Abstract
The effects of baffling of an agitated vessel on the production of floating particles suspension are presented in this paper. Critical agitator speed, needed for particles dispersion in a liquid agitated in a vessel of the inner diameter of 0.295 m, was determined. The just drawdown agitator speeds were defined analogously to the Zwietering criterion. Specific agitation energy was calculated from the power consumption experimental data obtained by means of the strain gauge method. The experiments were carried out for twelve configurations of the baffles differing in number, length and their arrangement in the vessels. The following high-speed impellers were used: up- and downpumping six blade pitched blade turbines, Rushton turbine, and propeller. The impeller was located in the vessel in the height equal to two-thirds or one-third of the vessel diameter from the bottom of the vessel. The results were described in the form of a dimensionless equation.
[1] Bakker, A., & Frijlink, J. J. (1989). The drawn down and dispersion of floating solids in aerated and unaerated vessel. Chemical Engineering Research & Design, 67, 208–210. Search in Google Scholar
[2] Bao, Y., Hao, Z., Gao, Z., Shi, L., & Smith, J. M. (2005). Suspension of buoyant particles in a three phase stirred tank. Chemical Engineering Science, 60, 2283–2292. DOI: 10.1016j.ces.2004.10040. http://dx.doi.org/10.1016/j.ces.2004.10.04010.1016/j.ces.2004.10.040Search in Google Scholar
[3] Edwards, M. F., & Ellis, D. I. (1984). The drawn down of floating solids into mechanically agitated vessel. Fluid Mixing II, Institution of Chemical Engineers, Symposium Series, 89, 1–13. Search in Google Scholar
[4] Etchells, A. W. (2001). Mixing of floating solids. Plenary Lecture. In Proceedings of the 4th International Symposium on Mixing in Industrial Processes ISMIP 4, 14–16 May 2001. Toulouse, France. Search in Google Scholar
[5] Hemrajani, R. R., Smith, D. L., Koros, R. M., & Tarmy, B. L. (1988). Suspending of floating solids in stirred tank: Mixing design, scale — up and optimisation. In Proceedings of the 6th European Conference on Mixing, 24–26 May 1988 (pp. 259–265). Pavia, Italy. Search in Google Scholar
[6] Joosten, G. E. H., Smith, J. G. M., & Broere, A. M. (1977). The suspension of floating solids in stirred vessel. Transactions of the Institution of Chemical Engineers, 55, 220–222. Search in Google Scholar
[7] Kamieński, J. (2004). Agitation of multi-phase systems. Warsaw: WNT. (in Polish) Search in Google Scholar
[8] Karcz, J., & Mackiewicz, B. (2006)a. Suspending of floating solids in an agitated vessel. Inżynieria Chemiczna i Procesowa, 27, 1517–1533. Search in Google Scholar
[9] Karcz, J., & Mackiewicz, B. (2006)b. Experimental analysis of the suspending of floating solids in an agitated vessel. In Proceedings of the 17th International Congress of Chemical and Process Engineering CHISA, 27–31 August 2006 (P1.71). Prague, Czech Republic. Search in Google Scholar
[10] Karcz, J., & Mackiewicz, B. (2006)c. An effect of the presence of the gas phase on the draw down of floating solids in an agitated vessel. In Proceedings of the 10th International Conference on Multiphase Flow in Industrial Plant, 20–22 September 2006 (pp. 151–159). Tropea, Italy. Search in Google Scholar
[11] Karcz, J., & Mackiewicz, B. (2007). An effect of particles wettability on the draw down of floating solids in a baffled agitated vessel equipped with a high-speed impeller. Inżynieria Chemiczna i Procesowa, 28, 661–672. Search in Google Scholar
[12] Ozcan-Taskin, G. (2006). Effect of scale on the draw down of floating solids. Chemical Engineering Science, 60, 2871–2879. DOI: 10.1016/j.ces.2005.10.061. http://dx.doi.org/10.1016/j.ces.2005.10.06110.1016/j.ces.2005.10.061Search in Google Scholar
[13] Ozcan-Taskin, G., & Wei, H. (2003). The effect of impellerto-tank diameter ratio on draw down of solids. Chemical Engineering Science, 58, 2011–2022. DOI: 10.1016/S0009-2509(03)00024-1. http://dx.doi.org/10.1016/S0009-2509(03)00024-110.1016/S0009-2509(03)00024-1Search in Google Scholar
[14] Takahashi, K., & Sasaki, S. J. (1999). Complete drawn down and dispersion of floating solids in agitated vessel equipped with ordinary impellers. Journal of Chemical Engineering of Japan, 32(1), 40–44. DOI: 10.1252/jcej.32.40. http://dx.doi.org/10.1252/jcej.32.4010.1252/jcej.32.40Search in Google Scholar
[15] Wesołowski, P., & Szaferski, W. (2002). Wpływ geometrii granulatów tworzyw sztucznych na wytwarzanie modelowych “zawiesin lekkich”. Inżynieria i Aparatura Chemiczna, 41(4s), 145–146. Search in Google Scholar
[16] Xu, S. A., Feng, L. F., Gu, X. P., Wang, K., & Hu, G. H. (2000). Gas-liquid floating particle mixing in an agitated vessel. Chemical Engineering & Technology, 23, 103–113. DOI: 10.1002/(SICI)1521-4125(200002)23:2. http://dx.doi.org/10.1002/(SICI)1521-4125(200002)23:2<103::AID-CEAT103>3.0.CO;2-B10.1002/(SICI)1521-4125(200002)23:2<103::AID-CEAT103>3.0.CO;2-BSearch in Google Scholar
[17] Xu, S. A., Ren, W. Z., & Zhao, X. M. (2001). Critical rotational speed for a flaming particle suspension in an aerated vessel. Chemical Engineering & Technology, 24, 189–194. DOI: 10.1002/1521-4125(200102)24:2. http://dx.doi.org/10.1002/1521-4125(200102)24:2<189::AID-CEAT189>3.0.CO;2-P10.1002/1521-4125(200102)24:2<189::AID-CEAT189>3.0.CO;2-PSearch in Google Scholar
[18] Zwietering, T. N. (1958). Suspending of solids particles in liquid by agitation. Chemical Engineering Science, 8, 244–253. DOI: 10.1016/0009-2509(58)85031-9. http://dx.doi.org/10.1016/0009-2509(58)85031-910.1016/0009-2509(58)85031-9Search in Google Scholar
© 2008 Institute of Chemistry, Slovak Academy of Sciences
Articles in the same Issue
- Biosynthesis of methanol from methane by Methylosinus trichosporium OB3b
- Influence of reaction medium composition on enzymatic synthesis of galactooligosaccharides and lactulose from lactose concentrates prepared from whey permeate
- Immobilization of modified penicillin G acylase on Sepabeads carriers
- Granulation of activated sludge in a laboratory upflow sludge blanket reactor
- Investigation of the effect of fluid elasticity on a cake filtration process
- Lab-scale testing of a low-loaded activated sludge process with membrane filtration
- Calcium sulphate scaling in membrane distillation process
- Characterization and filtration performance of coating-modified polymeric membranes used in membrane bioreactors
- Informational analysis of the grinding process of granular material using a multi-ribbon blender
- Effects of vessel baffling on the drawdown of floating solids
- N2O catalytic decomposition — effect of pelleting pressure on activity of Co-Mn-Al mixed oxide catalysts
- Intelligent control of a pH process
- Influence of suspended solid particles on gas-liquid mass transfer coefficient in a system stirred by double impellers
- A three-phase nonequilibrium model for catalytic distillation
- Membrane processes used for separation of effluents from wire productions
- A simple and efficient synthesis of 3-substituted derivatives of pentane-2,4-dione
- Formation of hydrated titanium dioxide from seeded titanyl sulphate solution
- Pyrolytic and catalytic conversion of rape oil into aromatic and aliphatic fractions in a fixed bed reactor on Al2O3 and Al2O3/B2O3 catalysts
- Oxidation of thiophene over copper-manganese mixed oxides
- Study of partitioning and dynamics of metals in contaminated soil using modified four-step BCR sequential extraction procedure
- Preparation and properties of a new composite photocatalyst based on nanosized titanium dioxide
Articles in the same Issue
- Biosynthesis of methanol from methane by Methylosinus trichosporium OB3b
- Influence of reaction medium composition on enzymatic synthesis of galactooligosaccharides and lactulose from lactose concentrates prepared from whey permeate
- Immobilization of modified penicillin G acylase on Sepabeads carriers
- Granulation of activated sludge in a laboratory upflow sludge blanket reactor
- Investigation of the effect of fluid elasticity on a cake filtration process
- Lab-scale testing of a low-loaded activated sludge process with membrane filtration
- Calcium sulphate scaling in membrane distillation process
- Characterization and filtration performance of coating-modified polymeric membranes used in membrane bioreactors
- Informational analysis of the grinding process of granular material using a multi-ribbon blender
- Effects of vessel baffling on the drawdown of floating solids
- N2O catalytic decomposition — effect of pelleting pressure on activity of Co-Mn-Al mixed oxide catalysts
- Intelligent control of a pH process
- Influence of suspended solid particles on gas-liquid mass transfer coefficient in a system stirred by double impellers
- A three-phase nonequilibrium model for catalytic distillation
- Membrane processes used for separation of effluents from wire productions
- A simple and efficient synthesis of 3-substituted derivatives of pentane-2,4-dione
- Formation of hydrated titanium dioxide from seeded titanyl sulphate solution
- Pyrolytic and catalytic conversion of rape oil into aromatic and aliphatic fractions in a fixed bed reactor on Al2O3 and Al2O3/B2O3 catalysts
- Oxidation of thiophene over copper-manganese mixed oxides
- Study of partitioning and dynamics of metals in contaminated soil using modified four-step BCR sequential extraction procedure
- Preparation and properties of a new composite photocatalyst based on nanosized titanium dioxide