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Preparation of sulfur nanoparticles in chitosan-copper complex and investigation of its nematicidal activity against Pratylenchus pratensis in vitro

  • Duy Du Bui , Hong Nhung Nguyen , Phuoc Tho Tran , Nghiem Anh Tuan Le , Quoc Hien Nguyen and Dinh Tuan Phan EMAIL logo
Published/Copyright: May 15, 2024
Pure and Applied Chemistry
From the journal Pure and Applied Chemistry Volume 96 Issue 8

Abstract

Sulfur nanoparticles (SNPs) in chitosan-copper (CS-Cu2+) complex solution were prepared by hydrolysis of sodium thiosulfate (Na2S2O3) in an acidic medium of CS-Cu2+ complex. The size of SNPs was inversely proportional to the Cu2+/−NH2 molar ratio, decreasing from 35 to 22 nm corresponding to the Cu2+/−NH2 molar ratio increasing from 0/1 to 1/1. The SNPs/CS-Cu2+ complex was characterized by Ultraviolet-Visible spectroscopy (UV–Vis), Fourier transform infrared spectroscopy (FTIR), and X-ray diffraction (XRD) spectroscopy. The nematicidal activity against Pratylenchus pratensis in vitro was investigated by treating the CS-Cu2+ complex and SNPs/CS-Cu2+ complex with Cu2+/−NH2 molar ratio of 0.5/1. Results showed that the nematicidal activity of the SNPs/CS-Cu2+ complex was higher than that of the CS-Cu2+ complex, particularly the 50 % lethal dose (LC50) after 48 h of treatment was 77 and 89 mg/L, respectively. The results demonstrated that the prepared SNPs/CS-Cu2+ complex can be used as a nematicide for plants.

Keywords: Advanced materials for environmental protection; chitosan; chitosan-copper complex; hydrolysis; nano sulfur; nematicidal; Pratylenchus pratensis
Corresponding author: Dinh Tuan Phan, Hochiminh City University of Natural Resources and Environment, Ho Chi Minh City 700000, Vietnam, e-mail:
Article note: A collection of invited papers on the advanced materials for environmental protection.

Funding source: Vietnam Academy of Science and Technology

Award Identifier / Grant number: CSCL19.02/23-24

Acknowledgments

This research work was financially supported by the Vietnam Academy of Science and Technology (grant No: CSCL19.02/23-24).

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Published Online: 2024-05-15
Published in Print: 2024-08-27

© 2024 IUPAC & De Gruyter

Articles in the same Issue

  1. Frontmatter
  2. In this issue
  3. Preface
  4. Special issue on “Advanced materials for environmental protection and sustainability in Asean countries”
  5. Special topic papers
  6. Nanocomposite nanofibrous membranes of graphene and graphene oxide: water remediation potential
  7. Selection of graphene as a conductive additive for biomass-based activated carbon electrode in capacitive deionization: acid-treated as a practical approach to reduce graphene content
  8. Biochar-based catalysts: a potential disposal of plant biomass from phytoremediation
  9. Bio-based aerogel composites of coconut pith-derived carbon and chitosan for efficient anionic dye-polluted water treatment
  10. Study on synthesizing the complex of sorafenib with 2-hydroxypropyl-β-cyclodextrin to enhance the anticancer activity of the drug substance
  11. An antimicrobial acrylic polyurethane coating with TiO2-Ag hybrid nanoparticles
  12. Efficient synthesis of tricaproin: catalyst and reaction optimization
  13. Enhanced photocatalytic and antibacterial properties of silver–zirconia nanoparticles for environmental pollution treatment
  14. Preparation of sulfur nanoparticles in chitosan-copper complex and investigation of its nematicidal activity against Pratylenchus pratensis in vitro
  15. Fabrication of cathode electrodes based on activated carbon, reduced-graphene for hybrid capacitive deionization technology
  16. Biodegradable thermochromic polylactic acid (PLA) sensor
  17. Effect of ground tyre rubber content on self-healing properties of natural rubber composites
  18. Preparation of composite based on MXene-Ti3C2 and coconutshell-derived activated carbon for desalination of brackish water
  19. Producing an antibacterial acrylic polyurethane coating with acylated mimosa tannins
  20. Effect of multi-walled carbon nanotubes reinforcement on self-healing performance of natural rubber
  21. Mechanical properties of web kapok/fiberglass-epoxy hybrid composites for marine structures
  22. Investigation on recycling and reprocessing ability of self-healing natural rubber based on ionic crosslink network
https://doi.org/10.1515/pac-2023-1208
Keywords for this article
Advanced materials for environmental protection; chitosan; chitosan-copper complex; hydrolysis; nano sulfur; nematicidal; Pratylenchus pratensis

Articles in the same Issue

  1. Frontmatter
  2. In this issue
  3. Preface
  4. Special issue on “Advanced materials for environmental protection and sustainability in Asean countries”
  5. Special topic papers
  6. Nanocomposite nanofibrous membranes of graphene and graphene oxide: water remediation potential
  7. Selection of graphene as a conductive additive for biomass-based activated carbon electrode in capacitive deionization: acid-treated as a practical approach to reduce graphene content
  8. Biochar-based catalysts: a potential disposal of plant biomass from phytoremediation
  9. Bio-based aerogel composites of coconut pith-derived carbon and chitosan for efficient anionic dye-polluted water treatment
  10. Study on synthesizing the complex of sorafenib with 2-hydroxypropyl-β-cyclodextrin to enhance the anticancer activity of the drug substance
  11. An antimicrobial acrylic polyurethane coating with TiO2-Ag hybrid nanoparticles
  12. Efficient synthesis of tricaproin: catalyst and reaction optimization
  13. Enhanced photocatalytic and antibacterial properties of silver–zirconia nanoparticles for environmental pollution treatment
  14. Preparation of sulfur nanoparticles in chitosan-copper complex and investigation of its nematicidal activity against Pratylenchus pratensis in vitro
  15. Fabrication of cathode electrodes based on activated carbon, reduced-graphene for hybrid capacitive deionization technology
  16. Biodegradable thermochromic polylactic acid (PLA) sensor
  17. Effect of ground tyre rubber content on self-healing properties of natural rubber composites
  18. Preparation of composite based on MXene-Ti3C2 and coconutshell-derived activated carbon for desalination of brackish water
  19. Producing an antibacterial acrylic polyurethane coating with acylated mimosa tannins
  20. Effect of multi-walled carbon nanotubes reinforcement on self-healing performance of natural rubber
  21. Mechanical properties of web kapok/fiberglass-epoxy hybrid composites for marine structures
  22. Investigation on recycling and reprocessing ability of self-healing natural rubber based on ionic crosslink network
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