8 O 2 , triclinic, P1̄ (no. 2), a = 7.3649(5) Å, b = 11.4075(8) Å, c = 13.0120(9) Å, α = 100.454(1)°, β = 102.089(1)°, γ = 103.229(1)°, V = 1010.0 Å 3 , Z = 1, R gt (F) = 0.0202, wR ref (F 2 ) = 0.0502, T = 291 K.
Open Access
Crystal structure of 2[(4-fluorophenylimino)methyl]-4,6-diiodophenol, C₁₃H₈FI₂NO

October 18, 2014

Zhong-Ming Yang, Hui Zhu, Hai-Liang Zhu

Page range: 447-448

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C 13 H 8 FI 2 NO, monoclinic, Cc (no. 9), a = 4.549(1) Å, b = 35.025(2) Å, c = 17.307(1) Å, β = 95.255(2)°, V = 2745.6 Å 3 , Z = 8, R gt (F) = 0.0674, wR ref (F 2 ) = 0.1701, T = 298 K.
Open Access
Crystal structure of 2-(2,3-dihydrobenzo[1,4]dioxin-6-yl)-5-(4-nitro benzylsulfanyl)-[1,3,4]oxadiazole, C₁₇H₁₃N₃O₅S

October 18, 2014

Hui Zhu, Zhong-Ming Yang, Hai-Liang Zhu

Page range: 449-450

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C 17 H 13 N 3 O 5 S, triclinic, P1̄ (no. 2), a = 7.199(1) Å, b = 8.002(2) Å, c = 14.547(3) Å, α = 96.722(2)°, β = 94.865(2)°, γ= 105.649(2)°, V = 795.5 Å 3 , Z = 2, R gt (F) = 0.0390, wR ref (F 2 ) = 0.0955, T = 298 K.
Open Access
Crystal structure of pentaerythrityl tetrakis(1-methyl-5-mercapto-1,2,3,4- tetrazole), C₁₃H₂₀N₁₆S₄

October 18, 2014

Jiao Guo, Ying-Ying Liu

Page range: 451-452

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C 13 H 20 N 16 S 4 , tetragonal, I4̄ (no. 82), a = 13.2259(4) Å, c = 6.6409(4) Å, V = 1161.7 Å 3 , Z = 2, R gt (F) = 0.0433, wR ref (F 2 ) = 0.1129, T = 293 K.
Open Access
Crystal structure of diaqua-bis-(1,10-phenanthroline)-manganese(II) thiophene-3,4-dicarboxylate heptahydrate, [Mn(H₂O)₂(C₁₂H₈N₂)₂(C₆H₃O₄S)₂]·7H₂O, C₃₆H₃₉MnN₄O₁₇S₂

October 18, 2014

Zhao-Hao Li, Li-Ping Xue

Page range: 453-454

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C 36 H 39 MnN 4 O 17 S 2 , monoclinic, C2/c (no. 15), a = 16.793(3) Å, b = 22.949(2) Å, c = 13.044(2) Å, β = 125.122(7)°, V = 4111.7 Å 3 , Z = 4, R gt (F) = 0.0610, wR ref (F 2 ) = 0.1642, T = 293 K.
Open Access
Crystal structure of 7,7’-bi-1,3,5-cycloheptatrien, C₁₄H₁₄

October 18, 2014

Ute Friedrich, Nikolaus Korber

Page range: 455-456

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C 14 H 14 , triclinic, P1̄ (no. 2), a = 6.450(1) Å, b = 9.614(2) Å, c = 9.712(2) Å, α = 112.11(2)°, β = 100.55(2)°, γ = 99.87(2)°, V = 529.1 Å 3 , Z = 2, R gt (F) = 0.0536, wR ref (F 2 ) = 0.1610, T = 123 K.
Open Access
Crystal structure of catena-[(μ₂-5-methylisophthalato)(μ₂-1,3-bis-(1,2,4- triazol-1-yl)propane)]zinc(II)dihydrate, [Zn(C₉H₆O₄)(C₇H₁₀N₆)]·2H₂O, C₁₆H₂₀N₆O₆Zn

October 18, 2014

Yu-Wei Song, Hong-Bing Yang, Jian-Ge Wang

Page range: 457-458

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C 16 H 20 N 6 O 6 Zn, monoclinic, P2 1 /c (no. 14), a = 9.534(1) Å, b = 21.463(3) Å, c = 10.158(1) Å, β = 110.980(1)°, V = 1940.8 Å 3 , Z = 4, R gt (F) = 0.0331, wR ref (F 2 ) = 0.0804, T = 296 K.
Open Access
Crystal structure of tetrakis-(imidazol-1-ylmethyl)methane cobalt(II) tungstate-monohydrate, [CoWO₄(C₁₇H₂₀N₈)](H₂O), C₁₇H₂₂CoN₈O₅W

October 18, 2014

Jiao Guo, Ying-Ying Liu

Page range: 459-460

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C 17 H 22 CoN 8 O 5 W, monoclinic, P2 1 /n (no. 14), a = 9.4893(2) Å, b = 18.1400(4) Å, c = 12.2891(2) Å, β = 102.035(2)°, V = 2068.9 Å 3 , Z = 4, R gt (F) = 0.0252, wR ref (F 2 ) = 0.0716, T = 293 K.
Open Access
Hydrothemal synthesis and crystal structure of a new compound [Cd(edpa)(2,2'-bpy)(H2O)]_n, C₁₉H₁₇CdN₃O₅

October 18, 2014

Xiao-Ling Li, Ling-Yun Xin, Ming-Qiao Feng

Page range: 461-462

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C 19 H 17 CdN 3 O 5 , monoclinic, C2/c (no. 15), a = 27.369(3) Å, b = 9.126(1) Å, c = 15.326(2) Å, β = 104.285(1)°, V = 3709.6 Å 3 , Z = 8, R gt (F) = 0.0288, wR ref (F 2 ) = 0.0626, T = 296 K
Open Access
Crystal structure of N'-(2-methoxynaphthylidene)-4-dimethylamino benzohydrazide, C₂₁H₂₁N₃O₂

October 18, 2014

Shi-Yong Liu, Mei Zhang

Page range: 463-464

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C 21 H 21 N 3 O 3 , monoclinic, P2 1 /c (no. 14), a = 5.0165(5) Å, b = 13.148(1) Å, c = 26.705(2) Å, β = 90.198(1)°, V = 1761.4 Å 3 , Z = 4, R gt (F) = 0.0656, wR ref (F 2 ) = 0.1768, T = 298 K.
Open Access
Crystal structure of N'-(3-hydroxybenzylidene)-4-dimethylamino benzohydrazide, C₁₆H₁₇N₃O₂

October 18, 2014

Shi-Yong Liu, Dong-Mei Xian

Page range: 465-466

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C 16 H 17 N 3 O 2 , monoclinic, P2 1 /n (no. 14), a = 10.825(3) Å, b = 8.916(2) Å, c = 15.310(2) Å, β = 106.291(2)°, V = 1418.3 Å 3 , Z = 4, R gt (F) = 0.0473, wR ref (F 2 ) = 0.1344, T = 298 K.
Open Access
Crystal structure of N'-(5-bromo-2-hydroxy-3-methoxybenzylidene)-4- hydroxy-3-methoxybenzohydrazide dihydrate, C₁₆H₁₅BrN₂O₅·2H₂O, C₁₆H₁₉BrN₂O₇

October 18, 2014

Dan-Xia Liang, Shi-Yong Liu, Mei Zhang

Page range: 467-468

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C 16 H 19 BrN 2 O 7 , monoclinic, P2 1 /c (no. 14), a = 9.279(2) Å, b = 8.697(2) Å, c = 24.223(2) Å, β = 111.671(2)°, V = 1816.6 Å 3 , Z = 4, R gt (F) = 0.0444, wR ref (F 2 ) = 0.1108, T = 298 K.
Open Access
Crystal structure of N'-(5-bromo-2-hydroxy-3-methoxybenzylidene)-2- methoxybenzohydrazide monohydrate, C₁₆H₁₅BrN₂O₄·H₂O, C₁₆H₁₇BrN₂O₅

October 18, 2014

Dan-Xia Liang, Shi-Yong Liu, Dong-Mei Xian

Page range: 469-470

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C 16 H 17 BrN 2 O 5 , triclinic, P1̄ (no. 2), a = 6.934(1) Å, b = 8.339(2) Å, c = 14.619(2) Å, α = 99.246(2)°, β = 91.861(2)°, γ = 102.506(2)°, V = 812.5 Å 3 , Z = 2,
Open Access
Crystal structure of 4-[(2-phenylbenzimidazole)-methyl]benzoic acid cadmium(II), C₄₂H₃₀CdN₄O₄

October 18, 2014

Jiao Guo, Ying-Ying Liu

Page range: 471-472

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C 42 H 30 CdN 4 O 4 , monoclinic, C2/c (no. 15), a = 9.6025(3) Å, b = 21.6248(5) Å, c = 16.4162(5) Å, β = 96.440(3)°, V = 3387.4 Å 3 , Z = 4, R gt (F) = 0.0340, wR ref (F 2 ) = 0.0880, T = 293 K.
Open Access
Crystal structure of ethyl 2-(5-methyl-4H-1,2,4-triazol-3-yl)acetate, C₇H₁₁N₃O₂

October 18, 2014

Guang-Zhou Zhu, Suo-Ping Xu, Zhong-Ming Yang

Page range: 473-474

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C 7 H 11 N 3 O 2 , triclinic, P1̄ (no. 2), a = 5.0843(3) Å, b = 7.8399(5) Å, c = 12.361(1) Å, α = 107.030(2)°, β = 95.273(1)°, γ = 103.183(1)°, V = 452.0 Å 3 , Z = 2, R gt (F) = 0.0672, wR ref (F 2 ) = 0.1895, T = 298 K.
Open Access
Crystal structure of N'-(5-bromo-2-hydroxy-3-methoxybenzylidene)-4- nitrobenzohydrazide monohydrate, C₁₅H₁₂BrN₃O₅·H₂O, C₁₅H₁₄BrN₃O₆

October 18, 2014

Zhe Hong, Yan Yu, Chun-Lin Du, Peng Liang, Xiao-Xu Xu

Page range: 475-476

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C 15 H 14 BrN 3 O 6 , monoclinic, P2 1 /n (no. 14), a = 4.546(2) Å, b = 13.831(3) Å, c = 26.124(2) Å, β = 91.146(2)°, V = 1642.1 Å 3 , Z = 4, Rgt(F) = 0.0704, wR ref (F 2 ) = 0.1827, T = 298 K.
Open Access
Crystal structure of (4-carboxy-2-sulfonatobenzoato-O,O')-bis-(2,2'- bipyridyl) manganese(II) sesterhydrate, Mn(C₁₀H₈N₂)₂(C₈H₄O₇S)·2.5H₂O, C₂₈H₂₅MnN₄O_9.50S

October 18, 2014

Zhaoxun Lian

Page range: 477-478

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C 28 H 25 MnN 4 O 9.50 S, triclinic, P1̄ (no. 2), a = 9.134(2) Å, b = 9.746(2) Å, c = 16.36(1) Å, α = 100.61(3)°, β = 98.59(3)°, γ = 91.26(2)°, V = 1413.1 Å 3 , Z = 2, R gt (F) = 0.0488, wR ref (F 2 ) = 0.1432, T = 298 K.
Open Access
Crystal structure of tetra-aqua-bis-(pyridine-4-carboxamide-N)-nickel(II) 1,5-naphthalenedisulfonate-isonicotinamide-water (1:2:4), [Ni(H₂O)₄(C₆H₆N₂O)₂][C₁₀H₆S₂O₆]·2C₆H₆N₂O·4H₂O, C₃₄H₄₆N₈NiO₁₈S₂

October 18, 2014

Zhaoxun Lian

Page range: 479-480

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C 34 H 46 N 8 NiO 18 S 2 , triclinic, P1̄ (no. 2), a = 10.345(7) Å, b = 10.864(5) Å, c = 10.895(3) Å, α = 70.87(3)°, β = 74.96(4)°, γ = 78.21(5)°, V = 1107.6 Å 3 , Z = 1, R gt (F) = 0.0453, wR ref (F 2 ) = 0.1241, T = 298 K.
Open Access
Crystal structure of catena-((μ₂-4,4'-biphenyldisulfonato-O,O')-diaquabis( isonicotinamide-N)-copper(II) tetrahydrate, [Cu(H₂O)₂(C₆N₂H₆O)₂](C₁₂H₈S₂O₆)·4H₂O, C₂₄H₃₂CuN₄O₁₄S₂

October 18, 2014

Zhao Ning

Page range: 481-482

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C 24 H 32 CuN 4 O 14 S 2 , triclinic, P1̄ (no. 2), a = 6.796(5) Å, b = 10.414(2) Å, c = 11.55(1) Å, α = 75.33(5)°, β = 77.05(1)°, γ = 78.875(6)°, V = 762.8 Å 3 , Z = 1, R gt (F) = 0.0651, wR ref (F 2 ) = 0.2086, T = 298 K
Open Access
Crystal structure of (3R,6R,Z)-3-hydroxy-3,6-dimethyl-2-(3- methylbutylidene)hexahydrobenzofuran-4(2H)-one, C₁₅H₂₄O₃

October 18, 2014

Biao Zhang, Shuangliang Tian, Xiong He, Jin Yang, Jin Yang, Xueli Hou, Nianyu Huang

Page range: 483-484

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C 15 H 24 O 3 , monoclinic, P2 1 (no. 4), a = 6.83(1) Å, b = 9.29(1) Å, c = 12.81(2) Å, β = 103.29(2)°, V = 790.8 Å 3 , Z = 2, R gt (F) = 0.0869, wR ref (F 2 ) = 0.2471, T = 296 K.
Open Access
Crystal structure of 2-(1H-imidazo-[4,5-c]-pyridine-2-yl)-6-methoxyphenol, C₁₃H₁₁N₃O₂

October 18, 2014

Xinfang Wang

Page range: 485-486

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C 13 H 11 N 3 O 2 , monoclinic, P2+/n (no. 14), a = 7.6199(9) Å, b = 12.357(2) Å, c = 12.460(1) Å, β = 95.139(2)°, V = 1168.5 Å 3 , Z = 4,R gt (F) = 0.0542, wR ref (F 2 ) = 0.1673, T = 293 K.
Open Access
Crystal structure of di-aqua-bis-[1-cyclopropyl-7-(4-ethylpiperazin-1-yl)- 6-fluor-4-oxo-1,4-dihydrochinolin-3-carboxylic acid]zinc(II)bibenzene- 1,4-dicarboxylate octahydrate, [Zn(C₁₉H₂₂N₃FO₃)₂(H₂O)_2]·2(C₈H₅O₄)·8(H₂O), C₅₄H₇₄F₂N₆O₂₄Zn

October 18, 2014

Xin-Ping Kang, Zhe An, Rena Kasimu

Page range: 487-488

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C 54 H 74 F 2 N 6 O 24 Zn, monoclinic, P2 1 /n (no. 14), a = 13.5443(3) Å, b = 13.7558(4) Å, c = 16.6644(4) Å, β = 106.666(2)°, V = 2974.4 Å 3 , Z = 2, R gt (F) = 0.0550, wR ref (F 2 ) = 0.1444, T = 296 K.
Open Access
Crystal structure of 2-amino-4,6-dimethylpyrimidinium hydrogen oxalate, C₈H₁₁N₃O₄

October 18, 2014

Cui-Hua Lin, Nai-Sheng Liu

Page range: 489-490

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C 8 H 11 N 3 O 4 , monoclinic, P2 1 /c (no. 14), a = 3.9213(7) Å, b = 14.556(1) Å, c = 17.268(2) Å, β = 102.410(2)°, V = 962.6 Å 3 , Z = 4, R gt (F) = 0.0659, wR ref (F 2 ) = 0.2386, T = 293 K.
Open Access
Crystal structure of [N'-(2-hydroxynaphthyl)ethylidene]-4-dimethyl aminobenzohydrazide, C₂₁H₂₁N₃O₂

October 18, 2014

Shi-Yong Liu, Hai-Hua Li

Page range: 491-492

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C 21 H 21 N 3 O 2 , monoclinic, P2 1 /n (no. 14), a = 10.111(2) Å, b = 6.623(2) Å, c = 26.969(2) Å, β = 98.241(2)°, V = 1787.3 Å 3 , Z = 4, R gt (F) = 0.0578, wR ref (F 2 ) = 0.1544, T = 298 K.
Open Access
Crystal structure of 2-amino-4,6-dimethylpyrimidinium dichloroacetate, C₈H₁₁Cl₂N₃O₂

October 18, 2014

Cui-Hua Lin, Nai-Sheng Liu

Page range: 493-494

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C 8 H 11 Cl 2 N 3 O 2 , triclinic, P1̄ (no. 2), a = 6.887(1) Å, b = 8.572(2) Å, c = 11.074(2) Å, α = 112.600(2)°, β = 95.183(1)°, γ = 101.874(1)°, V = 580.2 Å 3 , Z = 2, R gt (F) = 0.0422, wR ref (F 2 ) = 0.1211, T = 293 K.
Open Access
Crystal structure of 2-hydroxybenzylidene-5-methylisoxazole-4- carbohydrazide monohydrate, C₁₂H₁₃N₃O₄

October 18, 2014

Ai-Guo Zhong

Page range: 495-496

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C 12 H 13 N 3 O 4 , orthorhombic, Pna2 1 (no. 33), a = 12.8783(6) Å, b = 11.3108(6) Å, c = 8.6535(4) Å, V = 1260.5 Å 3 , Z = 4, R gt (F) = 0.0323, wR ref (F 2 ) = 0.0922, T = 296 K.
Open Access
Crystal structure of bis-{1-[1-(3-aminopentylimino)ethyl]naphthalen-2- olato}nickel(II), [Ni(C₁₇H₂₁N₂O)₂], C₃₄H₄₂N₄NiO₂

October 18, 2014

Bao-Hui Li

Page range: 497-498

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C 34 H 42 N 4 NiO 2 , monoclinic, P2 1 /n (no. 14), a = 9.426(2) Å, b = 15.610(3) Å, c = 10.018(2) Å, β = 92.115(2)°, V = 1473.0 Å 3 , Z = 2, R gt (F) = 0.0699, wR ref (F 2 ) = 0.1333, T = 298 K.
Open Access
Crystal structure of 2,3-dihydro-2-phenyl-3-[(E)-(1-phyenylethylidene) amino]-4(1H)-quinazolinone, C₂₂H₁₉N₃O

October 18, 2014

Zai-Sheng Lu, Xiang-Shan Wang, Guang-Zhou Zhu, Xiu-Lin Li, De-Zhong Niu

Page range: 499-500

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C 22 H 19 N 3 O, monoclinic, C2/c (no. 15), a = 10.597(5) Å, b = 13.740(6) Å, c = 24.82(1) Å, β = 94.764(5)°, V = 3600.9 Å 3 , Z = 8, R gt (F) = 0.0374, wR ref (F 2 ) = 0.1120, T = 296 K.
Open Access
Crystal structure of 2,3-dihydro-2-(4-nitrophenyl)-4H-1-benzopyran-4- one, C₁₅H₁₁NO₄

October 18, 2014

Yunhui Sun, Huihui Chen, Hongyu Chen, Duxia Cao, Zhiqiang Liu

Page range: 501-502

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C 15 H 11 NO 4 , triclinic, P1̄ (no. 2), a = 7.791(5)Å, b = 8.452(5)Å, c = 9.977(5) Å, α = 90.780(5)°, β = 104.066(5)°, γ = 93.562(5)°, V = 635.8 Å 3 , Z = 2, R gt (F) = 0.0503, wR ref (F 2 ) = 0.1226, T = 293 K.
Open Access
Crystal structure of catena-(5-tert-butylisophthalic)cadmium(II)-[1,4-bis- (2-methyl-imidazol-1-yl)butane], [Cd(C₁₂H₁₂O₄)(C₁₂H₁₈N₄)]n, C₁₈H₂₁CdN₂O₄

October 18, 2014

Wei-Wei Lu, Feng-Yang Ju

Page range: 503-504

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C 18 H 21 CdN 2 O 4 , triclinic, P1̄ (no. 2), a = 9.101(1) Å, b = 10.175(1) Å, c = 10.962(1) Å, α = 65.170(1)°, β = 75.095(1)°, γ = 88.586(1)°, V = 886.1 Å 3 , Z = 2, R gt (F) = 0.0216, wR ref (F 2 ) = 0.0557, T = 296 K.
Open Access
Crystal structure of 5,8-dimethyl-6-(p-dimethylaminophenylethynyl)-2,2- diphenyl- 2H-1-benzopyran, C₃₃H₂₉NO

October 18, 2014

Lucie Chabreuil, Corinne Moustrou, Gérard Pèpe

Page range: 505-506

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C 33 H 29 NO, monoclinic, P2 1 /a (no. 14), a = 16.832(3) Å , b = 9.325(2) Å, c = 16.999(3) Å, β = 105.03(6)°, V = 2576.9(9) Å 3 , Z = 4, R gt (F) = 0.0407, wR ref (F 2 ) = 0.2999, T = 293 K.
Open Access
Crystal structure of 5,8-dimethyl-6-(p-dimethylaminophenyl)-2,2- diphenyl-2H-1-benzopyran, C₃₄H₃₆NO

October 18, 2014

Lucie Chabreuil, Corinne Moustrou, Gérard Pèpe

Page range: 507-508

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C 34 H 36 NO, monoclinic, P2 1 /c (no. 14), a = 13.898(3) Å, b = 10.584(2) Å, c = 18.554(5) Å, β = 96.62(6)°, V = 2711.0(11) Å 3 , Z = 4, R gt (F) = 0.0385, wR ref (F 2 ) = 0.2161, T = 293 K
Open Access
Crystal structure of bis(diethylether)bis(fluorenyl)magnesium, [Mg(C₁₃H₉)₂(Et₂O)₂], C₃₄H₃₈MgO₂

October 18, 2014

Ulrich Behrens, Elena Aglaia Dimos

Page range: 509-510

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C 34 H 38 MgO 2 , monoclinic, P2 1 /c (no. 14), a = 10.321(1) Å, b = 16.365(2) Å, c = 16.981(2) Å, β = 104.615(2)°, V = 2775.3 Å 3 , Z = 4, R gt (F) = 0.0595, wR ref (F 2 ) = 0.1665, T = 153 K
Open Access
Crystal structure of Mn(II)(H₂O)(2,13-dimethyl-3,6,9,12,18-pentaazabicyclo[ 12.3.1]octadeca-1(18),2,12,14,16-pentaene)-bis-(maleonitriledithiolate) nickel(II), C₂₃H₂₅MnN₉NiOS₄

October 18, 2014

Ping Wang

Page range: 511-512

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C 23 H 25 MnN 9 NiOS 4 , monoclinic, P2 1 /c (no. 14), a = 19.48(1) Å, b = 7.462(4) Å, c = 21.41(1) Å, β = 109.824(8)°, V = 2928.6 Å 3 , Z = 4, R gt (F) = 0.0811, wR ref (F 2 ) = 0.2123, T = 293 K.
Open Access
Crystal structure of tert-butyl-3-(4-oxo-2-thioxo-3,4-dihydropyrimidin- 1(2H)-yl)propanoate, C₁₁H₁₅N₂O₃S

October 18, 2014

Wei Yuan, Jian-Ping Liu, Xia Song

Page range: 513-514

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C 11 H 15 N 2 O 3 S, monoclinic, P2 1 /c (no. 14), a = 11.852(2) Å, b = 7.467(1) Å, c = 15.548(2) Å, β = 103.983(2)°, V = 1335.2 Å 3 , Z = 4, R gt (F) = 0.1500, wR ref (F 2 ) = 0.2809, T = 298 K.
Open Access
Crystal structure of 3,5-dibromopyridin-2-amine, C₅H₄Br₂N₂

October 18, 2014

Zhan-Jiang Jiao, Shan-Shan Huang, Chuan-Xun Li, Yun-Peng Diao

Page range: 515-516

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C 5 H 4 Br 2 N 2 , monoclinic, P2 1 /n (no. 14), a = 6.07(1) Å, b = 10.53(2) Å, c = 11.89(2) Å, β = 104.49(3)°, V = 736.0 Å 3 , Z = 4, R gt (F) = 0.0307, wR ref (F 2 ) = 0.0795, T = 296 K.
Open Access
Crystal structure of (4,4'-bipyridine)-(4-hydroxypyridine-2,6-dicarboxylato)- zinc(II) hydrate, [Zn₂(C₁₀H₈N₂)(C₇H₃NO₅)₂(H₂O)₂]·4H₂O, C₂₄H₂₆N₄O₁₆Zn₂

October 18, 2014

Hua-Li Cui, Xiao-Li Chen, Ya-Li Qiao, Mei-Li Zhang, Jung-Fang Lv

Page range: 517-518

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C 24 H 26 N 4 O 16 Zn 2 , orthorhombic, Pbca (no. 61), a = 19.904(3) Å, b = 7.0438(9) Å, c = 20.240(3) Å, V = 2837.6 Å 3 , Z = 4, R gt (F) = 0.0279, wR ref (F 2 ) = 0.0772, T = 296 K.
Open Access
Crystal structure of 2,4,6-pyrimidinetriamine-trifluoroacetate(1:1), C₄H₈N₅⁺C₂F₃O₂^–, C₆H₈F₃N₅O₂

October 18, 2014

Zongyang Li, Yubo Li, Haixiang Gao, Fengpei Du

Page range: 519-520

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C 6 H 8 F 3 N 5 O 2 , monoclinic, P2 1 /n (no. 14), a = 5.718(1) Å, b = 13.990(3) Å, c = 12.223(2) Å, β = 102.67(3)°, V = 954.0 Å 3 , Z = 4, R gt (F) = 0.0510, wR ref (F 2 ) = 0.1551, T = 293 K
Open Access
Crystal structure of bis-[N,N'-bis-(3-allyl salicylidene)-o-phenylene diamine]thorium (IV), C₅₂H₄₄N₄O₄Th

October 18, 2014

Fang-Fang He, Hong-Qing Wang, Xiao-Feng Wang, Yu-Yuan Wang

Page range: 521-524

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C 52 H 44 N 4 O 4 Th, triclinic, P1̄ (no. 2), a = 16.3338(3) Å, b = 17.1662(3) Å, c = 18.5769(6) Å, α = 101.145(1)°, β = 95.195(1)°, γ = 117.054(1)°, V = 4455.6 Å 3 , Z = 4, R gt (F) = 0.0314, wR ref (F 2 ) = 0.0914, T = 296 K.
Open Access
Crystal structure of 2-amino-5,6-dihydro-7(4H)-benzothiazolone, C₇H₈N₂OS

October 18, 2014

Guang-Zhou Zhu, Zai-Sheng Lu, Han Lu, Xiang-Shan Wang

Page range: 525-526

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C 7 H 8 N 2 OS, monoclinic, P2 1 /c (no. 14), a = 6.432(3) Å, b = 14.898(8) Å, c = 8.165(4) Å, β = 95.294(5)°, V = 779.1 Å 3 , Z = 4, R gt (F) = 0.0337, wR ref (F 2 ) = 0.0942, T = 296 K.
Open Access
Crystal structure of bis{1-[(benzotriazol-1-yl)methyl]-1-H-1,3-(2-methylimdazol)} di-iodidocadmium(II), [Cd(C₁₁H₁₁N₅)₂I₂], C₂₂H₂₂CdI₂N₁₀

October 18, 2014

Hai-Yan Yang, Ying-Hua Li, Hong Chen

Page range: 527-528

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C 22 H 22 CdI 2 N 10 , monoclinic, P2 1 /c (no. 14), a = 7.456(2) Å, b = 27.667(6) Å, c = 13.607(3) Å, β = 104.44(3)°, V = 2718.2 Å 3 , Z = 4, R gt (F) = 0.0464, wR ref (F 2 ) = 0.0938, T = 293 K.
Open Access
Crystal structure of 2-amino-5,6,7,8-tetrahydro-4,7,7-trimethyl-4-(4- nitrophenyl)-5-oxo-4H-chromene-3-carbonitrile DMF solvate, C₁₉H₁₉N₃O₅·DMF, C₂₂H₂₆N₄O₅

October 18, 2014

Pei-Jun Cai, Xiao-Feng Guo, Jun-Hao Huo, Chong Shi

Page range: 529-530

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C 22 H 26 N 4 O 5 , triclinic, P1̄ (no. 2), a = 8.4753(6) Å, b = 9.5662(7) Å, c = 14.479(1) Å, α = 101.674(4)°, β = 93.813(4)°, γ= 104.676(4)°, V = 1103.5 Å 3 , Z = 2, R gt (F) = 0.0581, wR ref (F 2 ) = 0.1863, T = 296 K.
Open Access
Microwave solid phase synthesis and crystal structure of 2,4-diiodo-6- [(3-nitro-phenylimino)-methyl]-phenol, C₁₃H₈I₂N₂O₃

October 18, 2014

Suo-Ping Xu, Han Lu, Tuan-Jie Li

Page range: 531-532

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C 13 H 8 I 2 N 2 O 3 , orthorhombic, Pbcm (no. 57), a = 9.104(2) Å, b = 23.654(3) Å, c = 6.696(2) Å, V = 1442.0 Å 3 , Z = 4, R gt (F) = 0.0392, wR ref (F 2 ) = 0.1508, T = 298 K.
Open Access
Crystal structure of (Z)-N'-[amino(pyridin-2-yl)-methylene]-2-hydroxybenzohydrazide, C₁₃H₁₂N₄O₂

October 18, 2014

Guang-Zhou Zhu, Zai-Sheng Lu, Huan-Le Shi, Suo-Ping Xu, Huan Lu, Xiang-Shan Wang

Page range: 533-534

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C 13 H 12 N 4 O 2 , monoclinic, Cc (no. 9), a = 8.749(4) Å, b = 17.707(8) Å, c = 8.005(4) Å, β = 102.751(5)°, V = 1209.5 Å 3 , Z = 4, R gt (F) = 0.0270, wR ref (F2) = 0.0701, T = 296 K
Open Access
Crystal structure of (E)-1,2-bis(9-hexyl-9H-carbazol-3-yl)ethene, C₃₈H₄₂N₂

October 18, 2014

Long-Qiang Shi, Zhi Liu, Wei Guo, Dan Zhao, Lei Wang, Wen-Tao Yu, De-Liang Cui, Xu-Tang Tao

Page range: 535-537

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C 38 H 42 N 2 , monoclinic, P2 1 /c (no. 14), a = 5.1381(4) Å, b = 14.238(1) Å, c = 21.372(2) Å, β = 92.359(4)°, V = 1562.2 Å 3 , Z = 2, R gt (F) = 0.0863, wR ref (F 2 ) = 0.2868, T = 130(2) K.
Open Access
Crystal structure of aqua-bis-(2,2'-bipyridyl-N,N)(7-hydroxynaphthalene- 1,3-disulfonato) cadmium(II) monohydrate, [Cd(H₂O)(C₁₀N₂H₈)₂](C₁₀H₆S₂O₇)·H₂O, C₃₀H₂₆CdN₄O₉S₂

October 18, 2014

Li Chunying, Zhao Ning

Page range: 538-540

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C 30 H 26 CdN 4 O 9 S 2 , monoclinic, P2 1 /n (no. 14), a = 14.1889(2) Å, b = 15.6921(1) Å, c = 14.2049(2) Å, β = 105.449(1)°, V = 3048.5 Å 3 , Z = 4, R gt (F) = 0.0491, wR ref (F 2 ) = 0.1626, T = 298 K.
Open Access
Crystal structure of bis-(3-butyl-1-(1,10-phenanthrolin-2-yl) imidazolylidene)iridium(III) tris-hexafluorophosphate acetonitrile monosolvate, [Ir(C₁₉H₁₈N₄)₂(PF₆)₃]·(C₂H₃N), C₄₀H₃₉F₁₈IrN₉P₃

October 18, 2014

Jing-Jing Huang

Page range: 541-543

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C 40 H 39 F 18 IrN 9 P 3 , triclinic, P1̄ (no. 2), a = 13.199(1) Å, b = 13.452(1) Å, c = 13.453(1) Å, α = 88.099(2)°, β = 79.526(1)°, γ = 89.597(2)°, V = 2347.4 Å 3 , Z = 2, R gt (F) = 0.0500, wR ref (F 2 ) = 0.1365, T = 298 K.
Open Access
Crystal structure of μ-oxido-bis{2,2-[ethylidene(bis-(nitrilomethylidyne))] diphenolato} iron(III), [Fe₂O(C₁₆H₁₄N₂)₂]·2.5(C₇H₈), C_49.50H₄₈Fe₂N₄O₅

October 18, 2014

Liang-Zhao Li, Guo-Lin Song, Guo-Yi Tang

Page range: 544-546

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C 49.50 H 48 Fe 2 N 4 O 5 , monoclinic, P2 1 /c (no. 14), a = 12.7141(9) Å, b = 16.559(1) Å, c = 21.164(2) Å, β = 100.628(1)°, V = 4379.4 Å 3 , Z = 4, R gt (F) = 0.0624, wR ref (F 2 ) = 0.1592, T = 187 K.
Open Access
Crystal structure of (Bu4N)2[Mo6O18N(o-CH₃C₆H₃OOCCH₂CH₃)], C₄₂H₈₃Mo₆N₃O₂₀

October 18, 2014

Li Zhu, Yan-Fang Zhong, Xi-Yan Cao

Page range: 547-549

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C 42 H 83 Mo 6 N 3 O 20 , triclinic, P1̄ (no. 2), a = 12.683(3) Å, b = 12.878(4) Å, c = 19.433(6) Å, α = 74.27(2)°, β = 72.36(2)°, γ = 77.34(2)°, V = 2878.8 Å 3 , Z = 2, R gt (F) = 0.0664, wR ref (F 2 ) = 0.2268, T = 296 K.
Open Access
Crystal structure of aqua-bis-(2,2'-bipyridyl-N,N')(7-hydroxy naphthalene- 1,3-disulfonato) nickel(II), [Ni(H₂O)(C₁₀N₂H₈)₂(C₁₀H₆S₂O₇)], C₃₀H₂₄N₄NiO₈S₂

October 18, 2014

Chunying Li, Ning Zhao

Page range: 550-552

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C 30 H 24 N 4 NiO 8 S 2 , triclinic, P1̄ (no. 1), a = 8.059(3) Å, b = 8.2730(7) Å, c = 10.996(7) Å, α = 95.56(3)°, β = 96.98(4)°, γ = 96.54(2)°, V = 718.4 Å 3 , Z = 1, R gt (F) = 0.0280, wR ref (F 2 ) = 0.0935, T = 293 K.
Open Access
Crystal structure of tri-aqua-(pyridine-4-carboxamide-N)copper(II)2,7- naphthalenedisulfonate trihydrate, [Cu(H₂O)₃(C₆H₆N₂O)₂](C₁₀H₆O₆S₂)·3H₂O, C₂₂H₃₀CuN₄O₁₄S₂

October 18, 2014

Chunying Li, Ning Zhao

Page range: 553-555

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C 22 H 30 CuN 4 O 14 S 2 , monoclinic, Cc (no. 9), a = 13.453(3) Å, b = 15.082(3) Å, c = 14.961(3) Å, β = 99.41(3)°, V = 2994.7 Å 3 , Z = 4, R gt (F) = 0.0444, wR ref (F 2 ) = 0.1260, T = 298 K.
Open Access
Crystal structure of aqua-bis-[1-cyclopropyl-7-(4-ethylpiperazin-1-yl)-6- fluor-4-oxo-1,4-dihydrochinolin-3-carboxylato]copper(II), [Cu(C₁₉H₂₁N₃FO₃)₂(H₂O)]·2.5(H₂O), C₃₈H₄₉CuF₂N₆O_9.50

October 18, 2014

Zhu Ling

Page range: 556-558

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C 38 H 49 CuF 2 N 6 O 9.50 , triclinic, P1̄ (no. 2), a = 11.891(2) Å, b = 12.354(3) Å, c = 15.369(3) Å, α = 69.25(3)°, β = 70.34(3)°, γ = 84.00(3)°, V = 1987.9 Å 3 , Z = 2, R gt (F) = 0.0437, wR ref (F 2 ) = 0.1508, T = 293 K.
Open Access
Crystal structure of pentaphenylferrocenium tetrafluoroborate, C₄₀H₃₀BF₄Fe

October 18, 2014

Wolfgang Frey, Simon H. Eitel, René Peters

Page range: 559-561

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C 40 H 30 BF 4 Fe, monoclinic, P2 1 /n (no. 14), a = 9.8978(6) Å, b = 18.7154(10) Å, c = 16.7027(10) Å, β = 94.144(4)°, V = 3085.9(3) Å 3 ,Z = 4, R gt (F) = 0.0452, wR ref (F 2 ) = 0.1185, T = 100 K.
Open Access
Crystal structure of {2-[2-(1H-inden-3-yl)-2-phenylethyl]-1H-imidazolyl- κN¹}-tris[N,N-diethylamido-κN]titanium(IV), C₃₂H₄₇N₅Ti

October 18, 2014

Bingfeng Ma, Qi Sun, Wanli Nie, Maxim V. Borzov

Page range: 562-564

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C 32 H 47 N 5 Ti, orthorhombic, Pbca (no. 61), a = 16.100(2) Å, b = 19.904(2) Å, c = 20.196(2) Å, V = 6472.3 Å 3 , Z = 8, R gt (F) = 0.0405, wR ref (F 2 ) = 0.1178, T = 293 K.
Open Access
Crystal structure of catena-(5-bromoisophthalate)manganese(II)-[1,4-bis- (imidazol-1-ylmethyl)benzene], [Mn(C₇H₃O₄Br)(C₁₄H₁₄N₄)]_n, C₂₂H₁₇BrMnN₄O₄

October 18, 2014

Wei-Wei Lu, Feng-Yang Ju

Page range: 565-567

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C 22 H 17 BrMnN 4 O 4 , triclinic, P1̄ (no. 2), a = 9.358(2) Å, b = 10.258(2) Å, c = 13.016(3) Å, α = 89.383(3)°, β = 78.588(3)°, γ = 63.127(3)°, V = 1088.1 Å 3 , Z = 2, R gt (F) = 0.0350, wR ref (F 2 ) = 0.0886, T = 296 K.
Open Access
Crystal structure of (1,10-phenanthroline) (tetrafluorophtahlato) copper(II), [Cu(C₈F₄O₄)(C₁₂H₈N₂)₂](C₈H₂F₄O₄), C₄₀H₁₈CuF₈N₄O₈

October 18, 2014

Jun Zhang, Yuan-Ying Liu, Kun Ying

Page range: 568-570

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C 40 H 18 CuF 8 N 4 O 8 , triclinic, P1̄ (no. 2), a = 11.499(2) Å, b = 11.806(2) Å, c = 14.516(3) Å, α = 111.86(3)°, β = 101.90(3)°, γ = 95.54(3)°, V = 1756.8 Å 3 , Z = 2, R gt (F) = 0.0390, wR ref (F 2 ) = 0.0796, T = 293 K.
Open Access
Crystal structure of catena-(μ₂-4,4'-bipyridine)silver(I)hydrogen-bis-(5- nitro-1,2-carboxybenzene-3-carboxylato)tetrahydrate, [Ag(C₁₀H₈N₂)]·(C₁₈H₉O₁₆N₂)·4H₂O, C₂₈H₂₅AgN₄O₂₀

October 18, 2014

Min-Le Han, Shi-Hui Li

Page range: 571-573

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C 28 H 25 AgN 4 O 20 , triclinic, P1̄ (no. 2), a = 8.3973(9) Å, b = 9.519(1) Å, c = 11.273(1) Å, α = 66.089(1)°, β = 82.176(1)°, γ = 78.375(1)°, V = 805.3 Å 3 , Z = 1, R gt (F) = 0.0244, wR ref (F 2 ) = 0.0686, T = 296 K.
Open Access
Crystal structure of diaqua-bis(5-nitrobenzene-3-carboxy-1,2-dicarboxylato)- bis(1-(3-(1H-benzimidazol-1-yl)propyl)-benzimidazole)manganese( II), [Mn(H₂O)₂(O₂NC₉H₃O₆)₂(C₁₇H₁₇N₄)₂], C₅₂H₄₄MnN₁₀O₁₈

October 18, 2014

Min-Le Han, Xun-Li Ling

Page range: 574-576

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C 52 H 44 MnN 10 O 18 , monoclinic, P2 1 /c (no. 14), a = 8.6941(8) Å, b = 12.970(1) Å, c = 21.384(2) Å, β = 95.145(1)°, V = 2401.5 Å 3 , Z = 2, R gt (F) = 0.0376, wR ref (F 2 ) = 0.0900, T = 296 K.
Open Access
Crystal structure of catena-[(μ₄-bromo)-tetrakis(μ₃-bromo)-octakis(μ₃- isonicotinato)-tris(μ₂-bromo)-hexakis(μ₂-isonicotinato)-deca-aqua-decacopper( I)-tetra-terbium(III) dihydrate], C₄₂H₄₀Br₄Cu₅N₇O₂₀Tb₂

October 18, 2014

Le-Qing Fan

Page range: 577-579

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C 42 H 40 Br 4 Cu 5 N 7 O 20 Tb 2 , monoclinic, P2/c (no. 13), a = 17.677(5) Å, b = 9.812(2) Å, c = 32.145(8) Å, β= 103.625(4)°, V = 5418.6 Å 3 , Z = 4, R gt (F) = 0.0483, wR ref (F 2 ) = 0.1355, T = 293 K.
Open Access
Crystal structure of an aluminum spirocyclic hybrid complex, C₂₉H₄₁N₂AlO₃B₂(C₁₂H₇O)₂, C₅₃H₅₅AlB₂N₂O₅

October 18, 2014

Xiaoli Ma, Mingdong Zhong, Zhihong Liu, Shuai Sun

Page range: 580-582

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C 53 H 55 AlB 2 N 2 O 5 , triclinic, P 1 ̄ (no. 2), a = 11.663(4) Å, b = 13.476(5) Å, c = 15.988(7) Å, α = 89.70(2)°, β = 83.21(2)°, γ = 67.01(1)°, V = 2294.7 Å 3 , Z = 2, R gt (F) = 0.0659, wR ref (F 2 ) = 0.1611, T = 153 K.
Open Access
Crystal structure of 4-(4-(N-(5,6-dimethoxypyrimidin-4-yl)sulfamoyl) phenylcarbamoyl)-2,6-dimethoxyphenyl acetate, C₂₃H₂₄N₄O₉S

October 18, 2014

Wei-Gao Pan, Zhi-Dong Zhao, Peng Luo, Cui-Wu Lin, Jian-Hua Miao

Page range: 583-585

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C 23 H 24 N 4 O 9 S, triclinic, P 1 ̄ (no. 2), a = 8.297(1) Å, b = 11.199(1) Å, c = 13.876(2) Å, α = 88.856(2)°, β = 76.540(2)°, γ = 80.098(2)°, V = 1235.0 Å 3 , Z = 2, R gt (F) = 0.0405, wR ref (F 2 ) = 0.1084, T = 296 K.

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