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Bulk cure study of nanoclay filled epoxy glass fiber reinforced composite material

  • John Olusanya , Krishnan Kanny EMAIL logo and Shalini Singh
Published/Copyright: July 13, 2016
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Abstract

The correlation between cure properties and structure of nanoclay filled composite laminate has not been studied extensively. Most of the cure studies were preferably done using small samples through a calorimetric method. In this study, the effect of varying weight ratio of nanoclay (1–5 wt%) on bulk cure properties of epoxy glass fiber reinforced composite (GFRC) laminates was studied. Bulk cure of unfilled and clay filled GFRC laminates was determined using the dynamic mechanical analysis-reheat method (DMA-RM). DMA-RM cure properties gave a better coordinate method, with better cure efficiency achieved in clay filled GFRC laminates when compared to unfilled GFRC laminates. The correlation between nanoclay and DMA-RM degree of cure was coordinated with compressive and in-plane shear strength properties. The degree of cure value of 78% by DMA-RM at 1 wt% clay filled GFRC corresponds with the compressive modulus and in-plane shear strength highest values, which are 20% and 14% increase, respectively, also at 1 wt% clay filled GFRC. The structures of the unfilled and clay filled epoxy were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Clay filled epoxy up to 3 wt% showed no distinct diffraction peak, which suggested that nanoclay is randomly dispersed in the matrix.

Acknowledgments

This research project is achieved as a result of an Indian-South African project. The authors wish to gratefully acknowledge the financial support provided by the National Research Foundation of South Africa (Grant no. 76460) under DST India-NRF South Africa bilateral research agreements. We also acknowledge the research and postgraduate support of Durban University Technology for postgraduate scholarship award to JS.

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Received: 2015-3-4
Accepted: 2016-5-21
Published Online: 2016-7-13
Published in Print: 2017-3-1

©2017 Walter de Gruyter GmbH, Berlin/Boston

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