Band 45, Heft 12

Porosity in starch consolidation casting technique is rightly related to original size and morphology of starch granules, leaving a pore structure after burning out. This work reports the results for the addition of different native potato and corn starch proportions in suspensions with TiO2 (rutile) powder. Gelling temperature have been defined after observation under light microscopy using a heating stage. Analysis of porous network and isolated pores have been done from images of samples surfaces obtained by depth from focus reconstruction, revealing a qualitative correlation of pores characteristics and starches additions in suspensions, suggesting that the presence of isolated or interconnected pores can be handled by starches selection to control the amylopectin and amylose contents in slurries. Also, the analysis of porous fraction distribution shows no consistent pattern through specimens’ volume according to starches in mixtures.

In this study, thick and hard alumina coatings were produced on 6061-T6 Al alloy substrates for different oxidation times and current densities by using of microarc oxidation (MAO) technique in an alkali-silicate electrolytic solution. The influence of oxidation time and current density on the kinetics, phase composition, hardness, surface roughness and structure of the coating were investigated. It is found that the kinetics of coating mainly depends on applied current density and oxidation time. The XRD results revealed that the coatings are composed of mainly α-Al 2 O 3 , γ-Al 2 O 3 and mullite phase. The relative ratio of harder and denser α-Al 2 O 3 phase increases with increasing current density and oxidation time. For the same coating time, the position of maximum hardness of coatings moves away from the substrate-coating interface to the coating surface with increasing current density. The surface roughness of coating is a function of coating thickness and increases with increasing deposition time and current density. The surface micro hardness of Al 6061-T6 alloy substrate was increased up to 2200 HV hardness after the coating.

In dual phase steels, the microstructure consists of a ferrite matrix and martensite islands along the grain boundaries of the ferrite. In this study, the microstructures of dual phase steels with different chemical compositions are characterized by applying different etchants and by using optical and electron microscopy. The most successful result was obtained with LePera and Na-metabisulfite etchants, which were applied using a special method.