Interdisciplinary study on pottery experimentally impregnated with wine
-
Eugenia Teodor
,
Georgiana Badea
Abstract
Experimentally developed ceramic pots, with two different sizes of grain, were half-filled with wine and subjected to thermal alteration at constant elevated temperature ((60 ± 2)°C) in darkness for 12 weeks. This work sought to characterise the samples thereby obtained from chemical and mineralogical perspectives using scanning electron microscopy and an energy-dispersive X-ray microanalysis system (SEM-EDX), Fourier transform infrared spectroscopy (FTIR) and capillary electrophoresis (CE) with UV detection as an alternative to chromatographic methods, due to its good resolution, automation, simplicity, high speed, low consumption of chemicals and short time required for sample preparation. The capillary electrophoresis method was used for the detection of five wine biomarkers: succinic acid, malic acid, tartaric acid, citric acid and lactic acid. In general, it was noted that the fine-grained ceramic assortment retained the organic material better than the coarser-grained ceramics. An interesting observation derived from this study was that not only could tartaric acid be considered as a biomarker for wine residues in archaeological pottery, but malic acid could also act similarly for white wine and lactic acid for red wine.
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© 2014 Institute of Chemistry, Slovak Academy of Sciences
Artikel in diesem Heft
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Artikel in diesem Heft
- Recent advances in application of liquid-based micro-extraction: A review
- Determination of nitrites and nitrates in drinking water using capillary electrophoresis
- Comparison of digestion methods for determination of total phosphorus in river sediments
- Interdisciplinary study on pottery experimentally impregnated with wine
- Improvement in γ-decalactone production by Yarrowia sp. after genome shuffling
- Development of an effective extraction process for coenzyme Q10 from Artemia
- Effect of anions on the structure and catalytic properties of a La-doped Cu-Mn catalyst in the water-gas shift reaction
- Effect of apple pomace powder addition on farinographic properties of wheat dough and biscuits quality
- Influence of caffeine and temperature on corrosion-resistance of CoCrMo alloy
- Cetyltrimethylammonium bromide- and ethylene glycol-assisted preparation of mono-dispersed indium oxide nanoparticles using hydrothermal method
- Sol-gel synthesis, characterisation, and photocatalytic activity of porous spinel Co3O4 nanosheets
- Solvent-free synthesis of β-enamino ketones and esters catalysed by recyclable iron(III) triflate
- Potassium phthalimide-catalysed one-pot multi-component reaction for efficient synthesis of amino-benzochromenes in aqueous media
- Organocatalytic SOMO reactions of copper(I)-acetylide and alkylindium compounds with aldehydes
- Molecular modelling and quantitative structure-activity relationship studies of anatoxin-a and epibatidine derivatives with affinity to rodent nAChR receptors
- Efficient one-pot synthesis of 2-hydroxyethyl per-O-acetyl glycosides
- Properties of singlet- and triplet-excited states of hemicyanine dyes
