Home Physical Sciences Präzisionsbestimmung des Skalierungsfaktors für Relativwerte von Strukturamplituden mit Messung von Absolutintensitäten an Pulverpräparaten
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Präzisionsbestimmung des Skalierungsfaktors für Relativwerte von Strukturamplituden mit Messung von Absolutintensitäten an Pulverpräparaten

Published/Copyright: August 25, 2010
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Abstract

A method for the precise determination of the X-ray scale factor measuring absolute intensities from powder specimens has been tested. It proved to be applicable to electron density determinations of high accuracy with a relative standard deviation of 1 – 2% of the observed relative structure amplitudes. The necessary sample quality showed to be the most serious possible handicap.

Published Online: 2010-08-25
Published in Print: 1989
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