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Removal of acid dye from wastewater by cloud point extraction and regeneration of surfactant by pH regulation

  • Halima Ghouas

    Halima Ghouas, Professor of chemical engineering at the Higher School of Eelectrical Engineering and Energy of Oran (ESGEEO).

     EMAIL logo     , Abdelkader Benderrag

    Abdelkader Benderrag, Professor of chemical engineering at the University of Science and Technology of Oran (USTO).

         , Boumedienne Haddou

    Boumedienne Haddou, Professor of chemical engineering at the University of Science and Technology of Oran (USTO).

         und Cristophe Gourdon

    Cristophe Gourdon, Professor of Chemical Engineering at the ENSIACET (INP Toulouse).
Veröffentlicht/Copyright: 8. Januar 2024
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Abstract

This work concerns the coacervate extraction of industrial dye, namely Acid Green 9 (AG-9) from aqueous solution by nonionic surfactant Lutensol AO7 and TX-114 (readily biodegradable). Binary water/surfactant and pseudo-binary phase diagrams were plotted. The extraction results as a function of wt% of the surfactant and temperature are expressed by: percentage of solute extracted, E%, residual concentrations of solute and surfactant in the dilute phase (X s,w and X t,w respectively) and volume fraction of coacervate at equilibrium (Фc). For each parameter, whose values are determined by a design of experiments, these results are subjected to empirical smoothing in three dimensionsusing response surface methodology (RSM). The aim of this study is to find out the best compromise between E % and Фc. Under optimal conditions, the extraction extent of AG-9 reaches 98 % and 96 % using TX-114 and Lutensol AO7, respectively. The effect of Na2SO4 and CTAB addition is also studied. Finally, the possibility of recycling the surfactant is proved.

Keywords: extraction; textile dye; Acid Green 9 (AG-9); nonionic surfactant; cloud point
Corresponding author: Halima Ghouas, Laboratoire de Génie Électrique et Matériaux LGEM, Ecole Superieure en Génie Electrique et Energétique d’Oran, BP 64 CH2 ACHABA Hanifi Technopôle USTO, 31000 Oran, Algeria, E-mail:

About the authors

Halima Ghouas

Halima Ghouas, Professor of chemical engineering at the Higher School of Eelectrical Engineering and Energy of Oran (ESGEEO).

Abdelkader Benderrag

Abdelkader Benderrag, Professor of chemical engineering at the University of Science and Technology of Oran (USTO).

Boumedienne Haddou

Boumedienne Haddou, Professor of chemical engineering at the University of Science and Technology of Oran (USTO).

Cristophe Gourdon

Cristophe Gourdon, Professor of Chemical Engineering at the ENSIACET (INP Toulouse).

Acknowledgments

The authors thank the Key Laboratory of Materials Physico-Chemistry U. S. T. Oran and the Chemical Engineering Laboratory of INP-ENSIACET Toulouse for the technical support.

  1. Research ethics: Not applicable.

  2. Author contributions: Halima Ghouas was a major contributor in writing the manuscript, performed the experimental part in the laboratory and contributed in analysis and discussion of the results. Abdelkader Benderrag revised the manuscript and contributed key inputs. Boumedienne Haddou was responsible for the overall control of the article’s ideas and the structure of writing. Cristophe Gourdon revised the manuscript. All authors read and approved the final manuscript.

  3. Competing interests: The authors state no conflict of interest.

  4. Research funding: None declared.

  5. Data availability: Not applicable.

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Received: 2023-08-31
Accepted: 2023-10-09
Published Online: 2024-01-08
Published in Print: 2024-01-29

© 2023 Walter de Gruyter GmbH, Berlin/Boston

Artikel in diesem Heft

  1. Frontmatter
  2. Bis-Quaternary Ammonium Salts
  3. A novel approach to mixed micelles formation: study the interactions between bis-quaternary ammonium salts and nonionic surfactant Triton X-100
  4. Applications
  5. Brevity is the soul of wit – how time, temperature and detergent choice impact the cleaning performance in domestic dishwashers
  6. The preparation of a novel modified chitosan: application to the removal of lead and cephalexin
  7. Removal of acid dye from wastewater by cloud point extraction and regeneration of surfactant by pH regulation
  8. Effect of glauconite and SLS surfactant on phosphate and calcite rheology
  9. Physical Chemistry
  10. Iterative evaluation of micellar and thermodynamic properties of 12-2-12 in 1 % BSA aqueous solution in the presence of organic solvents and temperature
  11. Novel Surfactants
  12. Corrosion inhibition of pure iron by Eurohypnum leptothallum extract in 0.5 mol L−1 H2SO4: an experimental and GC-MS based study
  13. Study on rheology of a novel UV-light sensitive trimeric anionic–cationic surfactant/trans-o-methoxycinnamic acid micellar system
  14. Biosurfactants
  15. An overview on trehalolipids: a promising eco-friendly bio-surfactant
  16. A mini review on synthetic and biosurfactants: origin and structure, physicochemical properties, applications, cost of production, toxicity, biodegradability and environmental effects
https://doi.org/10.1515/tsd-2023-2557
Schlagwörter für diesen Artikel
extraction; textile dye; Acid Green 9 (AG-9); nonionic surfactant; cloud point

Artikel in diesem Heft

  1. Frontmatter
  2. Bis-Quaternary Ammonium Salts
  3. A novel approach to mixed micelles formation: study the interactions between bis-quaternary ammonium salts and nonionic surfactant Triton X-100
  4. Applications
  5. Brevity is the soul of wit – how time, temperature and detergent choice impact the cleaning performance in domestic dishwashers
  6. The preparation of a novel modified chitosan: application to the removal of lead and cephalexin
  7. Removal of acid dye from wastewater by cloud point extraction and regeneration of surfactant by pH regulation
  8. Effect of glauconite and SLS surfactant on phosphate and calcite rheology
  9. Physical Chemistry
  10. Iterative evaluation of micellar and thermodynamic properties of 12-2-12 in 1 % BSA aqueous solution in the presence of organic solvents and temperature
  11. Novel Surfactants
  12. Corrosion inhibition of pure iron by Eurohypnum leptothallum extract in 0.5 mol L−1 H2SO4: an experimental and GC-MS based study
  13. Study on rheology of a novel UV-light sensitive trimeric anionic–cationic surfactant/trans-o-methoxycinnamic acid micellar system
  14. Biosurfactants
  15. An overview on trehalolipids: a promising eco-friendly bio-surfactant
  16. A mini review on synthetic and biosurfactants: origin and structure, physicochemical properties, applications, cost of production, toxicity, biodegradability and environmental effects
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