Structure of MgLiAl alloys after various routes of severe plastic deformation studied by TEM
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Jan Dutkiewicz
, Stanislav Rusz , Ondrej Hilsner , Tomasz A. Tański , Wojciech Borek , Maciej Szlezynger , Piotr Bobrowski and Wojciech Maziarz
Abstract
Two MgLiAl alloys consisting either of α (hcp) + β (bcc) phases or only β phase were subjected to twist channel angular pressing TCAP (with helical component) or cyclic compression to a total strain of ∊ = 5 in order to study the effectiveness of various deformation modes on grain refinement. After the first TCAP pass grains of α phase were refined from 30 μm down to about 6 μm and of β phase from initial 200 μm down to 8 μm. MAXStrain cycling led to much finer grains of α and β phases in the range 200 – 300 nm causing higher hardening and indicating higher effectiveness of the process. The Li2MgAl precipitates were refined during severe plastic deformation (SPD) processes and in addition fine particles of hexagonal α phase of size below 100 nm were observed within the β phase showing orientation relationship (0001) α ‖ (011) β. Two-phase material after SPD showed deviation of about 1.5° from the ideal Burgers orientation relationship (0001) α ‖ (011) β.
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Articles in the same Issue
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- XVI International Conference on Electron Microscopy
- Original Contributions
- Application of analytical electron microscopy and FIB-SEM tomographic technique for phase analysis in as-cast Allvac 718Plus superalloy
- Microstructure and properties of laser interference crystallized amorphous FeSiB ribbon
- Analysis of amorphous regions in severely marformed NiTi shape memory alloy
- Structure of MgLiAl alloys after various routes of severe plastic deformation studied by TEM
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- Microstructure of an oxide scale formed on ATI 718Plus superalloy during oxidation at 850 °C characterised using analytical electron microscopy
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- Short Communications
- Characterization of Inconel 625 surface layer modified by laser shock processing
- DGM News
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Articles in the same Issue
- Contents
- Contents
- Editorial
- XVI International Conference on Electron Microscopy
- Original Contributions
- Application of analytical electron microscopy and FIB-SEM tomographic technique for phase analysis in as-cast Allvac 718Plus superalloy
- Microstructure and properties of laser interference crystallized amorphous FeSiB ribbon
- Analysis of amorphous regions in severely marformed NiTi shape memory alloy
- Structure of MgLiAl alloys after various routes of severe plastic deformation studied by TEM
- Microstructure and selected mechanical and electrical property analysis of Sr-doped LaCoO3 perovskite thin films deposited by the PLD technique
- Microstructure of an oxide scale formed on ATI 718Plus superalloy during oxidation at 850 °C characterised using analytical electron microscopy
- Effect of powder morphology on the microstructure and properties of cold sprayed Ni coatings
- Microstructure of Ti/Al multilayer foils ignited with electric current
- Evolution of γ′ morphology and γ/γ′ lattice parameter misfit in a nickel-based superalloy during non-equilibrium cooling
- Effect of heat treatment on the precipitation hardening in FeNiCoAlTaB shape memory alloys
- The structure and formation mechanism of FeS2/Fe3S4/S8 nanocomposite synthesized using spherical shaped Fe3O4 nanoparticles as the precursor
- Short Communications
- Characterization of Inconel 625 surface layer modified by laser shock processing
- DGM News
- DGM News