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Indentation-induced densification of soda-lime silicate glass

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Published/Copyright: May 23, 2013
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International Journal of Materials Research
From the journal International Journal of Materials Research Volume 98 Issue 5

Abstract

Glass is densified under a sharp diamond indenter. The densification is not a volume conservative process, and does not contribute to the volume strain around the indentation. This means that densification affects residual stresses around the indentation impression. In order to estimate the densification volume, three-dimensional images of Vickers indentations on soda-lime silicate glasses were obtained before and after annealing. Only the densified volume can be recovered by annealing. After annealing at around glass transition temperature, large volume recovery (55 – 80 %) of Vickers indentation was observed for soda-lime silicate glass. The volume recovery is much larger than the recoveries of indentation diagonal and depth. It is found that the densification of glass under the sharp indenter cannot be ignored for evaluating crack initiation and brittleness of glass. In addition, the residual stresses around the indentation impression were also estimated from the plastically deformed volume and the size of plastic zone around the indentation.

Keywords: Glass; Densification; Residual stress; Indentation; Atomic force microscopy
* Correspondence address, Dr. Satoshi Yoshida, Department of Materials Science, The University of Shiga Prefecture, 2500, Hassaka, Hikone, 522-533 Shiga, Japan, Tel.: +81 749 28 8366, Fax: +81 749 28 8596, E-mail:

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Received: 2006-10-11
Accepted: 2007-1-14
Published Online: 2013-05-23
Published in Print: 2007-05-01

© 2007, Carl Hanser Verlag, München

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  6. Getting accurate nanoindentation data from time-dependent and microstructural effects of zinc
  7. Indentation-induced densification of soda-lime silicate glass
  8. Nanomechanical characterization of relaxation processes in As–S chalcogenide glasses
  9. Nanoindentation behavior and mechanical properties measurement of polymeric materials
  10. Model of a superlattice indentation
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  12. Mechanical properties of nanostructured polymer particles for anisotropic conductive adhesives
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  14. Testing the viscoelastic properties of SU8 photo resist thin films at different stages of processing by nanoindentation creep and stress relaxation
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  19. Multiscale modelling of nanoindentation
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  21. Notifications
  22. DGM News
https://doi.org/10.3139/146.101478
Keywords for this article
Glass; Densification; Residual stress; Indentation; Atomic force microscopy

Articles in the same Issue

  1. Contents
  2. Contents
  3. Editorial
  4. Editorial
  5. Basic
  6. Getting accurate nanoindentation data from time-dependent and microstructural effects of zinc
  7. Indentation-induced densification of soda-lime silicate glass
  8. Nanomechanical characterization of relaxation processes in As–S chalcogenide glasses
  9. Nanoindentation behavior and mechanical properties measurement of polymeric materials
  10. Model of a superlattice indentation
  11. Nanomechanical studies of MEMS structures
  12. Mechanical properties of nanostructured polymer particles for anisotropic conductive adhesives
  13. Nanomechanical studies of ultrathin polymeric resist films
  14. Testing the viscoelastic properties of SU8 photo resist thin films at different stages of processing by nanoindentation creep and stress relaxation
  15. Microscale characterization of bitumen – back-analysis of viscoelastic properties by means of nanoindentation
  16. Applied
  17. Visco-elastic properties of thin nylon films using multi-cycling nanoindentation
  18. Area function calibration in nanoindentation using the hardness instead of Young's modulus of fused silica as a reference value
  19. Multiscale modelling of nanoindentation
  20. Unusual architecture of the exceedingly tough Macadamia “nut”-shell as revealed by atomic force microscopy and nanomechanics
  21. Notifications
  22. DGM News
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