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Mutual consistency of hardness testing at micro- and nanometer scales

  • Alexey Useinov , Kirill Gogolinskiy and Vladimir Reshetov
Published/Copyright: June 11, 2013

Abstract

To a considerable degree hardness is an empirical value which depends on many details involved in the measuring process. In the present work, hardness values were measured in the depth range 2 – 800 nm using microhardness, nanoindentation and scratch hardness tests on fused silica, steel and sapphire. It is shown that overestimation of hardness values for steel and sapphire with the nanoindentation method can be directly related to the relative height of pile-ups observed on the topography image of the indentation imprint. It is also shown that the scratch hardness test is a promising technique for nanoscaled hardness measurements.


* Correspondence address, Dr. Alexey Useinov, 7a, Centralnaya str., Troitsk, Moscow region, 142190, Russia, Tel.: +7 495 334 08 55, Fax: +7 495 330 99 60, E-mail:

References

[1] S.I.Bulychev, V.P.Alekhin, M.Kh.Shorshorov, A.P.Ternovskii, G.D.Shnyrev: Zavod. Lab.39 (1973) 1242 [in Russian].Search in Google Scholar

[2] A.P.Ternovskii, V.P.Alekhin, M.K.Shorshorov, M.M.Khrushchov, V.N.Skvortsov: Zavod. Lab.41 (1975) 1137 [in Russian].Search in Google Scholar

[3] S.I.Bulychev, V.P.Alekhin, M.K.Shorshorov, A.P.Ternovskii, G.D.Shnyrev: Prob. Prochn.9 (1976) 79 [in Russian].Search in Google Scholar

[4] W.C.Oliver, G.M.Pharr: J. Mater. Res.7 (1992) 1564.Search in Google Scholar

[5] W.C.Oliver, G.M.Pharr: J. Mater. Res.19 (2004) 3.Search in Google Scholar

[6] ISO/FDIS 14577-1: 2002; Metallic materials – Instrumented indentation test for hardness and materials parameters.Search in Google Scholar

[7] F.Mohs: Grundriss der Mineralogie, Arnold, Dresden (1822).Search in Google Scholar

[8] J.A.Williams: Trib. Int.29 (1996) 675.10.1016/0301-679X(96)00014-XSearch in Google Scholar

[9] V.Blank, K.Gogolinsky, N.Lvova, M.Popov, V.Reshetov: J. Mater. Res.12 (1997) 3109.Search in Google Scholar

[10] V.Blank, M.Popov, G.Pivovarov, N.Lvova, K.Gogolinsky, V.Reshetov: Diam. Rel. Mater.7 (1998) 427.Search in Google Scholar

[11] I.A.Chaban, K.V.Gogolinski, Z.Y.Kosakovskaya, A.S.Useinov: Acoust. Phys.50 (2004) 664.Search in Google Scholar

[12] A.S.Useinov: Instr. Exp. Tech.47 (2004) 119.10.1023/B:INET.0000017264.83566.69Search in Google Scholar

[13] W.D.Nix, H.Gao: J. Mech. Phys. Solids46 (1998) 411.Search in Google Scholar

[14] K.Durst, B.Backes, O.Franke, M.Goken: Acta Mater.54 (2006) 2547.Search in Google Scholar

[15] K.O.Kese, Z.C.Li, B.Bergman: Mater. Sci. Eng. A404 (2005) 1.Search in Google Scholar

Received: 2008-11-1
Accepted: 2009-2-1
Published Online: 2013-06-11
Published in Print: 2009-07-01

© 2009, Carl Hanser Verlag, München

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