Corrosion failure analysis of a perforated F32 reactor
-
Li-Hua Gong
Abstract
The principle reason for corrosion failure because of perforation on a fluorination reactor was analyzed by chemical composition tests, microstructure and corrosion products observation tests in combination with the investigation of the working conditions of the reactor. The results show that a certain amount of complex inclusions containing MnS in the failure parts – are the principle cause of perforation. The relatively poor condition of the middle of the reactor, resulting in particular from excess hydrogen fluoride, is another principle cause.
References
1 H.Ouyang, H. L.He, L. Y.Zhou, Y. J.Zhong: Reaction mechanism in liquid phase fluorinated catalytic synthesizing difluoromethane and the corrosivity, Chemical Production and Technology19 (2012), No. 1, pp. 1–310.3969/j.issn.1006-6829.2012.01.001Search in Google Scholar
2 Q.He, W. X.Tang, J.Zhang, X. R.Wang: Effects of concentrated rigid inclusions defects on the in-plane impact behavior of hexagonal honeycombs, Journal of Mechanical Science and Technology31 (2017), No. 10, pp. 4691–470110.1007/s12206-017-0915-5Search in Google Scholar
3 C. B.Zheng, Y. L.Huang, Q.Yu, C. Y.Huo: Effect of H2S on stress corrosion cracking and hydrogen permeation behaviour of X56 grade steel in atmospheric environment, Corrosion Engineering, Science and Technology44 (2009), No. 2, pp. 96–100, 10.1179/174327808X272414Search in Google Scholar
4 H. B.Wu, D.Wang, J. M.Liang, P. C.Zhang, X. T.Liu, Y. J.Yue: Influence of inclusion on pitting corrosion behavior of low-alloy steel for bottom plates of cargo oil tanks, Transactions of Materials and Heat Treatment35 (2014), No. 12, pp. 172–17810.13289/j.issn.1009-6264.2014.12.031Search in Google Scholar
5 M.Li, L. Q.Guo, L. J.Qiao: The mechanism of hydrogen-induced pitting corrosion in duplex stainless steel studied by SKPFM, Corrosion Science60 (2012), pp. 76–8110.1016/j.corsci.2012.04.010Search in Google Scholar
6 W.Zheng, X. H.Fu, Y.Qu, S.Xiong, G. Q.Li: Inclusion-induced pitting corrosion behaviors in Al-Mg/Ti-Mg deoxidized steel, Journal of Wuhan University of Science and Technology40 (2017), No. 2, pp. 81–8710.3969/j.issn.1674-3644.2017.02.001Search in Google Scholar
7 B.Lin, R. G.Hu, C.Ye, Y.Li, C. J.Lin: A Study on the initiation of pitting corrosion in carbon steel in chloride containing media using scanning electrochemical probes, Electrochimica Acta55 (2010), No. 22, pp. 6542–654510.1016/j.electacta.2010.06.024Search in Google Scholar
8 C. Y.Zhang, Q.Zhang, J. G.Li, C. G.Xiong, Z.Li: Micro-corrosion test research on pitting initiation site of the inclusions of carbon steel and low alloy steel in chlorine ion solution, Metallurgical Analysis34 (2014), No. 1, pp. 22–2710.13228/j.issn.1000-7571.2014.01.004Search in Google Scholar
9 X. C.Ren, W. Y.Chu, J.Li, J. Y.Su, L. J.Qiao: Influence of inclusions on initiation of hydrogen blister in iron, Acta Metallurgica Sinica43 (2007), No. 7, pp. 673–67710.3321/j.issn:0412-1961.2007.07.001Search in Google Scholar
10 C. B.Zheng, B. H.Yan, K.Zhang, G.Yi: Electrochemical investigation on the hydrogen permeation behavior of 7075-T6 Al alloy and its influence on stress corrosion cracking, International Journal of Minerals, Metallurgy and Materials22 (2015), No. 7, pp. 729–736, 10.1007/S12613-015-1128-5.Search in Google Scholar
© 2019, Carl Hanser Verlag, München
Articles in the same Issue
- Inhalt/Contents
- Contents
- Fachbeiträge/Technical Contributions
- Investigation of phase transformations in mill scales for the purification process
- Exposure response function for a quantitative prediction of weathering caused aging of polyethylene
- Mechanical properties characterization of resistance spot welded DP1000 steel under uniaxial tensile tests
- Corrosion failure analysis of a perforated F32 reactor
- Prediction of mechanical properties of Al6061 metal matrix composites reinforced with zircon sand and boron carbide
- Tribological behavior of a hydrostatically extruded ultra-fine grained Ti-13Nb-13Zr alloy
- Characterization of boronized AISI 1050 steel and optimization of process parameters
- Experimental investigation on mechanical properties of AA7075-AlN composites
- Modeling of machining parameters for MRR and TWR in EDM characteristics on Al/10 wt.-% TiB2 composites
- Artificial neural network approach to predict ion nitrided case depth and surface hardness of AISI 4340 steel
- Theoretical and experimental investigation of stress distribution in a crane hook
- Mechanical properties, degradation and flue gas analysis of basalt and glass fiber reinforced recycled polypropylene
- Corrosion behavior of a precipitation hardened Ni–Cr–Co–Mo alloy under partial slagging coal gasification conditions
- Effect of different loading systems on acousto-ultrasonic characteristics of concrete under axial compression
Articles in the same Issue
- Inhalt/Contents
- Contents
- Fachbeiträge/Technical Contributions
- Investigation of phase transformations in mill scales for the purification process
- Exposure response function for a quantitative prediction of weathering caused aging of polyethylene
- Mechanical properties characterization of resistance spot welded DP1000 steel under uniaxial tensile tests
- Corrosion failure analysis of a perforated F32 reactor
- Prediction of mechanical properties of Al6061 metal matrix composites reinforced with zircon sand and boron carbide
- Tribological behavior of a hydrostatically extruded ultra-fine grained Ti-13Nb-13Zr alloy
- Characterization of boronized AISI 1050 steel and optimization of process parameters
- Experimental investigation on mechanical properties of AA7075-AlN composites
- Modeling of machining parameters for MRR and TWR in EDM characteristics on Al/10 wt.-% TiB2 composites
- Artificial neural network approach to predict ion nitrided case depth and surface hardness of AISI 4340 steel
- Theoretical and experimental investigation of stress distribution in a crane hook
- Mechanical properties, degradation and flue gas analysis of basalt and glass fiber reinforced recycled polypropylene
- Corrosion behavior of a precipitation hardened Ni–Cr–Co–Mo alloy under partial slagging coal gasification conditions
- Effect of different loading systems on acousto-ultrasonic characteristics of concrete under axial compression