Zeitschrift für Kristallographie - New Crystal Structures

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Volume 218, Issue 4

February 2014

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

Open Access
Crystal structure of manganese gallium germanium silicon oxide (garnet type), Mn₃(Ga_2–yMn_y)(Ge_3–zSi_z)O₁₂ (y = 0.6, z = 0.14; y = 0.44, z = 0), and of manganese gallium germanium silicon oxide (braunite type), Mn(Mn_6–yGa_y)(Si_1–zGe_z)O₁₂ (y = 0.7, z = 0.4)

February 11, 2014

R. Wartchow, L. Müller, M. Binnewies

Page range: 373-375

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Ga 1.4 Ge 2.86 Mn 3.6 O 12 Si 0.14 ( 1 ), cubic, Ia 3̅ d (No. 230), a = 12.043(3) Å, V = 1746.6 Å 3 , Z = 8, R gt (F) = 0.028, wR ref (F 2 ) = 0.062, T = 300 K. Ga 1.56 Ge 3 Mn 3.44 O 12 ( 2 ), cubic, Ia 3̅ d (No. 230), a = 12.049(3) Å, V = 1749.3 Å 3 , Z = 8, R gt (F) = 0.023, wR ref (F 2 ) = 0.052, T = 300 K. Ga 0.7 Ge 0.4 Mn 6.3 O 12 Si 0.6 ( 3 ), tetragonal, I 4 1 / acd (No. 142), a = 9.464(4) Å, c = 18.78(3) Å, V = 1682.1 Å 3 , Z = 8, R gt (F) = 0.023, wR ref (F 2 ) = 0.053, T = 300 K.
Open Access
Crystal structure of tricerium dialuminide diiodide, Ce₃Al₂I₂

February 11, 2014

Hj. Mattausch, A. Simon

Page range: 376-376

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Al 2 Ce 3 I 2 , monoclinic, C 12/ m 1 (No. 12), a = 19.542(2) Å, b = 4.272(1) Å, c = 12.198(2) Å, β = 121.35(2)°, V = 869.7 Å 3 , Z = 4, R gt (F) = 0.042, wR ref (F 2 ) = 0.107, T = 293 K.
Open Access
Crystal structure of discandium tris-monohydrogenphosphate(III), Sc₂(HPO₃)₃

February 11, 2014

B. Ewald, Yu. Prots, R. Kniep

Page range: 377-378

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H 3 O 9 P 3 Sc 2 , hexagonal, P 6 3 / m (No. 176), a = 8.3055(7) Å, c = 7.697(1) Å, V = 459.8 Å 3 , Z = 2, R gt (F) = 0.028, wR ref (F 2 ) = 0.061, T = 293 K.
Open Access
Crystal structure of rubidium copper silver oxide, Rb₃Cu_0.5Ag_0.5O₂

February 11, 2014

M. Sofin, E.-M. Peters, M. Jansen

Page range: 379-380

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Ag 0.5 Cu 0.5 O 2 Rb 3 , tetragonal, P 4 1 2 1 2 (No. 92), a = 9.0169(3) Å, c = 14.1195(6) Å, V = 1148.0 Å 3 , Z = 8, R gt (F) = 0.054, wR ref (F 2 ) = 0.150, T = 293 K.
Open Access
Crystal structure of trichloro(N-trimethylsilyl)phosphoraniminetrichloroaluminum, [(CH3)₃Si(N)PCl₃AlCl₃]

February 11, 2014

B. Jäschke, M. Jansen

Page range: 381-382

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C 3 H 9 AlCl 6 NPSi, monoclinic, P 12 1 / c 1 (No. 14), a = 15.541(3) Å, b = 12.615(2) Å, c = 16.210(3) Å, β = 116.128(2)°, V = 2853.3 Å 3 , Z = 8, R gt (F) = 0.077, wR ref (F 2 ) = 0.231, T = 100 K.
Open Access
Crystal structure of tetrasodium tetraselenidosilicate(IV), Na₄SiSe₄

February 11, 2014

H. Preishuber-Pflügl, K. O. Klepp

Page range: 383-384

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Na 4 Se 4 Si, orthorhombic, Pnma (No. 62), a = 14.182(5) Å, b = 9.208(3) Å, c = 7.122(3) Å, V = 930.0 Å 3 , Z = 4, R gt (F) = 0.066, wR ref (F) = 0.059, T = 294 K.
Open Access
Refinement of the crystal structure of dirubidium trithioargentate(I), Rb₂Ag₄S₃

February 11, 2014

K. O. Klepp, M. Sing

Page range: 385-386

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Ag 4 Rb 2 S 3 , monoclinic, C 12/ m 1 (No. 12), a = 17.808(8) Å, b = 4.310(2) Å, c = 11.799(5) Å, β = 108.55(2)°, V = 858.6 Å 3 , Z = 4, R gt (F) = 0.038, wR obs (F) = 0.038, T = 294 K.
Open Access
Crystal structure of tetrarubidium hexathiodigermananate(IV), Rb₄Ge₂S₆

February 11, 2014

H. Preishuber-Pflügl, K. O. Klepp

Page range: 387-388

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Ge 2 Rb 4 S 6 , monoclinic, C 12/ m 1 (No. 12), a = 13.43(5) Å, b = 6.898(3) Å, c = 11.15(3) Å, β = 135.06(9)°, V = 729.7 Å 3 , Z = 2, R gt (F) = 0.043, wR ref (F) = 0.052, T = 296 K.
Open Access
Crystal structure of tricalcium tantalum trigallium disilicon oxide, Ca₃TaGa₃Si₂O₁₄

February 11, 2014

Z.-M. Wang, W.-T. Yu, D.-R. Yuan, X.-Q. Wang, G. Xue, X.-Z. Shi, D. Xu, M.-K. Lv

Page range: 389-390

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Ca 3 Ga 3 O 14 Si 2 Ta, trigonal, P 321 (No. 150), a = 8.1081(4) Å, c = 4.9850(4) Å, V = 283.8 Å 3 , Z = 1, R gt (F) = 0.025, wR ref (F 2 ) = 0.064, T = 293 K.
Open Access
Crystal structure of iron nickel phosphide, Fe_1.7Ni_1.3P, a Schreibersite extracted from Canyon Diablo meteorite

February 11, 2014

O. Moretzki, Th. Doering, V. Geist, W. Morgenroth, M. Wendschuh

Page range: 391-392

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Fe 1.7 Ni 1.3 P 8 , tetragonal, I 4̅ (No. 82), a = 9.049(1) Å, c = 4.4646(9) Å, V = 365.6 Å 3 , Z = 8, R gt (F) = 0.042, wR ref (F 2 ) = 0.093, T = 293 K
Open Access
Crystal structure of iron nickel phosphide, Fe_1.65Ni_1.35P, a Rhabdite extracted from Morasko meteorite

February 11, 2014

O. Moretzki, Th. Doering, V. Geist, W. Morgenroth, M. Wendschuh

Page range: 393-394

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Fe 1.65 Ni 1.35 P 8 , tetragonal, I 4̅ (No. 82), a = 9.059(2) Å, c = 4.479(1) Å, V = 367.6 Å 3 , Z = 8, R gt (F) = 0.022, wR ref (F 2 ) = 0.049, T = 293 K.
Open Access
Crystal structure of iron nickel phosphide, Fe1.8Ni1.2P, a Schreibersite extracted from Orange River meteorite

February 11, 2014

O. Moretzki, Th. Doering, V. Geist, W. Morgenroth, M. Wendschuh

Page range: 395-396

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Fe 1.8 Ni 1.2 P 8 , tetragonal, I 4̅ (No. 82), a = 9.085(5) Å, c = 4.481(3) Å, V = 369.8 Å 3 , Z = 8, R gt (F) = 0.037, wR ref (F 2 ) = 0.086, T = 293 K.
Open Access
Crystal structure of barium europium germanide, Ba_6-xEu_xGe₂₅ (x = 0.6), a chiral clathrate

February 11, 2014

W. Carrillo-Cabrera, R. Cardoso Gil, S. Paschen, Yu. Grin

Page range: 397-398

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Ba 5.40 Eu 0.60 Ge 25 , cubic, P 4 1 32 (No. 213), a = 14.5271(2) Å, V = 3065.8 Å 3 , Z = 4, R gt (F) = 0.055, wR ref (F 2 ) = 0.091, T = 295 K.
Open Access
Crystal structure of lithium ammonium hexachlorotellurate(IV), [Li_0.2(NH₄)_0.8]₂TeCl₆

February 11, 2014

R. Karray, A. Kabadou, M. Loukil, A. Ben Salah

Page range: 399-400

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Cl 6 H 6.4 Li 0.4 N 1.6 Te, cubic, Fm 3̅ m (No. 225), a = 10.357(2) Å, V = 1111.0 Å 3 , Z = 4, R gt (F) = 0.060, wR ref (F 2 ) = 0.149, T = 299 K.
Open Access
Crystal structure of dirubidium dichromate(VI), Rb₂Cr₂O₇, a fourth polymorph

February 11, 2014

U. Kolitsch

Page range: 401-402

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Cr 2 O 7 Rb 2 , triclinic, P 1̅ (No. 2), a = 7.433(1) Å, b = 7.571(2) Å, c = 7.832(2) Å, α = 109.44(3)°, β = 90.81(3)°, γ = 108.89(3)°, V = 389.6 Å 3 , Z = 2, R gt (F) = 0.028, wR ref (F 2 ) = 0.076, T = 293 K.
Open Access
Crystal structure of potassium antimony hexathiodiphosphate, KSbP₂S₆

February 11, 2014

V. Manriquez, A. Galdámez, D. Ruiz León, M. T. Garland

Page range: 403-404

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KSbP 2 S 6 , monoclinic, P 12 1 1 (No. 4), a = 6.605(1) Å, b = 7.651(2) Å, c = 9.754(2) Å, β = 92.11(3)°, V = 492.6 Å 3 , Z = 2, R gt (F) = 0.018, wR ref (F 2 ) = 0.044, T = 293 K.
Open Access
Crystal structure of Tutton’s salts, Cs₂[M^II(H₂O)₆](SeO₄)₂, M^II = Mg, Mn, Co, Ni, Zn

February 11, 2014

H. Euler, B. Barbier, A. Meents, A. Kirfel

Page range: 405-408

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Cs 2 H 12 MgO 14 Se 2 , monoclinic, P 12 1 / a 1 (No. 14), a = 9.513(1) Å, b = 13.037(1) Å, c = 6.4730(8) Å, β = 106.244(8)°, V = 770.7 Å 3 , Z = 2, R gt (F) = 0.020, wR ref (F 2 ) = 0.036, T = 293 K. Cs 2 H 12 MnO 14 Se 2 , monoclinic, P 12 1 / a 1 (No. 14), a = 9.591(1) Å, b = 13.141(2) Å, c = 6.5040(9) Å, β = 106.38(1)°, V = 786.5 Å 3 , Z = 2, R gt (F) = 0.021, wR ref (F 2 ) = 0.043, T = 293 K. CoCs 2 H 12 O 14 Se 2 , monoclinic, P 12 1 / a 1 (No. 14), a = 9.494(1)Å, b = 13.009(1) Å, c = 6.4833(8) Å, β = 106.239(9)°, V = 768.8 Å 3 , Z = 2, R gt (F) = 0.016, wR ref (F 2 ) = 0.032, T = 293 K. Cs 2 H 12 NiO 14 Se 2 , monoclinic, P 12 1 / a 1 (No. 14), a = 9.426(3)Å, b = 12.961(2) Å, c = 6.473(2) Å, β = 106.17(2)°, V = 759.5 Å 3 , Z = 2, R gt (F) = 0.017, wR ref (F 2 ) = 0.034, T = 293 K. Cs 2 H 12 O 14 Se 2 Zn, monoclinic, P 12 1 / a 1 (No. 14), a = 9.483(1) Å, b = 13.005(2) Å, c = 6.4850(8) Å, β = 106.16(1)°, V = 768.2 Å 3 , Z = 2, R gt (F) = 0.019, wR ref (F 2 ) = 0.037, T = 293 K.
Open Access
Crystal structure of Tutton’s salts, Cs₂[M^II(H₂O)₆](SO₄)₂, M^II = Mg, Mn, Fe, Co, Ni, Zn

February 11, 2014

H. Euler, B. Barbier, A. Meents, A. Kirfel

Page range: 409-413

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Cs 2 H 12 MgO 14 S 2 , monoclinic, P 12 1 / a 1 (No. 14), a = 9.338(2) Å, b = 12.849(4) Å, c = 6.361(2) Å, β = 107.07(2)°, V = 729.6 Å 3 , Z = 2, R gt (F) = 0.017, wR ref (F 2 ) = 0.041, T = 293 K. Cs 2 H 12 MnO 14 S 2 , monoclinic, P 12 1 / a 1 (No. 14), a = 9.418(3) Å, b = 12.963(2) Å, c = 6.386(3) Å, β = 107.17(4)°, V = 744.9 Å 3 , Z = 2, R gt (F) = 0.017, wR ref (F 2 ) = 0.030, T = 293 K. Cs 2 FeO 14 H 12 S 2 , monoclinic, P 12 1 / a 1 (No. 14), a = 9.357(2) Å, b = 12.886(2) Å, c = 6.381(1) Å, β = 106.94(1)°, V = 736.0 Å 3 , Z = 2, R gt (F) = 0.015, wR ref (F 2 ) = 0.030, T = 293 K. CoCs 2 H 12 O 14 S 2 , monoclinic, P 12 1 / a 1 (No. 14), a = 9.318(1) Å, b = 12.826(3) Å, c = 6.3650(9) Å, β = 107.13(1)°, V = 727.0 Å 3 , Z = 2, R gt (F) = 0.021, wR ref (F 2 ) = 0.049, T = 293 K. Cs 2 H 12 NiO 14 S 2 , monoclinic, P 12 1 / a 1 (No. 14), a = 9.259(2) Å, b = 12.767(2) Å, c = 6.358(1) Å, β = 107.00(2)°, V = 718.7 Å 3 , Z = 2, R gt (F) = 0.014, wR ref (F 2 ) = 0.027, T = 293 K. Cs 2 H 12 O 14 S 2 Zn, monoclinic, P 12 1 / a 1 (No. 14), a = 9.314(2) Å, b = 12.817(2) Å, c = 6.369(2) Å, β = 106.94(2)°, V = 727.3 Å 3 , Z = 2, R gt (F) = 0.015, wR ref (F 2 ) = 0.033, T = 293 K.
Open Access
Refinement of the crystal structure of Sb-I, at 2.22 GPa

February 11, 2014

L. G. Akselrud, M. Hanfland, U. Schwarz

Page range: 414-414

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Sb, trigonal, R 3̅ m (No. 166), a = 4.2687(2) Å, c = 10.9244(6) Å, V = 172.4 Å 3 , Z = 6, R(P) = 0.066, R(I ) = 0.059, T = 295 K, P = 2.22 GPa.
Open Access
Refinement of the crystal structure of Bi-II, at 2.54 GPa

February 11, 2014

L. G. Akselrud, M. Hanfland, U. Schwarz

Page range: 415-416

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Bi, monoclinic, C 12/ m 1 (No. 12), a = 6.67256(1) Å, b = 6.1108(2) Å, c = 3.30013(9) Å, β = 110.412(2)°, V = 126.1 Å 3 , Z = 4, R(P) = 0.118, R(I ) = 0.087, T = 295 K, P = 2.54 GPa.
Open Access
Crystal structure of lanthanum borocarbide, La₅B₄C_5–x (x = 0.15)

February 11, 2014

Hj. Mattausch, V. Babizhetskyy, A. Simon

Page range: 417-418

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B 8 C 9.71 La 10 , orthorhombic, Pna 2 1 (No. 33), a = 24.657(1) Å, b = 8.6051(5) Å, c = 8.6540(7) Å, V = 1836.2 Å 3 , Z = 4, R gt (F) = 0.039, wR ref (F 2 ) = 0.106, T = 293 K.
Open Access
Crystal structure of bisacetonitrile-tetracarbonylmolybdenum— acetonitrile solvate, Mo(CO)₄(NCCH₃)₂ · CH₃CN

February 11, 2014

Frank Biesemeier, Klaus Harms, Ulrich Müller

Page range: 419-420

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C 10 H 9 MoN 3 O 4 , monoclinic, C 12/ c 1 (No. 15), a = 12.904(2) Å, b = 12.771(2) Å, c = 9.211(1) Å, β = 116.16(2)°, V = 1362.5 Å 3 , Z = 4, R gt (F) = 0.064, wR ref (F 2 ) = 0.156, T = 193 K.
Open Access
Crystal structure of 4,4′-bipyridinum dibromide, (C₁₀H₁₀N₂)Br₂

February 11, 2014

B.-S. Zhang, Y.-Q. Zheng

Page range: 421-422

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C 10 H 10 Br 2 N 2 , triclinic, P 1̅(No. 2), a = 4.8975(6) Å, b = 7.654(1) Å, c = 7.9711(9) Å, α = 70.468(9)°, β = 87.029(9)°, γ = 77.15(1)°, V = 274.5 Å 3 , Z = 1, R gt (F) = 0.034, wR ref (F 2 ) = 0.091, T = 293 K.
Open Access
Crystal structure of 5,11,17,23-tetra-tert-butyl-25,26-bis(diphenylphosphinoylmethoxy)- 27,28-bis(benzoylmethoxy)calix[4]arene— ethyl acetate—hexane (1:1:0.5), C₈₆H₉₀O₈P₂ · C₄H₈O₂ · 0.5C₆H₁₄, a new cavity-shaped ligand with eight oxygen donors

February 11, 2014

S. Steyer, D. Matt, A. Louat

Page range: 423-426

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C 93 H 105 O 10 P 2 , triclinic, P 1̅ (No. 2), a = 10.4556(2) Å, b = 15.1838(2) Å, c = 26.8979(5) Å, α = 103.1431(9)°, β = 91.4030(7)°, γ = 95.4738(7)°, V = 4134.7 Å 3 , Z = 2, R gt (F) = 0.111, wR ref (F 2 ) = 0.285, T = 173 K.
Open Access
Crystal structure of 11,23-bis-(tert-butyl)-25,27-bis-(ethoxyethoxy)-26,28-bis-(propoxy)calix[4]arene, C₅₀H₆₈O₆

February 11, 2014

I. A. Bagatin, F. Balegroune, D. Matt

Page range: 427-428

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C 50 H 68 O 6 , monoclinic, C 12/ c 1 (No. 15), a = 25.4702(8) Å, b = 11.013(1) Å, c = 18.5662(8) Å, β = 119.078(3)°, V = 4551.6 Å 3 , Z = 4, R gt (F) = 0.063, wR ref (F 2 ) = 0.230, T = 293 K.
Open Access
Crystal structure of 5,11,17,23-tetra-t-butyl-25,27-dihydroxy-26,28-di-tosyloxy-calix[4]arene, C₅₈H₆₈O₈S₂

February 11, 2014

E. F. Paulus, W. Joswig, V. Böhmer, M. Saadioui, M. Krilow, M. Peikert-Regelien, B. Urschel

Page range: 429-431

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C 58 H 68 O 8 S 2 , monoclinic, C 1 c 1 (No. 9), a = 23.888(5) Å, b = 11.225(2) Å, c = 21.431(4) Å, β = 112.41(3)°, V = 5312.7 Å 3 , Z = 4, R gt (F) = 0.041, wR ref (F 2 ) = 0.105, T = 293 K.
Open Access
Crystal structure of bis(2,6-diaminopyridinium) diaqua-bis-(2,6-pyridinedicarboxylato)-bis(2,6-pyridinedicarboxylato)- dibismuthate(III) tetrahydrate, (C₂₈H₁₆O₁₈N₄Bi₂)(C₅H₈N₃)₂ · 4H₂O

February 11, 2014

M. Ranjbar, H. Aghabozorg, A. Moghimi

Page range: 432-434

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C 38 H 40 Bi 2 N 10 O 22 , triclinic, P 1̅̅ (No. 2), a = 9.699(1) Å, b = 10.500(1) Å, c = 10.890(1) Å, α = 85.587(3)°, β = 88.128(3)°, γ = 84.257(3)°, V = 1099.9 Å 3 , Z = 1, R gt (F) = 0.028, wR ref (F 2 ) = 0.061, T = 295 K.
Open Access
Crystal structure of 2,2′-bis(4,5-dimethylimidazole)(dithiocyanato)mercury(II), Hg(C₁₀H₁₄N₄)(CNS)₂

February 11, 2014

A. R. Mahjoub, A. Ramazani, A. Morsali

Page range: 435-436

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C 12 H 14 HgN 6 S 2 , triclinic, P 1̅̅̅ (No. 2), a = 7.732(2) Å, b = 10.252(2) Å, c = 11.802(2) Å, α = 65.57(3)°, β = 72.19(3)°, γ = 88.13(3)°, V = 806.2 Å 3 , Z = 2, R gt (F) = 0.048, wR * (F 2 ) = 0.123, T = 293 K.
Open Access
Crystal structure of {2-[4-(4-chlorophenyl)-4-hydroxy-1-piperidinylmethyl] cyclopentyl}-(4-fluorophenyl)-methanone, C₂₄H₂₇ClFNO₂

February 11, 2014

U. Casellato, R. Graziani, M. Teijeira, E. Uriarte

Page range: 437-438

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C 24 H 27 ClFNO 2 , triclinic, P 1̅̅̅̅ (No. 2), a = 9.494(2) Å, b = 10.769(2) Å, c = 11.377(3)Å, α = 87.18(3)°, β = 67.27(3)°, γ = 88.01(3)°, V = 1071.4 Å 3 , Z = 2, R gt (F) = 0.076, wR obs (F 2 ) = 0.302, T = 293 K.
Open Access
Refinement of the crystal structure of the δ-modification of tris(8-hydroxyquinoline) aluminum(III), δ-Al(C₉H₆NO)₃, the blue luminescent Alq₃

February 11, 2014

M. Rajeswaran, T. N. Blanton, K. P. Klubek

Page range: 439-440

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C 27 H 18 AlN 3 O 3 , triclinic, P 1̅̅̅̅̅ (No. 2), a = 6.181(1) Å, b = 13.268(3) Å, c = 14.430(3) Å, α = 66.06(3)°, β = 88.56(3)°, γ = 84.03(3)°, V = 1075.5 Å 3 , Z = 2, R gt (F) = 0.108, wR ref (F 2 ) = 0.437, T = 293 K.
Open Access
Crystal structure of N-(4-(3,6-dioxo-4-phenylsulfanylcyclo-1,4-dienylamino))-5-dimethylaminonaphtalene-sulfonamide, C₃₀H₂₅N₃O₄S₂

February 11, 2014

J. M. Rubin-Preminger, R. A. Illos, S. Bittner

Page range: 441-442

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C 30 H 25 N 3 O 4 S 2 , monoclinic, P 12 1 / c 1 (No. 14), a = 7.031(2) Å, b = 33.12(1) Å, c = 13.149(4) Å, β = 119.63(1)°, V = 2661.9 Å 3 , Z = 4, R gt (F) = 0.058, wR ref (F 2 ) = 0.174, T = 293 K.
Open Access
Crystal structure of catena-poly{[tetra[μ-(benzoato-O,O′)]dicopper(II)]-μ-2-N,N′-(4,4″-bi-3,5-dimethylpyrazolate)} hydrate, [Cu₂(O₂CC₆H₅)₄(C₁₀N₄H₁₄)] · H₂O

February 11, 2014

H. Huang, Q.-H. Jin, S.-Y. Yu, H.-W. Ma, S.-H. Li, H.-P. Huang, K.-B. Yu

Page range: 443-444

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C 38 H 36 Cu 2 N 4 O 9 , monoclinic, C 12/ c 1 (No. 15), a = 18.336(4) Å, b = 19.494(4) Å, c = 11.389(2) Å, β = 113.76(1)°, V = 3725.9 Å 3 , Z = 4, R gt (F) = 0.029, wR ref (F 2 ) = 0.073, T = 296 K.
Open Access
Crystal structure of di(2,2′-bipyridine)tetra(μ-3-methoxylbenzoato-O,O′)-di(3-methoxybenzoato)diterbium(III), Tb₂(C₈H₇O₃)₆(C₁₀H₈N₂)₂

February 11, 2014

X. Li, Y.-Q. Zou

Page range: 445-447

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C 68 H 58 N 4 O 18 Tb 2 , monoclinic, P 12 1 / c 1 (No. 14), a = 10.582(4) Å, b = 16.149(5) Å, c = 18.821(6) Å, β = 100.554(6)°, V = 3161.9 Å 3 , Z = 2, R gt (F) = 0.058, wR ref (F 2 ) = 0.178, T = 293 K.
Open Access
Crystal structure of di(2,2′-bipyridine)tetra[μ-(4-methylbenzoato-O,O′)]- di(4-methylbenzoato)disamarium(III), Sm₂(C₈H₇O₂)₆(C₁₀H₈N₂)₂

February 11, 2014

X. Li, Y.-Q. Zou

Page range: 448-450

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C 68 H 58 N 4 O 12 Sm 2 , monoclinic, C 12/ c 1 (No. 15), a = 14.123(7) Å, b = 19.151(9) Å, c = 23.12(1) Å, β = 96.600(8)°, V = 6211.0 Å 3 , Z = 4, R gt (F) = 0.029, wR ref (F 2 ) = 0.053, T = 293 K.
Open Access
Crystal structure of di(2,2′-bipyridine)di[μ-(2,3-dimethoxylbenzoato- O,O′)]di[μ-(2,3-dimethoxylbenzoato-O,O′:O′)]di(nitrato)diterbium(III), Tb₂(NO₃)₂(C₉H₉O₄)₄(C₁₀H₈N₂)₂

February 11, 2014

X. Li, Y.-Q. Zou

Page range: 451-452

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C 28 H 26 N 3 O 11 Tb, triclinic, P 1̅ (No. 2), a = 10.620(7) Å, b = 10.766(7) Å, c = 13.182(8) Å, α = 76.11(1)°, β = 79.51(1)°, β = 74.39(1)°, V = 1398.0 Å 3 , Z = 2, R gt (F) = 0.062, wR ref (F 2 ) = 0.151, T = 293 K.
Open Access
Crystal structure of di(1,10-phenanthroline-N,N′)di[μ-(2-furancarboxylato- O,O′)-μ-(2-furancarboxylato-O,O′:O′)]di(nitrato)diterbium(III), Tb₂(NO₃)₂(C₅H₃O₃)₄(C₁₂H₈N₂)₂

February 11, 2014

X. Li, Y.-Q. Zou

Page range: 453-454

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C 22 H 14 N 3 O 9 Tb, triclinic, P 1̅ (No. 2), a = 10.383(3) Å, b = 10.512(3) Å, c = 11.001(3) Å, α = 81.201(6)°, β = 88.491(6)°, γ = 67.595(5)°, V = 1096.3 Å 3 , Z = 2, R gt (F) = 0.039, wR ref (F 2 ) = 0.067, T = 293 K.
Open Access
Crystal structure of di[potassium(diaza-18-crown-6)]dicaesium nonastannide( 4–) diethylenediamine, [K(C₁₂H₂₆N₂O₄)]2Cs₂[Sn₉] · 2C₂N₂H₈, a polyanion ²_∞[KCs₂Sn₉]^– with low-dimensional arrangement of [Sn₉] clusters

February 11, 2014

R. Hauptmann, T. F. Fässler

Page range: 455-457

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C 28 H 68 Cs 2 K 2 N 8 O 8 Sn 9 , monoclinic, P 12 1 / c 1 (No. 14), a = 13.897(3) Å, b = 16.091(3) Å, c = 26.432(5) Å, β = 91.03(3)°, V = 5909.7 Å 3 , Z = 4, R gt (F) = 0.050, wR ref (F 2 ) = 0.127, T = 153 K.
Open Access
Crystal structure of di[potassium(18-crown-6)]dipotassium nonastannide(4–)—diethylenediamine solvate (1:1.5), [K(C₁₂H₂₄O₆)]₂K₂[Sn₉] · 1.5C₂N₂H₈

February 11, 2014

R. Hauptmann, T. F. Fässler

Page range: 458-460

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C 27 H 60 K 4 N 3 O 12 Sn 9 , monoclinic, P 12 1 / n 1(No. 14), a = 10.410(2) Å, b = 25.659(5) Å, c = 20.636(4) Å, β = 102.56(3)°, V = 5380.2 Å 3 , Z = 4, R gt (F) = 0.030, wR ref (F 2 ) = 0.072, T = 150 K.
Open Access
Crystal structure of di[potassium([2.2.2]crypt)]tetrapotassium octadecagermanide(6–)—ethylenediamine solvate (1:6), [K(C₁₈H₃₆N₂O₆)]₂K₄(Ge₉)₂ · 6C²N₂H₈

February 11, 2014

R. Hauptmann, T. F. Fässler

Page range: 461-463

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C 24 H 60 Ge 9 K 3 N 8 O 6 , triclinic, P 1̅ (No. 2), a = 9.408(2) Å, b = 13.606(3) Å, c = 19.507(4) Å, α = 84.74(3)°, β = 81.35(3)°, γ = 80.18(3)°, V = 2426.8 Å 3 , Z = 2, R gt (F) = 0.064, wR ref (F 2 ) = 0.192, T = 150 K.
Open Access
Crystal structure of bis[2-(benzylamino)-6-methylpyridinato]- bis(hexahydro-2-azepinato)zirconium(IV), C₃₈H₄₆N₆O₂Zr

February 11, 2014

R. Kempe, G. Hillebrand

Page range: 464-466

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C 38 H 46 N 6 O 2 Zr, monoclinic, P 12 1 / c 1 (No. 14), a = 13.575(3) Å, b = 15.903(3) Å, c = 17.404(3) Å, β = 106.85(3)°, V = 3596.0 Å 3 , Z = 4, R gt (F) = 0.046, wR ref (F 2 ) = 0.126, T = 293 K.
Open Access
Crystal structure of dimethylamido-hexahydro-2-azepinato-bis[2-(trimethylsilylamino)-4-methylpyridinato]-titanium(IV), C₂₆H₄₆N₆OSi₂Ti

February 11, 2014

R. Kempe, G. Hillebrand

Page range: 467-468

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C 26 H 46 N 6 OSi 2 Ti, triclinic, P 1̅ (No. 2), a = 10.178(2) Å, b = 10.906(2) Å, c = 16.254(3) Å, α = 91.82(1)°, β = 102.60(2)°, γ = 112.81(2)°, V = 1609.5 Å 3 , Z = 2, R gt (F) = 0.046, wR obs (F 2 ) = 0.116, T = 293 K.
Open Access
Crystal structure of 1′-(1,2′-binaphthyl) 1-naphthyl ketone, C₃₁H₂₀O

February 11, 2014

K. Skobridis, E. Weber, W. chter

Page range: 469-470

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C31H20O, monoclinic, P 121/ n 1 (No. 14), a = 11.588(2) Å, b = 12.306(2) Å, c = 15.794(3) Å, β = 105.65(3)°, V = 2168.8 Å3, Z = 4, R gt (F) = 0.071, wR ref (F 2 ) = 0.203, T = 298 K.
Open Access
Crystal structure of (1R*,2S*,5S*,6S*,7R*)-6-(3,5-dinitrobenzoyloxy)methyl-2,7-dimethyl-tricyclo [5.2.2.0^1,5]undec-8-ene, C₂₁H₂₄N₂O₆

February 11, 2014

H. Euler, A. Kirfel, C. Valder, M. Neugebauer, M. Meier, N. A. Braun

Page range: 471-472

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C 21 H 24 N 2 O 6 , orthorhombic, P 2 1 2 1 2 1 (No. 19), a = 6.285(2) Å, b = 9.044(4) Å, c = 35.52(2) Å, V = 2019.0 Å 3 , Z = 4, R(F) = 0.095, wR ref (F 2 ) = 0.279, T = 295 K.
Open Access
Crystal structure of 9-benzyl-6-ethoxy-7-ethyl-2-phenyl-7,9- dihydropurin-8-one, C₂₂H₂₂N₄O₂

February 11, 2014

H. Euler, A. Kirfel, A. Bauer, C. E. Müller

Page range: 473-474

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C 22 H 22 N 4 O 2 , monoclinic, C 12/ c 1 (No. 15), a = 22.44(1) Å, b = 7.878(2) Å, c = 23.295(6) Å, β = 97.75(3)°, V = 4080.9 Å 3 , Z = 8, R gt (F) = 0.045, wR ref (F 2 ) = 0.131, T = 295 K.
Open Access
Crystal structure of (S)-3-(Z-1′,3′-butadienyl)-4-phenylthiazoline-2-one, C₁₃H₁₃NOS, a chiral 1-amino-diene useful in Diels-Alder cycloaddition reactions

February 11, 2014

B. Tinant, R. Robiette, J. Marchand-Brynaert

Page range: 475-476

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C 13 H 13 NOS, monoclinic, P 12 1 1 (No. 4), a = 6.144(2) Å, b = 12.398(5) Å, c = 8.160(3) Å, β = 97.00(2)°, V = 616.9 Å 3 , Z = 2, R gt (F) = 0.044, wR ref (F 2 ) = 0.103, T = 293 K.
Open Access
Crystal structure of ammonium oxo(peroxo)(pyridine-2,6-dicarboxylato- N,O,O′)aquavanadate(V), (NH₄)[VO(O₂)(H₂O)(C₇H₃NO₄)]

February 11, 2014

B. Tinant, D. Bayot, M. Devillers

Page range: 477-478

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C 7 H 9 N 2 O 8 V, orthorhombic, Pcca (No. 54), a = 13.575(4) Å, b = 20.603(6) Å, c = 8.026(3) Å, V = 2244.8 Å 3 , Z = 8, R gt (F) = 0.046, wR ref (F 2 ) = 0.155, T = 293 K.
Open Access
Crystal structure of cis-bis(N,N-dimethyl-N′-4-chlorobenzoylthioureato) palladium(II), Pd(C₁₀H₁₀ClN₂OS)₂

February 11, 2014

H. Arslan, D. Vanderveer, F. Emen, N. Külcü

Page range: 479-480

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C 20 H 20 Cl 2 N 4 O 2 PdS 2 , monoclinic, P 12 1 / c 1 (No. 14), a = 12.323(4) Å, b = 8.629(3) Å, c = 21.212(7) Å, β = 97.170(6)°, V = 2238.0 Å 3 , Z = 4, R gt (F) = 0.045, wR ref (F 2 ) = 0.133, T = 193 K.
Open Access
Crystal structure of 4-aminopyrimidine, C₄H₅N₃

February 11, 2014

L. Van Meervelt, K. Uytterhoeven

Page range: 481-482

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C 4 H 5 N 3 , orthorhombic, Pcab (No. 61), a = 10.983(2) Å, b = 12.287(3) Å, c = 14.052(3) Å, V = 1896.3 Å 3 , Z = 16, R gt (F) = 0.054, wR ref (F 2 ) = 0.146, T = 289 K.
Open Access
Crystal structure of 2-acetonyl-5-benzyl-4,6-dimethoxy-5-nitro-2,5-dihydropyrimidine, C₁₆H₁₉N₃O₅

February 11, 2014

L. Van Meervelt, K. Uytterhoeven

Page range: 483-484

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C 16 H 19 N 3 O 5 , monoclinic, P 12 1 / c 1 (No. 14), a = 12.010(1) Å, b = 11.877(1) Å, c = 12.110(1) Å, β = 95.83(2)°, V = 1718.5 Å 3 , Z = 4, R gt (F) = 0.044, wR ref (F 2 ) = 0.129, T = 289 K.
Open Access
Crystal structure of N-(3,5-benzenedicarboxy)-2,5-phenyl-3,4-(9,10-dihydroanthracen-diyl)-pyrrole—acetone—water (1:1:1), C₃₈H₂₅NO₄ · C₃H₆O · H₂O

February 11, 2014

K. Uytterhoeven, L. Van Meervelt, M. Smet, W. Dehaen

Page range: 485-487

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C 41 H 33 NO 6 , triclinic, P 1̅ (No. 2), a = 9.610(3) Å, b = 12.877(3) Å, c = 15.138(4) Å, α = 109.29(2)°, β = 105.16(2)°, γ = 94.24(2)°, V = 1680.0 Å 3 , Z = 2, R gt (F) = 0.059, wR ref (F 2 ) = 0.161, T = 289 K.
Open Access
Crystal structure of tris(N-(n-butyl)-4-methoxy-2-hydroxybenzaldimine)-tris(nitrato)lanthanum(III), La(C₁₂H₁₇NO₂)₃(NO₃)₃

February 11, 2014

L. Van Meervelt, K. Uytterhoeven, R. Van Deun, K. Binnemans

Page range: 488-490

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C 36 H 51 LaN 6 O 15 , triclinic, P 1̅̅ (No. 2), a = 11.455(2) Å, b = 13.859(3) Å, c = 14.101(4) Å, α = 98.50(2)°, β = 98.87(1)°, γ = 92.52(2)°, V = 2182.4 Å 3 , Z = 2, R gt (F) = 0.035, wR ref (F 2 ) = 0.082, T = 289 K.
Open Access
Crystal structure of di(μ-3,5-dinitrobenzoato-O,O′)di(μ-3,5-dinitrobenzoato-O,O:O′)di(3,5-dinitrobenzoato-O,O′)di(1,10-phenanthroline- N,N′)-diterbium(III), Tb₂(C₁₂H₈N₂)₂(C₇H₃N₂O₆)₆

February 11, 2014

M.-L. Hu, H.-P. Xiao, S. Wang, X.-H. Li

Page range: 491-493

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C 66 H 34 N 16 O 36 Tb 2 , triclinic, P 1̅̅ (No. 2), a = 12.027(7) Å, b = 12.908(7) Å, c = 13.210(7) Å, α = 104.086(7)°, β = 113.774(7)°, γ = 100.425(7)°, V = 1728.1 Å 3 , Z = 1, R gt (F) = 0.025, wR ref (F 2 ) = 0.042, T = 298 K.
Open Access
Crystal structure of tris(1,10-phenanthroline-N,N′)nickel(III) 1,2,4,5-benzene-tetracarboxylate, C₅₁H₃₀N₆NiO₁₂

February 11, 2014

X.-H. Li, M.-L. Hu

Page range: 494-496

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C 51 H 30 N 6 NiO 12 , triclinic, P 1̅̅ (No. 2), a = 12.402(7) Å, b = 12.908(8) Å, c = 14.471(9) Å, α = 96.44(1)°, β = 106.45(1)°, γ = 105.12(1)°, V = 2101.1 Å 3 , Z = 2, R gt (F) = 0.079, wR ref (F 2 ) = 0.170, T = 298 K.
Open Access
Crystal structure of 1-[(4-chloro-phenyl)-phenyl-methyl]piperazine, C₁₇H₁₉ClN₂

February 11, 2014

X.-R. Hu, J.-M. Gu, G.-L. Lu

Page range: 497-498

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C 17 H 19 ClN 2 , orthorhombic, P 2 1 2 1 2 1 (No. 19), a = 18.0920(1) Å, b = 5.8896(1) Å, c = 14.6011(2) Å, V = 1555.8 Å 3 , Z = 4, R gt (F) = 0.048, wR ref (F 2 ) = 0.114, T = 298 K.
Open Access
Crystal structure of diethylenetriaminesilver(I) perchlorate, Ag(C₄H₁₃N₃)(ClO₄)

February 11, 2014

H.-L. Zhu, S.-C. Shao, J.-L. Ma, X.-Y. Qiu, S. Yang, L. Sun

Page range: 499-500

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C 4 H 13 AgClN 3 O 4 , orthorhombic, Pccn (No. 56), a = 17.730(7) Å, b = 7.162(3) Å, c = 15.891(7) Å, V = 2017.9 Å 3 , Z = 8, R gt (F) = 0.047, wR ref (F 2 ) = 0.152, T = 298 K.
Open Access
Crystal structure of hexaaquanickel(II) dinitrate hexamethylenetetramine hydrate (1:2:4), Ni(H₂O)₆(NO₃)₂ · (C₆H₁₂N₄)₂ · ₄H₂O

February 11, 2014

J.-L. Ma, X.-Y. Qiu, S.-C. Shao, S. Yang, L. Sun, H.-L. Zhu

Page range: 501-502

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C 12 H 44 N 10 NiO 16 , triclinic, P 1̅̅̅ (No. 2), a = 9.06(1) Å, b = 9.32(1) Å, c = 9.67(1) Å, α = 87.64(2)°, β = 75.59(2)°, γ = 61.11(1)°, V = 689.7 Å 3 , Z = 1, R gt (F) = 0.056, wR ref (F 2 ) = 0.147, T = 298 K.
Open Access
Crystal structure of monoaquabenzoato-2,5,8-triaza-1,9-di(2-fluorobenzyl)-nonanecopper(II) benzoate dihydrate, Cu(C₂₅H₃₀F₂N₃O₃)(C₇H₅O₂) · 2H₂O

February 11, 2014

H.-L. Zhu, S.-C. Shao, J.-L. Ma, X.-Y. Qiu, S. Yang, L. Sun

Page range: 503-505

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C 32 H 39 CuF 2 N 3 O 7 , triclinic, P 1̅̅̅ (No. 2), a = 7.331(3) Å, b = 8.983(3) Å, c = 26.34(1) Å, α = 95.570(6)°, β = 95.797(6)°, γ = 110.811(5)°, V = 1596.3 Å 3 , Z = 2, R gt (F) = 0.040, wR ref (F 2 ) = 0.103, T = 298 K.
Open Access
Crystal structure of bis[dinitrato-2,5,8-triaza-1,9-di(2-fluorobenzylnonanecopper( II)] monohydrate, Cu(C₁₈H₂₂F₂N₅O₆)₂ · H₂O

February 11, 2014

H.-L. Zhu, S.-C. Shao, J.-L. Ma, X.-Y. Qiu, S. Yang, L. Sun

Page range: 506-508

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C 36 H 48 Cu 2 F 4 N 10 O 13 , monoclinic, C 1 c 1 (No. 9), a = 14.870(8) Å, b = 20.78(1) Å, c = 14.660(7) Å, β = 101.308(9)°, V = 4441.6 Å 3 , Z = 4, R gt (F) = 0.053, wR ref (F 2 ) = 0.147, T = 298 K.
Open Access
Crystal structure of di(2-aminopyridine)-tetrakis[N-(2-aminopropyl)-salicylaldiminato)]tricobalt(III) diperchlorate, Co₃(C₅₈H₄₈N₁₂O₄)(ClO₄)₂

February 11, 2014

H.-L. Zhu, S. Yang, S.-C. Shao, J.-L. Ma, X.-Y. Qiu, L. Sun

Page range: 509-510

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C 58 H 48 Cl 2 Co 3 N 12 O 12 , triclinic, P 1̅̅̅̅ (No. 2), a = 11.640(3) Å, b = 11.693(3) Å, c = 12.218(3) Å, α = 78.968(5)°, β = 89.827(5)°, γ = 60.605(4)°, V = 1414.0 Å 3 , Z = 1, R gt (F) = 0.062, wR ref (F 2 ) = 0.136, T = 293 K.
Open Access
Crystal structure of diethylenetriammonium silver(I) di(4-nitrobenzoate) monohydrate, [Ag(C₄H₁₄N₃)](C₇H₄NO₄)₂ · H₂O

February 11, 2014

H.-L. Zhu, S.-C. Shao, S. Yang, X.-Y. Qiu, J.-L. Ma, H.-K. Fun

Page range: 511-512

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C 18 H 24 AgN 5 O 9 , monoclinic, P 12 1 / n 1 (No. 14), a = 6.2181(3) Å, b = 26.975(2) Å, c = 13.1982(7) Å, β = 99.648(2)°, V = 2182.5 Å 3 , Z = 4, R gt (F) = 0.038, wR ref (F 2 ) = 0.082, T = 293 K.
Open Access
Crystal structure of diaqua-trans-dicinnamato-dihexamethylenetetraminecobalt(II) dihydrate, Co(C₆H₁₂N₄)₂(C₉H₇O₂)₂(H₂O)₂ · 2H₂O

February 11, 2014

H.-L. Zhu, S.-C. Shao, X.-Y. Qiu, L. Sun, S. Yang, J.-L. Ma

Page range: 513-514

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C 30 H 46 CoN 8 O 8 , monoclinic, P 12 1 / c 1 (No. 14), a = 12.779(3) Å, b = 10.938(2) Å, c = 12.218(2) Å, β = 97.56(3)°, V = 1693.0 Å 3 , Z = 2, R gt (F) = 0.085, wR ref (F 2 ) = 0.201, T = 293 K.
Open Access
Crystal structure of bis(3,3′-diethyl-4-maleimidophenyl)methane, C₂₅H₂₂N₂O₄

February 11, 2014

H.-L. Zhu, H. Zhang, J.-L. Ma, X.-Y. Qiu, S. Yang, L. Sun

Page range: 515-516

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C 25 H 22 N 2 O 4 , orthorhombic, Pccn (No. 56), a = 12.745(2) Å, b = 16.974(2) Å, c = 10.218(1) Å, V = 2210.4 Å 3 , Z = 4, R gt (F) = 0.114, wR ref (F 2 ) = 0.300, T = 293 K.
Open Access
Crystal structure of diaqua-dibenzoato-dihexamethylenetetraminenickel(II) dihydrate, Ni(C₆H₁₂N₄)₂(C₇H₅O₂)₂(H₂O)₂ · 2H₂O

February 11, 2014

H.-L. Zhu, L. Sun, S. Yang, X.-Y. Qiu, S.-C. Shao, J.-L. Ma

Page range: 517-518

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C 26 H 42 N 8 NiO 8 , monoclinic, C 12/ c 1 (No. 15), a = 22.784(5) Å, b = 10.886(2) Å, c = 12.208(2) Å, β = 95.50(3)°, V = 3014.0 Å 3 , Z = 4, R gt (F) = 0.074, wR ref (F 2 ) = 0.156, T = 293 K.
Open Access
Crystal structure of trans-diaqua-bis(salicylaldehydato-O,O′) chromium(III) chloride, [Cr(C₇H₅O₂)₂(H₂O)₂]Cl

February 11, 2014

H.-L. Zhu, Y. Qu, Z.-L. You, M.-Y. Tan, W.-S. Liu, J.-L. Ma

Page range: 519-520

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C 14 H 14 ClCrO 6 , monoclinic, P 12 1 / c 1 (No. 14), a = 8.998(18) Å, b = 18.68(4) Å, c = 4.945(10) Å, β = 105.95(2)°, V = 799.2 Å 3 , Z = 2, R gt (F) = 0.069, wR ref (F 2 ) = 0.170, T = 298 K.
Open Access
Crystal structure of di(4-aminopyridine)silver(I) trifluoromethylsulfate, Ag(C₅H₆N₂)₂(CF₃SO₃)

February 11, 2014

H.-L. Zhu, M. Zhang, Z.-Y. Sun, N.-N. Rong, B. Zhang, Y. Li, H.-K. Fun

Page range: 521-522

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C 11 H 12 AgF 3 N 4 O 3 S, monoclinic, P 12 1 / n 1 (No. 14), a = 6.901(1) Å, b = 11.106(2) Å, c = 20.958(4) Å, β = 94.799(3)°, V = 1600.6 Å 3 , Z = 4, R gt (F) = 0.033, wR ref (F 2 ) = 0.081, T = 293 K.
Open Access
Crystal structure of triaquasulfato-2,3-diaza-1,6-di(4-fluorobenzyl)-hexanecopper(II) dihydrate, Cu(C₁₆H₁₈N₂F₂)(H₂O)₃(SO₄) · 2H₂O

February 11, 2014

H.-L. Zhu, X.-Y. Qiu, S. Yang, J.-L. Ma

Page range: 523-524

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C 16 H 28 CuF 2 N 2 O 9 S, monoclinic, P 12 1 / c 1 (No. 14), a = 15.169(8) Å, b = 12.614(6) Å, c = 11.387(6) Å, β = 94.651(7)°, V = 2171.6 Å 3 , Z = 4, R gt (F) = 0.046, wR ref (F 2 ) = 0.138, T = 298 K.
Open Access
Crystal structure of dimethylglyoxime 2-picoloylhydrazone, C₁₀H₁₂N₄O₂

February 11, 2014

H. Lin, W.-S. Wu

Page range: 525-526

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C 10 H 12 N 4 O 2 , monoclinic, P 12 1 / c 1 (No. 14), a = 5.7138(3) Å, b = 25.771(1) Å, c = 7.3379(4) Å, β = 100.385(2)°, V = 1062.8 Å 3 , Z = 4, R gt (F) = 0.051, wR ref (F 2 ) = 0.170, T = 293 K.
Open Access
Crystal structure of (2-picoloylcarbonyl)thiosemicarbazone, C₇H₁₀N₄O₂S

February 11, 2014

W.-S. Wu, Y.-L. Feng

Page range: 527-528

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C 7 H 10 N 4 O 2 S, orthorhombic, Pbca (No. 61), a = 12.1705(9) Å, b = 7.421(2) Å, c = 22.7584(5) Å, V = 2055.3 Å 3 , Z = 8, R gt (F) = 0.033, wR ref (F 2 ) = 0.075, T = 293 K.
Open Access
Crystal structure of [bis(2-hydroxybenzylidenethiosemicarbazone)-iron(II)] hydrate, Fe(C₁₆H₁₆N₆O₂S₂) · H₂O

February 11, 2014

W.-S. Wu, Y.-L. Feng

Page range: 529-530

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C 16 H 18 FeN 6 O 3 S 2 , monoclinic, P 12 1 / n 1 (No. 14), a = 8.9754(5) Å, b = 18.229(1) Å, c = 11.5546(7) Å, β = 93.006(2)°, V = 1887.9 Å 3 , Z = 4, R gt (F) = 0.039, wR ref (F 2 ) = 0.080, T = 293 K.
Open Access
Crystal structure of tris(nitrato-O,O′)bis(1,10-phenanthroline-N,N′)- cerium(III), Ce(NO₃)₃(C₁₂H₈N₂)₂

February 11, 2014

Q.-Y. Lin, Y.-L. Feng

Page range: 531-532

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C 24 H 16 CeN 7 O 9 , monoclinic, C 12/ c 1 (No. 15), a = 11.162(2) Å, b = 18.070(4) Å, c = 13.102(3) Å, β = 100.56(3)°, V = 2597.9 Å 3 , Z = 4, R gt (F) = 0.021, wR ref (F 2 ) = 0.056, T = 293 K.
Open Access
Crystal structure of (aqua)(benzimidazole-N)bis(2,4-pentanedionato-O,O′)cobalt(II), C₁₇H₂₂CoN₂O₅

February 11, 2014

H. Lin, Y.-L. Feng

Page range: 533-534

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C 17 H 22 CoN 2 O 5 , orthorhombic, Pnma (No. 62), a = 7.944(2) Å, b = 14.346(3) Å, c = 16.544(3) Å, V = 1885.5 Å 3 , Z = 4, R gt (F) = 0.044, wR ref (F 2 ) = 0.123, T = 293 K.
Open Access
Crystal structure of 2-dimethoxy-phosphinyl-1,3-benzodithiole, (C₆H₄S₂CH)PO(OCH₃)₂

February 11, 2014

F.-Y. Xu, F.-S. Zhang, R.-J. Wang, S.-Z. Pu, X.-H. Zhou, F. Sun, P. Yuan

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C 9 H 11 O 3 PS 2 , monoclinic, P 12 1 / n 1 (No. 14), a = 9.791(3) Å, b = 10.943(2) Å, c = 11.619(3) Å, β = 108.970(2)°, V = 1177.3 Å 3 , Z = 4, R gt (F) = 0.035, wR ref (F 2 ) = 0.078, T = 293 K.
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Crystal structure of dichloro(3-methylthio-2-methylpropyl)diphenylphosphine-palladium(II)—dichloromethane (1:1), Pd(C₁₇H₂₁PS)Cl₂ · CH₂Cl₂

February 11, 2014

E. M. Al-Shami, A. S. Abu-Surrah, M. Klinga, M. Ahlgren, H. A Hodali

Page range: 537-538

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C 18 H 23 Cl 4 PPdS, monoclinic, P 12 1 / n 1 (No. 14), a = 11.8279(1) Å, b = 14.6142(2) Å, c = 12.4063(1) Å, β = 93.876(1)°, V = 2139.6 Å 3 , Z = 4, R gt (F) = 0.021, wR ref (F 2 ) = 0.049, T = 120 K.
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Crystal structure of 1,3,5-trimethyl-6-phenyl-2,4-dioxohexahydro-1,3,5-triazine, C₁₂H₁₅N₃O₂

February 11, 2014

K. O. Klepp, H. Schmidt

Page range: 539-540

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C 12 H 15 N 3 O 2 , monoclinic, P 12 1 / n 1 (No. 14), a = 8.902(6) Å, b = 12.674(2) Å, c = 10.647(4) Å, β = 98.84(2)°, V = 1187.0 Å 3 , Z = 4, R gt (F) = 0.048, wR obs (F) = 0.048, T = 294 K.
Open Access
Crystal structure of diaqua-bis(pyridine)-μ2-squarato(1,3)-nickel(II), Ni(C₄O₄)(C₅H₅N)₂(H₂O)₂

February 11, 2014

R. Kirchmaier, E. Altin, A. Lentz

Page range: 541-542

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C 14 H 14 N 2 NiO 6 , orthorhombic, Pbca (No. 61), a = 7.914(1) Å, b = 12.020(2) Å, c = 15.718(3) Å, V = 1495.3 Å 3 , Z = 4, R gt (F) = 0.026, wR ref (F 2 ) = 0.062, T = 293 K.
Open Access
Crystal structure of 4,5-methylenedithio-1,3-dithiol-2-thione, C₄H₂S₅

February 11, 2014

Z. Liu, W.-T. Yu, X.-T. Tao, M.-H. Jiang

Page range: 543-544

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C 4 H 2 S 5 , orthorhombic, Pnma (No. 62), a = 13.015(1) Å, b = 9.193(1) Å, c = 6.151(1) Å, V = 735.9 Å 3 , Z = 4, R gt (F) = 0.040, wR ref (F 2 ) = 0.118, T = 293 K.
Open Access
Crystal structure of 4,5-bis(2′-cyanoethylthio)-1,3-dithiole-2-thione, C₉H₈N₂S₅

February 11, 2014

W.-T. Yu, G. Xue, Q. Fang, G.-Q. Liu

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C 9 H 8 N 2 S 5 , monoclinic, P 12 1 / n 1 (No. 14), a = 9.070(5) Å, b = 27.123(5) Å, c = 10.736(5) Å, β = 104.461(5)°, V = 2557.5 Å 3 , Z = 8, R gt (F) = 0.038, wR ref (F 2 ) = 0.086, T = 293 K.
Open Access
Crystal structure of nonafluoro-{N-[(E)-2-(4-hydroxyphenyl)diazenyl]-phenyl}-1-butanesulfonamide, C₁₆H₁₀F₉N₃O₃S

February 11, 2014

X. Àlvarez Micó, M. Richter, S. Schwarz, J. Strähle, T. Ziegler, L. R. Subramanian

Page range: 547-548

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C 16 H 10 F 9 N 3 O 3 S, triclinic, P 1̅ (No. 2), a = 5.4635(2) Å, b = 10.266(1) Å, c = 17.645(2) Å, α = 105.731(6)°, β = 93.187(5)°, γ = 97.036(7)°, V = 941.3 Å 3 , Z = 2, R gt (F) = 0.048, wR ref (F 2 ) = 0.134, T = 213 K.
Open Access
Crystal structure of nonafluoro-{N-[(E)-2-(2-hydroxyphenyl)diazenyl]-phenyl}-1-butanesulfonamide, C₁₆H₁₀F₉N₃O₃S

February 11, 2014

X. Àlvarez Micó, M. Richter, S. Schwarz, J. Strähle, T. Ziegler, L. R. Subramanian

Page range: 549-550

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C 16 H 10 F 9 N 3 O 3 S, monoclinic, P 12 1 / c 1 (No. 14), a = 5.6549(3) Å, b = 12.2550(9) Å, c = 27.170(6) Å, β = 90.446(8)°, V = 1882.8 Å 3 , Z = 4, R gt (F) = 0.088, wR ref (F 2 ) = 0.261, T = 213 K.
Open Access
Crystal structure of 7-(p-toluenesulfonyl)-7-aza-1,4-dithiacyclononane (Ts[9]aneNS₂), C₁₃H₁₉NO₂S₃

February 11, 2014

M. Wilhelm, H. Strasdeit

Page range: 551-552

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C 13 H 19 NO 2 S 3 , monoclinic, P 2 1 (No. 4), a = 11.7973(9) Å, b = 5.6054(3) Å, c = 11.9380(9) Å, β = 107.977(9)°, V = 750.9 Å 3 , Z = 2, R gt (F) = 0.032, wR ref (F 2 ) = 0.083, T = 193 K.
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Crystal structure of 4-N-phenylisoindolinone, C₁₄H₁₁NO

February 11, 2014

M. Polamo, M. Talja

Page range: 553-554

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C 14 H 11 NO, monoclinic, P 12 1 / n 1 (No. 14), a = 5.925(4) Å, b = 7.556(2) Å, c = 23.11(1) Å, β = 94.67(5)°, V = 1031.3 Å 3 , Z = 4, R gt (F) = 0.055, wR ref (F 2 ) = 0.140, T = 193 K.
Open Access
Crystal structure of 4,7-dibromo-2,1,3-benzothiadiazole, C₆H₂Br₂N₂S

February 11, 2014

M. Tomura, Y. Yamashita

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C 6 H 2 Br 2 N 2 S, monoclinic, P 12 1 / c 1 (No. 14), a = 18.3670(9) Å, b = 3.9522(2) Å, c = 22.120(2) Å, β = 97.390(6)°, V = 1592.4 Å 3 , Z = 8, R gt (F) = 0.045, wR ref (F 2 ) = 0.127, T = 296 K.
Open Access
Crystal structure of diaqua-monodimethylglycine-hexakis(μ₂-dimethylglycine- O:O)-μ₃-oxo-triiron(III) heptanitrate—water—dimethylgycine solvate (1:4:0.63), Fe₃O(C₄H₉NO₂)₇(H₂O)₂(NO₃)₇ · 4H₂O · 0.63C₄H₉NO₂

February 11, 2014

M. Ramos Silva, A. Matos Beja, J. A. Paixão, J. Martin-Gil

Page range: 557-560

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C 30.20 H 80.60 Fe 3 N 14.30 O 43.26 , triclinic, P 1̅ (No. 2), a = 12.424(6) Å, b = 16.565(5) Å, c = 17.627(3) Å, α = 90.59(4)°, β = 101.48(4)°, γ = 108.97(4)°, V = 3351.1 Å 3 , Z = 2, R gt (F) = 0.070, wR ref (F 2 ) = 0.261, T = 293 K.
Open Access
Crystal structure of (±)-[(2R,3S)-3-(hydroxymethyl)oxiran-2-yl](phenyl)- methanone, C₁₀H₁₀O₃

February 11, 2014

B. W. Greatrex, D. K. Taylor, E. R. T. Tiekink

Page range: 561-562

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C 10 H 10 O 3 , orthorhombic, Pca 2 1 (No. 29), a = 20.165(4) Å, b = 5.667(1) Å, c = 7.583(2) Å, V = 866.6 Å 3 , Z = 4, R gt (F) = 0.072, wR ref (F 2 ) = 0.177, T = 223 K.
Open Access
Crystal structure of triaqua(1,10-phenanthroline-N,N′)sulfatonickel(II), Ni(H₂O)₃(C₁₂H₈N₂)SO₄

February 11, 2014

H.-Y. He, Y.-L. Zhou, L.-G. Zhu

Page range: 563-564

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C 12 H 14 N 2 NiO 7 S, monoclinic, P 12 1 / c 1 (No. 14), a = 11.8362(9) Å, b = 9.9634(8) Å, c = 13.560(1) Å, β = 112.852(1)°, V = 1473.6 Å 3 , Z = 4, R gt (F) = 0.042, wR ref (F 2 ) = 0.106, T = 293 K.
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Crystal structure of the adduct of sulfosalicylic acid and thiourea, C₇H₆O₆S · CH₄N₂S

February 11, 2014

J. Xiong, M.-L. Hu, Q. Shi, H.-P. Xiao

Page range: 565-566

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C 8 H 10 N 2 O 6 S 2 , monoclinic, P 12 1 / n 1 (No. 14), a = 7.6806(5) Å, b = 12.8546(8) Å, c = 12.2389(7) Å, β = 97.071(2)°, V = 1199.2 Å 3 , Z = 4, R gt (F) = 0.035, wR ref (F 2 ) = 0.099, T = 273 K.
Open Access
Crystal structure of imidazolium decanedioate, C₁₈H₃₁N₂O₆

February 11, 2014

J. Garbarczyk, K. Pogorzelec-Glaser

Page range: 567-568

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C 18 H 31 N 2 O 6 , triclinic, P 1̅(No. 2), a = 8.8249(8) Å, b = 8.992(2) Å, c = 12.897(2) Å, α = 95.22(1)°, β = 92.91(1)°, γ = 94.62(1)°, V = 1014.1 Å 3 , Z = 2, R gt (F) = 0.042, wR ref (F 2 ) = 0.124, T = 293 K.
Open Access
Crystal structure of 13,27-dichloro-29,30-dihydroxy-3,9,17,23-tetramethyl-6,20-dioxa-3,9,17,23-tetraazatri-cyclo[23.3.1.1^11.15]triaconta- 1(29),11,13,15(30),25,27-hexaene-(aqua)magnesium hydrate, Mg[C₂₈H₄₀Cl₂N₄O₄(H₂O)] · H₂O

February 11, 2014

A. Y. Nazarenko, N. K. Dalley, J. S. Bradshaw, V. N. Pastushok, J. D. Lamb

Page range: 569-571

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C 28 H 44 Cl 2 MgN 4 O 6 , triclinic, P 1̅ (No. 2), a = 10.397(3) Å, b = 11.152(3) Å, c = 14.728(5) Å, α = 74.25(2)°, β = 80.51(2)°, γ = 77.00(2)°, V = 1591.6 Å 3 , Z = 2, R gt (F) = 0.056, wR ref (F 2 ) = 0.174, T = 293 K.
Open Access
Crystal structure of tetraguanidinium dioxo-tetraperoxo-μ-tartratodimolybdate(VI) dihydrate, (CN₃H₆)₄[Mo₂O₂(O₂)₄(C₄H₂O₆)] · 2H₂O

February 11, 2014

B. Tinant, D. Bayot, M. Devillers

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C 16 H 60 Mo 4 N 24 O 36 , orthorhombic, Pna 2 1 (No. 33), a = 29.387(9) Å, b = 9.979(3) Å, c = 19.062(5) Å, V = 5590.0 Å 3 , Z = 4, R gt (F) = 0.094, wR ref (F 2 ) = 0.264, T = 293 K.
Open Access
Crystal structure of the antibiotic SY-1 (20-deoxy-salinomycin): sodium 2-(6-[2- (5-ethyl-5-hydroxy-6-methyl-tetrahydro-pyran-2-yl)-2,10,12-trimethyl- 1,6,8-trioxa-dispiro[4.1.5.3]pentadec-13-en-9-yl]-2-hydroxy-1,3-dimethyl-4-oxo-heptyl-5-methyl-tetrahydro-pyran-2-yl)-butyrate—methanol solvate (1:0.69), C₄₂H₆₉NaO₁₀ · 0.69CH₃OH

February 11, 2014

E. F. Paulus, L. Vértesy

Page range: 575-577

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C 42.693 H 71.772 NaO 10.693 , orthorhombic, P 2 1 2 1 2 1 (No. 19), a = 11.295(1) Å, b = 18.628(1) Å, c = 21.823(1) Å, V = 4591.6 Å 3 , Z = 4, R gt (F) = 0.037, wR ref (F 2 ) = 0.099, T = 293 K.

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