Startseite Solid phase conformational analysis of a 13-membered heterocycle: 8,13-Dioxo-1,4,7-trioxacyclotridecane (diethylene glycol cyclic adipate)
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Solid phase conformational analysis of a 13-membered heterocycle: 8,13-Dioxo-1,4,7-trioxacyclotridecane (diethylene glycol cyclic adipate)

Veröffentlicht/Copyright: 28. Juli 2010
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Zeitschrift für Kristallographie
Aus der Zeitschrift Zeitschrift für Kristallographie Band 202 Heft 1-2

Abstract

The crystal structure of the title compound (C10H16O5) has been determined by X-ray diffraction methods in order to ascertain the preferred conformation. Crystals are monoclinic, space group P21/c (No. 14) with a = 8.020(2), b = 16.188(1), c = 8.559(1) Å, β = 99.87(1), V = 1094.7(3) Å3, Z = 4, D = 1.312 g · cm−3, λ(MoKα) = 0.71069 Å, μ = 0.9 cm−1, F(000) = 432, T = 293 K. The final R was 0.045 for 1026 observed reflections. The conformation is of the [13333] type with corners at C2, C3, C6, C9 and C12. Both ester groups are in syn conformation.

Published Online: 2010-07-28
Published in Print: 1992

Artikel in diesem Heft

  1. Structure of p-methylbenzene sulfonamide
  2. The crystal structures of two solid phases of 4-cyano-4′-ethyl-biphenyl
  3. Crystal structure of 2-hydroxy-N-methylbenzamide and 2-hydroxy-N-methylthiobenzamide
  4. Crystal structure of mesogenic material – 2-(4′-Undecoxy phenyl)-5-N-hexyl pyrimidine
  5. Crystal structure of lignocaine hydrochloride – platinum complex
  6. Tobermorite, jennite, and cement gel
  7. On the geometry of Co(II)O6 polyhedra in inorganic compounds
  8. The crystal structure of a rare earth bearing leucophanite: (Ca,RE)CaNa2Be2Si4O12(F,O)2
  9. The crystal structure of tetramethylammonium tetrafluoroborate, (CH3)4NBF4, and the disorder of the BF4− ion
  10. The crystal structure of the conformationally constrained peptide Z-(Aib)6-OBut
  11. The crystal structure of SeO2 at 139 and 286 K
  12. Solid phase conformational analysis of a 13-membered heterocycle: 8,13-Dioxo-1,4,7-trioxacyclotridecane (diethylene glycol cyclic adipate)
  13. Crystal structure of calcium ultraphosphate, Ca2P6O17
  14. Crystal structure of 3-(9-anthryl)-6H-benz[de]anthracen-6-one, C31H18O
  15. Crystal structure of 3-(9-anthryl)-7H-benz[de]anthracen-7-one, C31H18O
  16. Crystal structure of 3-(9-anthryl)-1-methoxy-1H-2,3-dihydrobenz[de]anthracene, C32H24O
  17. Crystal structure of 3-(9-anthryl)-1H-2,3-dihydrobenz[de]anthracene, C31H22
  18. Crystal structure of 1-acetoxy-1,3-di-anthrylpropane, C33H26O2
  19. Crystal structure of aqua-2,2′-bipyridine-N,N′-dioxide-bis(2-furancarboxylato)-copper(II), (H2O)(C4H4OCO2)2Cu(ONC5H4C5H4NO)
  20. Crystal structure of bis(aqua)bis(2,2′-bipiperidine)copper(II) bromide, (NH(CH2)4(CH)2(CH2)4NH)2Cu(OH2)2Br2
  21. Crystal structure of aqua-2,2′-bipyridine-N,N′-dioxide-bis(nitrato)-copper(II), (H2O)(NO3)Cu(ONC5H4C5H4NO)
  22. Crystal structure of μ-bromo-bis(bis(2,2′-bipiperidine)copper(II)) perchlorate, ((NH(CH2)4(CH)2(CH2)4NH)2Cu)2Br(ClO4)3
  23. Crystal structure of high temperature thallium lead antimony sulfide, Tl0.333Pb0.333Sb0.333S
  24. Crystal structure of dibromo-bis(tricarbonyl-η-cyclopentadienyl-molybdenum)-tin(II), Br2((CO)3(C5H5)Mo)2Sn
  25. Crystal structure of dipotassium iron thiohypodiphosphate, K2FeP2S6
  26. Crystal structure of copper mercury tetrathiophosphate, CuHgPS4
  27. Crystal structure of o-hydroxybenzeneazo-β-naphthol, C16H12N2O2
  28. Crystal structure of 1,3-diisopropyl-2,4-diisopropylamino-2,4-dithioxo-1,3,2-λ5,4λ5-diazadiphosphetidine, C12H28N4P2S2
  29. Crystal structure of 2,4-bis(p-methoxyphenyl)-2,4-dithioxo-1,3,2-λ5,4λ5-dithiadiphosphetane, C14H14P2S4
  30. Crystal structure refinement of osmium(II) disulfide, OsS2
  31. Crystal structure refinement of osmium(II) ditelluride, OsTe2
  32. Crystal structure of (E)-2,3,6-trimethoxypentafulvene-1-carbonitrile, (CH3O)3(C6H2)(CN)
  33. Crystal structure of cyclo(C-α-methyl-phenylalanine-proline) (S,S)/(R,S) diastereomeric mixture, C15H18N2O2
  34. Crystal structure of N-tert-butyloxycarbonyl-(S)-pipecolyl-α-aminoisobutyric acid, C15H26N2O5
  35. Crystal structure of (S)-pipecolic acid (2R,3R)-tartrate, C10H17NO8
https://doi.org/10.1524/zkri.1992.202.1-2.109

Artikel in diesem Heft

  1. Structure of p-methylbenzene sulfonamide
  2. The crystal structures of two solid phases of 4-cyano-4′-ethyl-biphenyl
  3. Crystal structure of 2-hydroxy-N-methylbenzamide and 2-hydroxy-N-methylthiobenzamide
  4. Crystal structure of mesogenic material – 2-(4′-Undecoxy phenyl)-5-N-hexyl pyrimidine
  5. Crystal structure of lignocaine hydrochloride – platinum complex
  6. Tobermorite, jennite, and cement gel
  7. On the geometry of Co(II)O6 polyhedra in inorganic compounds
  8. The crystal structure of a rare earth bearing leucophanite: (Ca,RE)CaNa2Be2Si4O12(F,O)2
  9. The crystal structure of tetramethylammonium tetrafluoroborate, (CH3)4NBF4, and the disorder of the BF4− ion
  10. The crystal structure of the conformationally constrained peptide Z-(Aib)6-OBut
  11. The crystal structure of SeO2 at 139 and 286 K
  12. Solid phase conformational analysis of a 13-membered heterocycle: 8,13-Dioxo-1,4,7-trioxacyclotridecane (diethylene glycol cyclic adipate)
  13. Crystal structure of calcium ultraphosphate, Ca2P6O17
  14. Crystal structure of 3-(9-anthryl)-6H-benz[de]anthracen-6-one, C31H18O
  15. Crystal structure of 3-(9-anthryl)-7H-benz[de]anthracen-7-one, C31H18O
  16. Crystal structure of 3-(9-anthryl)-1-methoxy-1H-2,3-dihydrobenz[de]anthracene, C32H24O
  17. Crystal structure of 3-(9-anthryl)-1H-2,3-dihydrobenz[de]anthracene, C31H22
  18. Crystal structure of 1-acetoxy-1,3-di-anthrylpropane, C33H26O2
  19. Crystal structure of aqua-2,2′-bipyridine-N,N′-dioxide-bis(2-furancarboxylato)-copper(II), (H2O)(C4H4OCO2)2Cu(ONC5H4C5H4NO)
  20. Crystal structure of bis(aqua)bis(2,2′-bipiperidine)copper(II) bromide, (NH(CH2)4(CH)2(CH2)4NH)2Cu(OH2)2Br2
  21. Crystal structure of aqua-2,2′-bipyridine-N,N′-dioxide-bis(nitrato)-copper(II), (H2O)(NO3)Cu(ONC5H4C5H4NO)
  22. Crystal structure of μ-bromo-bis(bis(2,2′-bipiperidine)copper(II)) perchlorate, ((NH(CH2)4(CH)2(CH2)4NH)2Cu)2Br(ClO4)3
  23. Crystal structure of high temperature thallium lead antimony sulfide, Tl0.333Pb0.333Sb0.333S
  24. Crystal structure of dibromo-bis(tricarbonyl-η-cyclopentadienyl-molybdenum)-tin(II), Br2((CO)3(C5H5)Mo)2Sn
  25. Crystal structure of dipotassium iron thiohypodiphosphate, K2FeP2S6
  26. Crystal structure of copper mercury tetrathiophosphate, CuHgPS4
  27. Crystal structure of o-hydroxybenzeneazo-β-naphthol, C16H12N2O2
  28. Crystal structure of 1,3-diisopropyl-2,4-diisopropylamino-2,4-dithioxo-1,3,2-λ5,4λ5-diazadiphosphetidine, C12H28N4P2S2
  29. Crystal structure of 2,4-bis(p-methoxyphenyl)-2,4-dithioxo-1,3,2-λ5,4λ5-dithiadiphosphetane, C14H14P2S4
  30. Crystal structure refinement of osmium(II) disulfide, OsS2
  31. Crystal structure refinement of osmium(II) ditelluride, OsTe2
  32. Crystal structure of (E)-2,3,6-trimethoxypentafulvene-1-carbonitrile, (CH3O)3(C6H2)(CN)
  33. Crystal structure of cyclo(C-α-methyl-phenylalanine-proline) (S,S)/(R,S) diastereomeric mixture, C15H18N2O2
  34. Crystal structure of N-tert-butyloxycarbonyl-(S)-pipecolyl-α-aminoisobutyric acid, C15H26N2O5
  35. Crystal structure of (S)-pipecolic acid (2R,3R)-tartrate, C10H17NO8
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