Startseite Impedance and modulus spectroscopy of Bi0·5Na0·5Nb0·5Fe0·5O3 ceramic
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Impedance and modulus spectroscopy of Bi0·5Na0·5Nb0·5Fe0·5O3 ceramic

  • Parbati Naik und Sunanda Kumari Patri EMAIL logo
Veröffentlicht/Copyright: 25. Februar 2025
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International Journal of Materials Research
Aus der Zeitschrift International Journal of Materials Research Band 116 Heft 3

Abstract

The solid-state reaction method was used to prepare the lead-free Bi0·5Na0·5Nb0·5Fe0·5O3 ceramic. The X-ray diffraction pattern of the prepared ceramic confirmed the formation of tetragonal crystal structure with P4mm space group. The field emission scanning electron microscopy analysis reveals densely packed grains of different shape and sizes. The average grain size was calculated to be 16.22 µm. Complex impedance spectroscopy was used to analyze the electrical response of the ceramic. The Nyquist plot shows the influence of both grain and grain boundary effects on the electrical properties of the material. The impedance analysis confirmed the non-Debye type of relaxation mechanism and negative temperature coefficient of resistance behaviour of the compound. The frequency dependent ac conductivity was found to obey Jonscher’s power law.

Keywords: X-ray diffraction; FE-SEM; EDAX; Impedance spectroscopy; Modulus spectroscopy
Corresponding author: Sunanda Kumari Patri, Department of Physics, Veer Surendra Sai University of Technology, Burla, Sambalpur-768018, Odisha, India, E-mail:

  1. Research ethics: Not applicable.

  2. Informed consent: Not applicable.

  3. Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.

  4. Use of Large Language Models, AI and Machine Learning Tools: None declared.

  5. Conflict of interest: The authors state no conflict of interest.

  6. Research funding: None declared.

  7. Data availability: Not applicable.

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Received: 2023-10-27
Accepted: 2024-10-07
Published Online: 2025-02-25
Published in Print: 2025-03-26

© 2025 Walter de Gruyter GmbH, Berlin/Boston

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https://doi.org/10.1515/ijmr-2023-0322
Schlagwörter für diesen Artikel
X-ray diffraction; FE-SEM; EDAX; Impedance spectroscopy; Modulus spectroscopy

Artikel in diesem Heft

  1. Frontmatter
  2. Review
  3. Review of functionalised clay materials for removal of bisphenol A from industrial and wastewater effluents
  4. Original Papers
  5. Unlocking treasure from fish bones: bioinspired hydroxyapatite synthesis from Catla catla fish for sustainable waste-to-wealth
  6. Green synthesized ZnO NPs from bamboo stem: optical, structural, morphological, and chemical studies
  7. Impedance and modulus spectroscopy of Bi0·5Na0·5Nb0·5Fe0·5O3 ceramic
  8. A novel Al-based self-lubricating hybrid composite composed of 2D-WS2, SiC, and Al2O3 for tribological applications
  9. Metallurgical and mechanical characterization of nitrided low-alloy steels
  10. Short Communication
  11. One-step spark plasma sintering infiltration of B4C/Al functionally graded materials
  12. News
  13. DGM – Deutsche Gesellschaft für Materialkunde
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