Effect of the sintering temperature on the coating of duplex stainless steel with Ni3Al

Vedat Veli Çay; Nida Katı; Sermin Ozan; Tayfun Çetin

doi:10.3139/120.111185

Artikel

Effect of the sintering temperature on the coating of duplex stainless steel with Ni₃Al

Vedat Veli Çay , Nida Katı , Sermin Ozan und Tayfun Çetin

Veröffentlicht/Copyright: 15. November 2018

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Aus der Zeitschrift Materials Testing Band 60 Heft 6

Abstract

In this study, duplex stainless steel was coated with Ni₃Al powder via self-propagating high-temperature synthesis (SHS) and the effect of the sintering temperature on the coating characteristics was investigated. An SEM electron microscope with EDX (energy dispersive X-ray spectroscopy) was used to examine the microstructure of samples that were coated according to the SHS method and likewise to detect the element content of the phases in the structure. Microhardness tests were conducted on the samples to determine the mechanical properties of the coated material. As a result of these studies, it was found that duplex stainless steel can be reliably coated with an Ni₃Al intermetallic compound. The increase in sintering temperature within the given range significantly decreased the size of the disconnected area which completely disappeared.

Kurzfassung

In der diesem Beitrag zugrunde liegenden Studie wurde Duplexstahl mit Ni₃Al-Pulver mittels Hochtemperatursynthese (self-propagating high-temperature synthesis (SHS)) beschichtet und die Auswirkungen der Temperatur und Zeitdauer während der Herstellung untersucht. Hierzu wurden Rasterelektronenmikroskopien mittels EDX durchgeführt, um die Mikrostruktur der beschichteten Proben zu untersuchen und die Elementverteilung in den Phasen zu detektieren. Es wurden Messungen der Mikrohärte durchgeführt, um die mechanischen Eigenschaften der Beschichtungen zu prüfen. Als ein Ergebnis stellte sich heraus, dass Duplexstahl zuverlässig mit der intermetallischen Phase Ni₃Al beschichtet werden kann. Mit zunehmender Sintertemperatur wurde die nicht verbundene Fläche auf Null reduziert.

*Correspondence Address, Assoc. Prof. Vedat Veli Çay, Civil Aviation Higher School, Dicle University, 21280, Diyarbakır, Turkey, E-mail: vedatcay@yahoo.com

Associate Professor Vedat Veli Çay, born in 1977, received his MSc in 2003 and his PhD in 2009, respectively, at the Institute of Science and Technology in the Metal Education Department of te University of Firat in Elazığ, Turkey. Since 2009, he has been working at Dicle University, Diyarbakır, Turkey. His fields of interests include fusion welding method, solid state welding method, materials science, composite materials, powder metallurgy, manufacturing techniques, surface modification and tribology.

Assistant Professor Nida Katı, born in 1988, received his BSc in the Faculty of Technical Education and the Metal Education Department of the University of Firat n Elaziğ, Turkey, in 2009. In 2014, she received her PhD also at the University of Firat, in the Institute of Science and Technology and the Metallurgy Department,. Her research areas include fusion welding, solid state welding, materials science, composite materials, powder metallurgy, manufacturing techniques and surface modification.

Associate Professor SerminOzan, born in 1970, received her BSc in the Faculty of Engineering and the Mechanical Engineering Department in of the University of Firat, Elaziğ, Turkey, in 1994. In 2000, she received her PhD at the same university. Her research areas include fusion materials science, composite materials, powder metallurgy, manufacturing techniques welding, solid state welding, and surface modification.

Research Assistant Tayfun Çetin, born in 1988, received his BSc in the Faculty of Technical Education and the Metal Education Department of the University of Firat in Elaziğ, Turkey, in 2010. He completed his master's degree also atr Firat University, Metallurgy in Education Department in 2014. After completing the same year at Karabük University Faculty of Engineering Metallurgical and Materials Engineering from the Department of Licensing Program and graduated in 2016. He is continuing his doctoral training in the Manufactiring Engineering Department at the same universty.

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Published Online: 2018-11-15

Published in Print: 2018-06-30

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https://doi.org/10.3139/120.111185