Bicyclic and tricyclic phosphanes with p-block substituents

Jonas Bresien; Kirill Faust; Axel Schulz

doi:10.1515/revic-2020-0028

Artikel

Bicyclic and tricyclic phosphanes with p-block substituents

Jonas Bresien , Kirill Faust und Axel Schulz

Veröffentlicht/Copyright: 27. April 2021

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Aus der Zeitschrift Reviews in Inorganic Chemistry Band 42 Heft 1

Abstract

This review summarises the experimental and structural knowledge on polycyclic phosphanes, with a focus on bicyclic and tricyclic phosphanes, as they have not only been the most studied in the last 25 years, but also show the greatest diversity in terms of constitutional isomerism and structural motifs. Moreover, only polycyclic phosphanes that have p-block substituents at all free valences are discussed.

Keywords: oligophosphane; phosphane; phosphine; polycyclic phosphine

Corresponding author: Axel Schulz, Anorganische Chemie, Institut für Chemie, Universität Rostock, A.-Einstein-Str. 3a, 18059 Rostock, Germany; and Materialdesign, Leibniz-Institut für Katalyse an der Universität Rostock, A.-Einstein-Str. 29a, 18059 Rostock, Germany, E-mail: axel.schulz@uni-rostock.de

Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.
Research funding: None declared.
Conflict of interest statement: The authors declare no conflicts of interest regarding this article.

Appendix

Overview of tricyclic heptaphosphanes P₇R₃

Table 2:

Overview of tricyclic heptaphosphanes with the sum composition P₇R₃ and R being monodentate p-block substituents. The references include such in which the respective derivative was prepared, used as starting material or alternatively investigated.

#	Substituents	References
64	R¹=R²=R³=Me	(Baudler and Pontzen, 1983; Baudler et al., 1980; Charles et al., 1995; Fritz and Härer, 1983; Fritz et al., 1983b, 1992; Hölderich and Fritz, 1979; Noblet et al., 2011a; Patel et al., 2013)
	R¹=R²=R³=Et	(Fritz and Schneider, 1990; Fritz et al., 1990, 1992)
	R¹=R²=R³=ⁱPr	(Baudler et al., 1983a; Fritz and Schneider, 1990; Fritz et al., 1983a; Milyukov et al., 2007)
	R¹=R²=R³=ⁿBu	(Charles et al., 1995; Fritz and Schneider, 1990; Milyukov et al., 2007)
	R¹=R²=R³=ⁱBu	(Fritz and Schneider, 1990; Fritz et al., 1992; Milyukov et al., 2007)
	R¹=R²=R³=C(H)Et₂	Milyukov et al. (2007)
	R¹=R²=R³=ⁿHex	Milyukov et al. (2007)
	R¹=R²=R³=Ph	(Hölderich and Fritz, 1979; Patel et al., 2013)
	R¹=R²=R³=SiH₃	(Fritz and Schneider, 1990; Fritz et al., 1983a; Noblet et al., 2011a)
	R¹=R²=R³=SiH₂Me	Fritz and Schneider (1990)
63	R¹=R²=R³=SiMe₃	(Ahlrichs et al., 1996; Baudler et al., 1979; Cicač-Hudi et al., 2016; Cummins et al., 2014; Feierabend and von Hänisch, 2014; Fritz and Hanke, 1986; Fritz and Härer, 1983; Fritz and Hölderich, 1975a; Fritz et al., 1982, 1983a, 1983b, 1987, 1992; Hölderich and Fritz, 1979; Hönle and von Schnering, 1978; Huang and Diaconescu, 2012; Mujica et al., 1986; Noblet et al., 2011a; Patel et al., 2013; Peruzzini and Stoppioni, 1985; Schmidbaur and Bauer, 1995; Tondreau et al., 2014)
	R¹=R²=R³=Si^tBu₃	(Karaghiosoff et al., 2002; Kovács et al., 1993; Wiberg et al., 1998a, 2005)
	R¹=R²=R³=SiPh₃	(Fritz et al., 1983a; Mujica et al., 1986)
	R¹=R²=R³=Si₆Me₁₁	Noblet et al. (2011b)
	R¹=R²=R³= SiMe(SiMe₃)₂	Noblet et al. (2011b)
	R¹=R²=R³=SiMe₂(PEt₂)	Fritz and Schneider (1990)
	R¹=R²=R³=Si(SiMe₃)₂Ph	Noblet et al. (2011b)
	R¹=R²=R³=Si(SiMe₃)₃	(Cappello et al., 2006; Noblet et al., 2011b; Siegl et al., 1999)
	R¹=R²=R³=GeMe₃	Fritz et al. (1983a)
	R¹=R²=R³=GePh₃	Mujica et al. (1986)
	R¹=R²=R³=SnMe₃	(Abicht et al., 1984; Fritz et al., 1983a)
	R¹=R²=R³=SnPh₃	(Cummins et al., 2014; Mujica et al., 1986)
	R¹=R²=R³=PbMe₃	(Fritz et al., 1983a; Weber et al., 1982)
	R¹=R²=R³=P(^tBu)₂	(Fritz et al., 1991a, 1991b, 1991c)
	R¹=R²=R³=Sb(^tBu)₂	Fritz et al. (1991c)
	R¹=R²=R³=O⁻	Baudler and Floruss (1995)
	R¹=R²=R³=S⁻	Baudler and Floruss (1994)
	R¹=R²=R³=Br	Tattershall and Kendall (1994a)
	R¹=R²=R³=I	Tattershall and Kendall (1994a)
	R¹=SiMe₃, R²=R³=Me, Et, ⁱPr, ⁱBu, ^tBu	(Fritz and Härer, 1983; Fritz and Mayer, 1992; Fritz et al., 1983b, 1992; Hölderich and Fritz, 1979)
	R¹=R²=SiMe₃, R³=Me, Et, ⁱPr, ⁱBu, ^tBu	(Fritz and Härer, 1983; Fritz et al., 1983a, 1992)
	R¹=Bn, R²=R³=Me, ⁿBu	Milyukov et al. (2007)
	R¹=Me, R²=R³=ⁿBu	Milyukov et al. (2007)
	R¹=SiMe₃, R²=R³=Hyp	Noblet et al. (2011a)
66	R¹=R²=R³=[AsPh₃]⁺	Donath et al. (2014)
65		Weigand et al. (2009)
67		Noblet et al. (2011a)
		Fritz and Hölderich (1975a)

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Received: 2020-12-08

Accepted: 2021-04-09

Published Online: 2021-04-27

Published in Print: 2022-03-28

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https://doi.org/10.1515/revic-2020-0028

Schlagwörter für diesen Artikel

oligophosphane; phosphane; phosphine; polycyclic phosphine

Bicyclic and tricyclic phosphanes with p-block substituents

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Abstract

Overview of tricyclic heptaphosphanes P7R3

References

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Overview of tricyclic heptaphosphanes P₇R₃