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Ratio image seeking with multiple-wavelength X-ray diffraction data

Published/Copyright: August 25, 2010
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Zeitschrift für Kristallographie
From the journal Zeitschrift für Kristallographie Volume 188 Issue 3-4

Abstract

The deconvolution of (multiple wavelength) Patterson maps by minimum function was replaced by ratio image seeking (β synthesis). The resulting map shows less spurious peaks and more details in two heavyatom structures (hemimorphite, barium nitrite monohydrate). The transformation of Bijvoet differences in a Sinus-Patterson synthesis enabled the estimation of hydrogen positions which could not be derived by usual X-ray methods.

Published Online: 2010-08-25
Published in Print: 1989

Articles in the same Issue

  1. Limits of isomorphous substitution of CnH2n + 2 chains in paraffins as a function of temperature
  2. Crystal structure analysis from powder diffraction data
  3. Intensitätsstatistik für Strukturen mit Überstruktureffekten
  4. Crystal and molecular structure of 10-methoxy-8, 8-dimethyl 2H,8H-benzo (1,2-b:5,4-b′-dipyron-2-one) (Luvangetin)
  5. Crystal structure of a complex of glycine with zinc chloride
  6. Ratio image seeking with multiple-wavelength X-ray diffraction data
  7. Verfeinerung der Kristallstruktur von Anthophyllit vom Ochsenkogel/Gleinalpe, Österreich
  8. Präzisionsbestimmung des Skalierungsfaktors für Relativwerte von Strukturamplituden mit Messung von Absolutintensitäten an Pulverpräparaten
  9. The X-ray revised stereochemistry of the hydroperoxide of atractyligenin
  10. Crystal structures of N-benzylcarbonyl-α-aminoisobutyric acid mono- and tripeptide methyl ester derivatives
  11. The crystal structure of U4Ni5Al18
  12. The crystal structure of Cs2Nd(N3)5
  13. The crystal structure of Tl5Te3 and its relationship to the Cr5B3 type
  14. A phosphorous ylide with a secondary P…O bond. The crystal structure of a-[6-furazano][3,4-b]-quinoxalinyl-a-carbethoxymethylenetriphenylphosphorane(butene-2,3,4-dimethylhexene-3)solvate
  15. New data for 2-thiophenecarboxylic acid
  16. Elastic and thermoelastic properties of twelve adducts of betaine, (CH3)3NCH2COO, with H2O, HCl, HBr, HI, HNO3, H2SO4, H3PO3, H3PO4, 1,4-toluene sulfonic acid, MnCl2 and KBr
https://doi.org/10.1524/zkri.1989.188.3-4.223

Articles in the same Issue

  1. Limits of isomorphous substitution of CnH2n + 2 chains in paraffins as a function of temperature
  2. Crystal structure analysis from powder diffraction data
  3. Intensitätsstatistik für Strukturen mit Überstruktureffekten
  4. Crystal and molecular structure of 10-methoxy-8, 8-dimethyl 2H,8H-benzo (1,2-b:5,4-b′-dipyron-2-one) (Luvangetin)
  5. Crystal structure of a complex of glycine with zinc chloride
  6. Ratio image seeking with multiple-wavelength X-ray diffraction data
  7. Verfeinerung der Kristallstruktur von Anthophyllit vom Ochsenkogel/Gleinalpe, Österreich
  8. Präzisionsbestimmung des Skalierungsfaktors für Relativwerte von Strukturamplituden mit Messung von Absolutintensitäten an Pulverpräparaten
  9. The X-ray revised stereochemistry of the hydroperoxide of atractyligenin
  10. Crystal structures of N-benzylcarbonyl-α-aminoisobutyric acid mono- and tripeptide methyl ester derivatives
  11. The crystal structure of U4Ni5Al18
  12. The crystal structure of Cs2Nd(N3)5
  13. The crystal structure of Tl5Te3 and its relationship to the Cr5B3 type
  14. A phosphorous ylide with a secondary P…O bond. The crystal structure of a-[6-furazano][3,4-b]-quinoxalinyl-a-carbethoxymethylenetriphenylphosphorane(butene-2,3,4-dimethylhexene-3)solvate
  15. New data for 2-thiophenecarboxylic acid
  16. Elastic and thermoelastic properties of twelve adducts of betaine, (CH3)3NCH2COO, with H2O, HCl, HBr, HI, HNO3, H2SO4, H3PO3, H3PO4, 1,4-toluene sulfonic acid, MnCl2 and KBr
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