Zeitschrift für Kristallographie - New Crystal Structures

Heft Open Access

Band 219, Heft 2

Februar 2014

Veröffentlicht von

Veröffentlichen auch Sie bei De Gruyter Brill

Manuskript einreichen Informationen für Autor*innen

Heft der Zeitschrift

Zeitschrift für Kristallographie - New Crystal Structures

Inhalt

Open Access
Crystal structure of samarium nickel tetraaluminide, SmNiAl₄

11. Februar 2014

M. L. Fornasini, R. Raggio, G. Borzone

Seiten: 75-76

PDF downloaden

Al 4 NiSm, orthorhombic, Cmcm (no. 63), a = 4.0948(6) Å, b = 15.582(3) Å, c = 6.610(1) Å, V = 421.8 Å 3 , Z = 4, R gt (F) = 0.028, wR obs (F 2 ) = 0.074, T = 293 K.
Open Access
Crystal structure of samarium nickel aluminide, Sm₄Ni₆Al₂₃

11. Februar 2014

M. L. Fornasini, R. Raggio, G. Borzone

Seiten: 77-78

PDF downloaden

Al 23 Ni 6 Sm 4 , monoclinic, C 12/ m 1 (no. 12), a = 15.939(3) Å, b = 4.0967(6) Å, c = 18.320(3) Å, β = 113.09(2)°, V = 1100.4 Å 3 , Z = 2, R gt (F) = 0.017, wR obs (F 2 ) = 0.040, T = 293 K.
Open Access
Crystal structure of dieuropium lithium trigermanide, Eu₂LiGe₃

11. Februar 2014

Q.-X. Xie, R. Nesper

Seiten: 79-80

PDF downloaden

Eu 2 Ge 3 Li, orthorhombic, Pnnm (no. 58), a = 10.968(2) Å, b = 11.687(2) Å, c = 4.5482(7) Å, V = 583.0 Å 3 , Z = 4, R gt (F) = 0.023, wR ref (F 2 ) = 0.048, T = 293 K.
Open Access
Crystal structure of ytterbium lithium digermanide, YbLiGe₂

11. Februar 2014

Q.-X. Xie, R. Nesper

Seiten: 81-82

PDF downloaden

Ge 2 LiYb, orthorhombic, Pnma (no. 62), a = 7.939(2) Å, b = 3.882(1) Å, c = 10.524(3) Å, V = 324.4 Å 3 , Z = 4, R gt (F) = 0.030, wR ref (F 2 ) = 0.064, T = 293 K.
Open Access
Crystal structure of dieuropium and distrontium di(lithium, magnesium) trigermanide, M₂Li_xMg_2–xGe₃ (M= Eu, x = 1.16;M= Sr, x = 0.94)

11. Februar 2014

Q.-X. Xie, R. Nesper

Seiten: 83-84

PDF downloaden

Eu 2 Ge 3 Li 1 . 16 Mg 0.84 , orthorhombic, Cmcm (no. 63), a = 4.577(1) Å, b = 19.534(4) Å, c = 7.223(2) Å, V = 645.7 Å 3 , Z = 4, R gt (F) = 0.030, wR ref (F 2 ) = 0.072, T = 293 K. Ge3Li0.94Mg1.06Sr2, orthorhombic, Cmcm (no. 63), a = 4.6357(3) Å, b = 19.703(1) Å, c = 7.3239(5) Å, V = 669.0 Å 3 , Z = 4, R gt (F) = 0.023, wR ref (F 2 ) = 0.047, T = 293 K.
Open Access
Crystal structure of calcium zinc silicide, CaZn_xSi_2–x (x = 0.80), and strontium germanium silicide, SrGe_xSi_2–x (x = 1.20)

11. Februar 2014

Q.-X. Xie, R. Nesper

Seiten: 85-86

PDF downloaden

CaSi 1.20 Zn 0.80 , hexagonal, P 6/ mmm (no. 191), a = 4.1423(3) Å, c = 4.3176(4) Å, V = 64.2 Å 3 , Z = 1, R gt (F) = 0.018, wR ref (F 2 ) = 0.042, T = 293 K. Ge 1.20 Si 0.80 Sr, hexagonal, P 6/ mmm (no. 191), a = 4.360(1) Å, c = 4.537(2) Å, V = 74.7 Å 3 , Z = 1, R gt (F) = 0.038, wR ref (F 2 ) = 0.085, T = 293 K.
Open Access
Crystal structure of pentalanthanum trilead monoiodide, La₅Pb₃I

11. Februar 2014

Hj. Mattausch, A. Simon, C. Zheng

Seiten: 87-88

PDF downloaden

ILa 5 Pb 3 , hexagonal, P 63/ mcm (no. 193), a = 9.736(1) Å, c = 6.947(1) Å, V = 570.3 Å 3 , Z = 2, R gt (F) = 0.029, wR ref (F 2 ) = 0.068, T = 293 K.
Open Access
Refinement of the crystal structure of diniobium trisoxydisulfate hydrate, Nb₂O₃(SO₄)₂ · 0.25H₂O

11. Februar 2014

B. Ewald, Yu. Prots, M. Boström

Seiten: 89-90

PDF downloaden

H 0.5 Nb 2 O 11.25 S 2 , trigonal, R 3̅ (no. 148), a = 10.378(2) Å, c = 26.540(5) Å, V = 2475.7 Å 3 , Z = 24, R gt (F) = 0.031, wR ref (F 2 ) = 0.072, T = 295 K.
Open Access
Crystal structure of pentabismuth heptaoxide nitrate, Bi₅O₇NO₃

11. Februar 2014

P. Ziegler, M. Ströbele, H.-J. Meyer

Seiten: 91-92

PDF downloaden

Bi 5 NO 10 , monoclinic, P 12 1 / c 1 (no. 14), a = 8.5846(6) Å, b = 23.385(2) Å, c = 5.5422(4) Å, β = 108.103(8)°, V = 1057.5 Å 3 , Z = 4, R gt (F) = 0.029, wR ref (F 2 ) = 0.074, T = 210 K.
Open Access
Crystal structure of dirubidium aquapentachlorochromate(III), Rb₂[CrCl₅(H₂O)]

11. Februar 2014

J.-X. Mi, X. Zhou, H. Zhang, S.-Y. Mao, J.-T. Zhao

Seiten: 93-94

PDF downloaden

Cl 5 CrH 2 ORb 2 , orthorhombic, Pnma (no. 62), a = 13.8123(5) Å, b = 9.7705(4) Å, c = 7.1522(4) Å, V = 965.2 Å 3 , Z = 4, R gt (F) = 0.038, wR ref (F 2 ) = 0.073, T = 295 K.
Open Access
Crystal structure of dicesium aquapentachlorochromate(III), Cs₂[CrCl₅(H₂O)]

11. Februar 2014

J.-X. Mi, X. Zhou, H. Zhang, S.-Y. Mao, J.-T. Zhao

Seiten: 95-96

PDF downloaden

Cl 5 CrCs 2 H 2 O, orthorhombic, Cmcm (no. 63), a = 7.4297(6) Å, b = 17.234(1) Å, c = 8.0121(6) Å, V = 1025.9 Å 3 , Z = 4, R gt (F) = 0.041, wR ref (F 2 ) = 0.082, T = 295 K.
Open Access
Crystal structure of dithallium(I) octa-μ3-bromohexabromo-octahedrohexamolybdate, Tl₂[(Mo₆Br₈)Br₆]

11. Februar 2014

W. Xu, Y.-Q. Zheng, P. Wang

Seiten: 97-98

PDF downloaden

Br 14 Mo 6 Tl 2 , cubic, Pn 3̅ (no. 201), a = 13.813(1) Å, V = 2635.4 Å 3 , Z = 4, R gt (F) = 0.080, wR ref (F 2 ) = 0.147, T = 295 K.
Open Access
Crystal structure of tetraaquatrissuccinatodierbium hexahydrate, Er₂(H₂O)₄(C₄H₄O₄)₃ · 6H₂O

11. Februar 2014

J. Sun, Y.-Q. Zheng, J.-L. Lin

Seiten: 99-100

PDF downloaden

C 12 H 32 Er 2 O 22 , triclinic, P 1̅ (no. 2), a = 6.517(1) Å, b = 9.774(1) Å, c = 10.466(1) Å, α = 80.19(1)°, β = 89.84(1)°, γ = 71.37(1)°, V = 621.5 Å 3 , Z = 1, R gt (F) = 0.031, wR ref (F 2 ) = 0.080, T = 293 K.
Open Access
Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C₆H₅)₄]₂[VOCl₄] · 4CH₃CN, [P(C₆H₅)₄]₂[MCl₆] · 4CH₃CN (M = Sn, Mo)

11. Februar 2014

Susanne Rabe, Wilfried Bubenheim, Ulrich Müller

Seiten: 101-105

PDF downloaden

C 56 H 52 Cl 4 N 4 OP 2 V, monoclinic, P 12 1 / c 1 (no. 14), a = 9.473(2) Å, b = 19.832(6) Å, c = 14.461(2) Å, β = 99.00(2)°, V = 2683.3 Å 3 , Z = 2, R gt (F) = 0.035, wR ref (F 2 ) = 0.096, T = 193 K. C 56 H 52 Cl 6 N 4 P 2 Sn, monoclinic, P 12 1 / c 1 (no. 14), a = 9.606(7) Å, b = 19.842(9) Å, c = 15.129(9) Å, β = 98.91(2)°, V = 2848.8 Å 3 , Z = 2, R gt (F) = 0.038, wR ref (F 2 ) = 0.089, T = 300 K. C 56 H 52 Cl 6 MoN 4 P 2 , monoclinic, P 12 1 / c 1 (no. 14), a = 9.505(3) Å, b = 19.624(2) Å, c = 14.759(2) Å, β = 98.72(2)°, V = 2721.1 Å 3 , Z = 2, R gt (F) = 0.062, wR ref (F 2 ) = 0.175, T = 193 K.
Open Access
Crystal structure of aquabis(4-methyl-5-formyl-imidazolfuranoylhydrazone)- (trinitrato)praseodymium(III) monohydrate, Pr(H₂O)(C₉H₁₀O₂N₄)₂(NO₃)₃·H₂O

11. Februar 2014

P. M. Haba, M. Gaye, A. S. Sall, A. H. Barry, T. Jouini

Seiten: 106-108

PDF downloaden

C 20 H 24 N 11 O 15 Pr, monoclinic, P 12 1 / c 1 (no. 14), a = 18.956(4) Å, b = 8.161(2) Å, c = 22.151(3) Å, β = 114.53(2)°, V = 3117.5 Å 3 , Z = 4, R gt (F) = 0.025, wR ref (F 2 ) = 0.063, T = 293 K.
Open Access
Crystal structure of tin(II) acetate acetylacetonate, Sn(C₅H₇O₂)(C₂H₃O₂)

11. Februar 2014

H. Reuter

Seiten: 109-110

PDF downloaden

C 7 H 10 O 4 Sn, monoclinic, C 12/ c 1 (no. 15), a = 12.459(3) Å, b = 9.676(2) Å, c = 16.237(3) Å, β = 99.55(2)°, V = 1930.3 Å 3 , Z = 8, R gt (F) = 0.032, wR ref (F 2 ) = 0.084, T = 293 K.
Open Access
Crystal structure of (–)-hardwickiic acid, C₁₉H₂₇OCOOH

11. Februar 2014

C. Chaichantipyuth, N. Muangsin, N. Chaichit, S. Roengsumran, A. Petsom, T. Watanabe, T. Ishikawa

Seiten: 111-113

PDF downloaden

C 20 H 28 O 3 , monoclinic, P 2 1 (no. 4), a = 10.0279(2) Å, b = 11.1076(3) Å, c = 17.0856(4) Å, β = 105.522(1)°, V = 1833.7 Å 3 , Z = 4, R gt (F) = 0.058, wR ref (F 2 ) = 0.159, T = 293 K.
Open Access
Crystal structure of 3-diphenylamino-benzo[de]anthracen-7-one, C₂₉H₁₉NO

11. Februar 2014

M.-X. Yu

Seiten: 114-116

PDF downloaden

C 29 H 19 NO, monoclinic, P 12 1 / c 1 (no. 14), a = 23.218(4) Å, b = 14.748(2) Å, c = 12.094(2) Å, β = 90.986(4)°, V = 4140.6 Å 3 , Z = 8, R gt (F) = 0.045, wR ref (F 2 ) = 0.085, T = 293 K.
Open Access
Crystal structure of (1,4-cyclohexanedicarboxylato)(2,2′-bipyridine)- copper(II) monohydrate, Cu(C₈H₁₀O₄)(C₁₀H₈N₂) · H₂O

11. Februar 2014

A.-Q. Ma, M.-X. Yu, L.-G. Zhu

Seiten: 117-118

PDF downloaden

C 18 H 20 CuN 2 O 5 , monoclinic, P 12 1 / c 1 (no. 14), a = 9.1432(4) Å, b = 17.8251(8) Å, c = 10.1994(5) Å, β = 99.226(2)°, V = 1640.8 Å 3 , Z = 4, R gt (F) = 0.030, wR ref (F 2 ) = 0.080, T = 293 K.
Open Access
Crystal structure of 1,2,6,7,11,12-hexathia-cyclopentadecane, C₉H₁₈S₆

11. Februar 2014

Y.-Q. Sun, J. Sun, Y.-W. Guo

Seiten: 119-120

PDF downloaden

C 9 H 18 S 6 , triclinic, P 1̅ (no. 2), a = 5.637(1) Å, b = 14.748(4) Å, c = 17.913(4) Å, α= 86.663(5)°, β = 82.988(4)°, γ = 83.742(4)°, V = 1467.7 Å 3 , Z = 4, R gt (F) = 0.072, wR ref (F 2 ) = 0.166, T = 293 K.
Open Access
Crystal structure of 1,2,6,7,11,12-hexathia-cyclopentadecane-4,9,14-triol, C₉H₁₈O₃S₆

11. Februar 2014

Y.-Q. Sun, G. Zahn, Y.-W Guo

Seiten: 121-123

PDF downloaden

C 9 H 18 O 3 S 6 , orthorhombic, Pbca (no. 61), a = 17.419(2) Å, b = 10.6391(9) Å, c = 17.445(2) Å, V = 3232.9 Å 3 , Z = 8, R gt (F) = 0.079, wR ref (F 2 ) = 0.252, T = 293 K.
Open Access
Crystal structure of N,N′,N′′-tris(2-pyridinyl)phosphoric triamide, (NC₅H₄NH)₃PO

11. Februar 2014

K. Gholivand, M. D. Alavi, M. Pourayoubi

Seiten: 124-126

PDF downloaden

C 15 H 15 N 6 OP, monoclinic, P 12 1 / n 1 (no. 14), a = 10.558(2) Å, b = 13.448(2) Å, c = 21.814(4) Å, β = 92.314(4)°, V = 3094.6 Å 3 , Z = 8, R gt (F) = 0.051, wR ref (F 2 ) = 0.101, T = 120 K.
Open Access
Crystal structure of [9,22-(bisbutyloxy)hemiporphyrazinato]nickel(II), C₃₄H₃₀N₈O₂Ni

11. Februar 2014

K. Haberroth, M. Hanack, C. Maichle-Mössmer

Seiten: 127-128

PDF downloaden

C 34 H 30 N 8 NiO 2 , monoclinic, P 12 1 / n 1 (no. 14), a = 14.048(4) Å, b = 4.7256(1) Å, c = 21.491(6) Å, β = 99.10(1)°, V = 1408.7 Å 3 , Z = 2, R gt (F) = 0.054, wR ref (F) = 0.059, T = 293 K.
Open Access
Crystal structure of 5,10,15,20-tetrakis(5′-methylthien-2′-yl)porphyrin, C₄₀H₃₀N₄S₄

11. Februar 2014

M. Bellizzi, P. C. D. Foss, R. Pelto, G. Crundwell, C. Brückner, J. B. Updegraff, M. Zeller, A. D. Hunter

Seiten: 129-131

PDF downloaden

C 40 H 30 N 4 S 4 , triclinic, P 1̅ (no. 2), a = 6.5126(7) Å, b = 10.499(1) Å, c = 12.635(1) Å, α = 87.818(2)°, β = 79.141(2)°, γ = 86.737(2)°, V = 846.7 Å 3 , Z = 1, R gt (F) = 0.057, wR ref (F 2 ) = 0.150, T = 100 K.
Open Access
Crystal structure of (2R,2′R,5R,5′R)-1,1′-bis[1-(2-tert-butyl-1-carboxytert- butyl-3-methyl-4-oxo-imidazolidine-5-yl)-1-methyl]ferrocene, Fe(C₂₁H₃₃N₂O₃)₂

11. Februar 2014

H. Nöth, H. Dialer, T. Habereder, W. Beck

Seiten: 132-134

PDF downloaden

C 42 H 66 FeN 4 O 6 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 10.7723(9) Å, b = 11.7128(8) Å, c = 33.392(3) Å, V = 4213.2 Å 3 , Z = 4, R gt (F) = 0.071, wR ref (F 2 ) = 0.158, T = 193 K.
Open Access
Crystal structure of diaqua-bis(pyrazole)-μ2-squarato(1,3)nickel(II), Ni(C₄O₄)(C₃H₄N₂)₂(H₂O)₂

11. Februar 2014

R. Kirchmaier, E. Altin, A. Lentz

Seiten: 135-136

PDF downloaden

C 10 H 12 N 4 NiO 6 , orthorhombic, Pbca (no. 61), a = 11.890(3) Å, b = 7.909(2) Å, c = 14.664(4) Å, V = 1378.9 Å 3 , Z = 4, R gt (F) = 0.028, wR ref (F 2 ) = 0.068, T = 293 K.
Open Access
Crystal structure of diaqua-bis(pyridine-2,6-dicarboxylato-O,N,O′)-(μ2- pyrazino)dicopper(II) dihydrate, [Cu₂(C₄H₄N₂)(C₇H₃NO₄)₂(H₂O)₂] · 2H₂O

11. Februar 2014

E. Altin, R. Kirchmaier, A. Lentz

Seiten: 137-138

PDF downloaden

C 18 H 18 Cu 2 N 4 O 12 , monoclinic, P 12 1 / n 1 (no. 14), a = 5.808(1) Å, b = 15.541(3) Å, c = 11.962(3) Å, β = 92.79(3)°, V = 1078.3 Å 3 , Z = 2, R gt (F) = 0.028, wR ref (F 2 ) = 0.079, T = 293 K.
Open Access
Crystal structure of tetraaqua-bis(pyridine-2,6-dicarboxylato-O,N,O′)- (μ2-pyrazino)dinickel(II), [Ni₂(C₄H₄N₂)(C₇H₃NO₄)₂(H₂O)₄]

11. Februar 2014

E. Altin, R. Kirchmaier, A. Lentz

Seiten: 139-140

PDF downloaden

C 18 H 18 N 4 Ni 2 O 12 , monoclinic, P 12 1 / c 1 (no. 14), a = 7.558(2) Å, b = 20.004(3) Å, c = 7.135(2) Å, β = 92.02(3)°, V = 1078.1 Å 3 , Z = 2, R gt (F) = 0.023, wR ref (F 2 ) = 0.061, T = 293 K.
Open Access
Crystal structure of aqua[1,3-bis(2-pyridylimino)isoindolinato](salicylato)- copper(II), Cu(C₇O₃H₄)(C₁₈H₁₂N₅)(H₂O)

11. Februar 2014

J. Kaizer, J. Pap, G. Speier, L. Párkányi

Seiten: 141-142

PDF downloaden

C 25 H 18 CuN 5 O 4 , triclinic, P 1̅ (no. 2), a = 7.300(1) Å, b = 11.985(1) Å, c = 13.190(1) Å, α = 88.15(1)°, β = 78.68(1)°, γ = 78.62(1)°, V = 1109.3 Å 3 , Z = 2, R gt (F) = 0.048, wR ref (F 2 ) = 0.134, T = 293 K.
Open Access
Crystal structure of [N,N-bis(2-[2-pyridyl]ethyl)-2-(2-aminoethoxy)ethanol]- copper(II) bis(trifluoromethanesulfonate), (CuC₁₈H₂₅N₃O₂)(F₃CSO₃)₂

11. Februar 2014

K. Selmeczi, G. Speier, M. Réglier, M. Giorgi

Seiten: 143-144

PDF downloaden

C 20 H 25 CuF 6 N 3 O 8 S 2 , triclinic, P 1̅ (no. 2), a = 8.0561(4) Å, b = 11.766(1) Å, c = 14.859(1) Å, α = 75.539(3)°, β = 84.980(5)°, γ = 82.435(5)°, V = 1349.8 Å 3 , Z = 2, R gt (F) = 0.068, wR ref (F 2 ) = 0.135, T = 293 K.
Open Access
Crystal structure of 2-hydroxyimino-3-oxo-3-phenyl-propionic acid ethyl ester, C₁₁H₁₁NO₄

11. Februar 2014

M. Ramos Silva, A. Matos Beja, J. A. Paixão, S. H. Lopes, Ana M. T. D. P. V. Cabral, A. M. d′A. Rocha Gonsalves, A. J. F. N. Sobral

Seiten: 145-146

PDF downloaden

C 11 H 11 NO 4 , orthorhombic, Pna 2 1 (no. 33), a = 18.370(4) Å, b = 4.870(1) Å, c = 24.616(2) Å, V = 2202.4 Å 3 , Z = 8, R gt (F) = 0.082, wR ref (F 2 ) = 0.203, T = 293 K.
Open Access
Crystal structure of bis(8-chloro-5-(4-methylpiperazinium-1-yl)pyrido- [2,3-b][1,5]benzoxazepine) fumarate – fumaric acid solvate (1:1), (C₁₇H₁₈ClN₄O)₂(C₄H₂O₄) · C₄H₄O₄

11. Februar 2014

L. Dupont, J.-F. Liégeois

Seiten: 147-149

PDF downloaden

C 42 H 42 Cl 2 N 8 O 10 , triclinic, P 1̅ (no. 2), a = 9.625(1) Å, b = 9.929(3) Å, c = 11.860(2) Å, α = 108.12(2)°, β = 73.24(1)°, γ = 87.38(1)°, V = 1019.9 Å 3 , Z = 1, R gt (F) = 0.043, wR ref (F 2 ) = 0.131, T = 293 K.
Open Access
Crystal structure of sulfatobis{2-[N-(2-hydroxyethylaminoethyl)iminomethyl] phenolatozinc(II)}, [(ZnC₁₁H₁₅N₂O₂)₂SO₄]

11. Februar 2014

X.-Y. Qiu, Q.-X. Liu, Z.-G. Wang, Y.-S. Lin, W.-J. Zeng, H.-K. Fun, H.-L. Zhu

Seiten: 150-152

PDF downloaden

C 22 H 30 N 4 O 8 SZn 2 , monoclinic, P 12 1 / c 1 (no. 14), a = 8.2666(6) Å, b = 23.229(2) Å, c = 13.7531(9) Å, β = 102.329(1)°, V = 2580.1 Å 3 , Z = 4, R gt (F) = 0.050, wR ref (F 2 ) = 0.114, T = 293 K.
Open Access
Crystal structure of 1,3-di[2-(4,5-dihydrooxazole)]benzene, C₁₂H₁₂N₂O₂

11. Februar 2014

S.-H. Chen, S.-F. Li, Y. Zou, L. Yang, B. Chen, H.-L. Zhu

Seiten: 153-154

PDF downloaden

C 12 H 12 N 2 O 2 , monoclinic, P 12 1 / c 1 (no. 14), a = 7.033(4) Å, b = 14.768(9) Å, c = 10.377(6) Å, β = 96.026(9)°, V = 1071.8 Å 3 , Z = 4, R gt (F) = 0.054, wR ref (F 2 ) = 0.181, T = 293 K.
Open Access
Crystal structure of bis[N-(2-(2-hydroxyethylamino)ethyl)salicylideneimine] cadmium(II) dihydrate, Cd(C₁₁H₁₇N₂O₂)₂ · 2H₂O

11. Februar 2014

S. Yang, Q.-X. Liu, W.-J. Zeng, Y. Zou, Z.-G. Wang, H.-L. Zhu

Seiten: 155-156

PDF downloaden

C 22 H 34 CdN 4 O 6 , monoclinic, P 12 1 / n 1 (no. 14), a = 9.236(4) Å, b = 21.102(9) Å, c = 12.987(6) Å, β = 97.638(6)°, V = 2508.7 Å 3 , Z = 4, R gt (F) = 0.039, wR ref (F 2 ) = 0.117, T = 298 K.
Open Access
Crystal structure of bis(2-aminopyrimidine)silver(I) hexafluoroarsenate bis(2-aminopyrimidine) solvate, [Ag(C₄H₅N₃)₂]AsF₆ · 2C₄H₅N₃

11. Februar 2014

H.-L. Yang, S. Yang, X.-Y. Qiu, S.-C. Shao, J.-L. Ma, L. Sun, H.-L. Zhu

Seiten: 157-158

PDF downloaden

C 16 H 20 AgAsF 6 N 12 , triclinic, P 1̅ (no. 2), a = 7.004(1) Å, b = 8.696(2) Å, c = 11.006(2) Å, α = 68.95(3)°, β = 76.49(3)°, γ = 81.90(3)°, V = 607.1 Å 3 , Z = 1, R gt (F) = 0.044, wR ref (F 2 ) = 0.111, T = 293 K.
Open Access
Crystal structure of bis(4-aminopyridine)silver(I) bis(3-nitrobenzoato)- silver(I) dihydrate, Ag(C₅H₆N₂)₂[Ag(C₇H₄NO₄)₂] · 2H₂O

11. Februar 2014

J.-L. Ma, Y. Zou, F.-J. Meng, Y.-S. Lin, Z.-G. Wang, H.-L. Zhu

Seiten: 159-160

PDF downloaden

C 24 H 24 Ag 2 N 6 O 10 , triclinic, P 1̅ (no. 2), a = 3.807(3) Å, b = 11.55(1) Å, c = 16.21(1) Å, α = 74.17(1)°, β = 84.75(1)°, γ = 89.89(1)°, V = 682.6 Å 3 , Z = 1, R gt (F) = 0.045, wR ref (F 2 ) = 0.153, T = 293 K.
Open Access
Crystal structure of bis[N,N′-bis(2-fluorobenzylidene)ethylenediamine]silver( I) 4-chlorobenzoate 4-chlorobenzoic acid, Ag(C₁₆H₁₄N₂F₂)₂(C₁₄H₉O₂Cl₂)

11. Februar 2014

J.-L. Ma, L. Yang, B. Chen, Y. Zou, F.-J. Meng, H.-L. Zhu

Seiten: 161-162

PDF downloaden

C 46 H 37 AgCl 2 F 4 N 4 O 4 , orthorhombic, Pccn (no. 56), a = 27.93(1) Å, b = 7.208(3) Å, c = 21.083(8) Å, V = 4244.0 Å 3 , Z = 4, R gt (F) = 0.035, wR ref (F 2 ) = 0.069, T = 298 K.
Open Access
Crystal structure of diaquatetra(3,5-dinitrobenzoato)tetrasilver(I), Ag₄(C₇H₃N₂O₆)₄(H₂O)₂

11. Februar 2014

J. Xia, Z.-G. Wang, L. Yang, L.-L. Tang, H.-L. Zhu

Seiten: 163-164

PDF downloaden

C 28 H 16 Ag 4 N 8 O 26 , monoclinic, P 12 1 / c 1 (no. 14), a = 5.667(1) Å, b = 16.915(3) Å, c = 19.694(4) Å, β = 90.38(3)°, V = 1887.8 Å 3 , Z = 2, R gt (F) = 0.065, wR ref (F 2 ) = 0.177, T = 293 K.
Open Access
Crystal structure of bis[di(1,10-phenanthroline)azidocopper(II)] biphenyl- 4,4′-dicarboxylate pentahydrate, [Cu(C₁₂H₈N₂)₂N₃]₂(C₁₄H₈O₄) · 5H₂O

11. Februar 2014

M.-D. Ye, Y.-Q. Cheng, X.-H. Li, M.-L. Hu

Seiten: 165-167

PDF downloaden

C 62 H 50 Cu 2 N 14 O 9 , monoclinic, P 12/ n 1 (no. 13), a = 15.7454(6) Å, b = 7.9119(3) Å, c = 22.3267(9) Å, β = 96.150(2)°, V = 2765.4 Å 3 , Z = 2, R gt (F) = 0.071, wR ref (F 2 ) = 0.144, T = 293 K.
Open Access
Crystal structure of catena-bis-μ-terephthalato[2,2′-bipyridinecobalt(II)] [aqua-2,2′-bipyridinecobalt(II)], Co₂(C₈H₄O₄)₂(C₁₀H₈N₂)₂(H₂O)

11. Februar 2014

F. Chen, M.-L. Hu, M.-D. Ye, H.-P. Xiao

Seiten: 168-170

PDF downloaden

C 36 H 26 Co 2 N 4 O 9 , monoclinic, P 12 1 / c 1 (no. 14), a = 13.8648(7) Å, b = 17.1789(9) Å, c = 14.1938(7) Å, β = 104.525(1)°, V = 3272.7 Å 3 , Z = 4, R gt (F) = 0.076, wR ref (F 2 ) = 0.151, T = 298 K.
Open Access
Crystal structure of 2,3-bis(2-cyanoethylthio)-6,7-vinylenedithiotetrathiafulvalene, C₁₄H₁₀N₂S₈

11. Februar 2014

G. Xue, W.-T. Yu, Q. Fang

Seiten: 171-172

PDF downloaden

C 14 H 10 N 2 S 8 , triclinic, P 1̅ (no. 2), a = 7.753(2) Å, b = 11.403(3) Å, c = 12.371(5) Å, α = 64.10(2)°, β = 84.62(2)°, γ = 77.34(2)°, V = 959.9 Å 3 , Z = 2, R gt (F) = 0.061, wR ref (F 2 ) = 0.168, T = 293 K.
Open Access
Crystal structure of {1-benzyl-2-[(4-nitrobenzyl)sulfanyl]-1H-imidazol-5-yl}- methanol, C₁₈H₁₇N₃O₃S

11. Februar 2014

A. Ramazani, F. Marandi, A. Souldozi, A. R. Jalilian

Seiten: 173-174

PDF downloaden

C 18 H 17 N 3 O 3 S, monoclinic, P 12 1 / c 1 (no. 14), a = 15.705(2) Å, b = 12.083(2) Å, c = 9.368(1) Å, β = 102.404(3)°, V = 1736.3 Å 3 , Z = 4, R gt (F) = 0.078, wR ref (F 2 ) = 0.226, T = 120 K.
Open Access
Crystal structure of dimethyl 1-acetyl-1,2-dihydro-2,3-quinolinedicarboxylate, C₁₅H₁₅NO₅

11. Februar 2014

A. Ramazani, L. Dolatyari, A. R. Kazemizadeh, A. Souldozi

Seiten: 175-176

PDF downloaden

C 15 H 15 NO 5 , triclinic, P 1̅ (no. 2), a = 7.366(1) Å, b = 8.884(2) Å, c = 11.242(2) Å, α = 68.640(4)°, β = 81.328(4)°, γ = 85.050(4)°, V = 676.9 Å 3 , Z = 2, R gt (F) = 0.064, wR ref (F 2 ) = 0.151, T = 120 K.
Open Access
Crystal structure of dimethyl 1,1-diacetyl-8a-hydroxy-8-oxo-1,2,8,8a-tetrahydrocyclopenta[ a]indene-2,3-dicarboxylate, C₂₀H₁₈O₈

11. Februar 2014

A. Ramazani

Seiten: 177-178

PDF downloaden

C 20 H 18 O 8 , orthorhombic, Fdd 2 (no. 43), a = 19.060(4) Å, b = 35.937(7) Å, c = 10.571(2) Å, V = 7240.6 Å 3 , Z = 16, R gt (F) = 0.056, wR ref (F 2 ) = 0.139, T = 110 K.
Open Access
Crystal structure of dimethyl (Z)-2(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)- 2-butenedioate, C₁₄H₁₁NO₆

11. Februar 2014

A. Ramazani, F. Marandi, E. Ahmadi, A. Morsali

Seiten: 179-180

PDF downloaden

C 14 H 11 NO 6 , monoclinic, P 12 1 / n 1 (no. 14), a = 8.068(2) Å, b = 9.679(2) Å, c = 16.961(3) Å, β = 101.69(3)°, V = 1297.1 Å 3 , Z = 4, R gt (F) = 0.076, wR ref (F 2 ) = 0.160, T = 120 K.
Open Access
Crystal structure of diethyl 2-(dibenzoylmethyl)-3-(triphenylphosphoranylidene) succinate, C₄₁H₃₇O₆P

11. Februar 2014

A. Ramazani, L. Dolatyari, A. R. Kazemizadeh, E. Ahmad, A. A. Torabi, R. Welter

Seiten: 181-183

PDF downloaden

C 41 H 37 O 6 P, triclinic, P 1̅ (no. 2), a = 11.128(5) Å, b = 12.548(5) Å, c = 13.420(5) Å, α = 87.523(5)°, β = 84.819(5)°, γ = 64.188(5)°, V = 1680.0 Å 3 , Z = 2, R gt (F) = 0.058, wR ref (F 2 ) = 0.148, T = 173 K.
Open Access
Crystal structure of 2-(6-[2-(5-ethyl-5-hydroxy-6-methyl-tetrahydro-pyran- 2-yl)-15-oxo-2,10,12-trimethyl-1,6,8-trioxa-dispiro[4.1.5.3]pentadec-13-en- 9-yl]-2-hydroxy-1,3-dimethyl-4-oxo-heptyl-5-methyl-tetrahydro-pyran- 2-yl)-butyrate sodium, Na(C₄₂H₆₇O₁₁), SY-9 – antibiotic 20-oxo-salinomycin

11. Februar 2014

E. F. Paulus, L. Vértesy

Seiten: 184-186

PDF downloaden

C 42 H 67 NaO 11 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 10.5617(5) Å, b = 19.1580(9) Å, c = 21.5366(9) Å, V = 4357.7 Å 3 , Z = 4, R gt (F) = 0.035, wR ref (F 2 ) = 0.082, T = 293 K.
Open Access
Crystal structure of 2-(3-methoxyphenylethynyl)-6-methylpyridine, C₁₅H₁₃NO, M-MPEP – a mGluR5 antagonist

11. Februar 2014

D. Alagille, R. M. Baldwin, C. D. Incarvito, G. Tamagnan

Seiten: 187-188

PDF downloaden

C 15 H 13 NO, monoclinic, P 12 1 / c 1 (no. 14), a = 15.986(3) Å, b = 6.760(1) Å, c = 11.415(2) Å, β = 104.63(3)°, V = 1193.5 Å 3 , Z = 4, R gt (F) = 0.055, wR ref (F 2 ) = 0.139, T = 183 K.
Open Access
Crystal structure of 4-methylanilinium dihydrogenphosphate, ( p-CH₃C₆H₄NH₃)(H₂PO₄)

11. Februar 2014

W. Smirani, A. Ben Slimane, M. Rzaigui

Seiten: 189-190

PDF downloaden

C 7 H 12 NO 4 P, orthorhombic, Pbca (no. 61), a = 7.790(3) Å, b = 24.645(4) Å, c = 9.867(2) Å, V = 1894.3 Å 3 , Z = 8, R gt (F) = 0.048, wR ref (F) = 0.053, T = 296 K.
Open Access
Crystal structure of (3R,1S′,2S′)-3-[1-benzyloxy-2,3-isopropylidenedioxypropyl]- 2-methyltetrahydro-1,2-oxazole, C₁₇H₂₅NO₄

11. Februar 2014

W. Frey, M. Henneböhle, V. Jäger

Seiten: 191-192

PDF downloaden

C 17 H 25 NO 4 , monoclinic, P 12 1 1 (no. 4), a = 8.547(3) Å, b = 9.176(2) Å, c = 11.166(2) Å, β = 102.24(2)°, V = 855.8 Å 3 , Z = 2, R gt (F) = 0.053, wR ref (F 2 ) = 0.137, T = 293 K.
Open Access
Crystal structure of (3S,4S)-4,5-O-cyclohexylidene-4,5-dihydroxy-3- methylamino-pentanoic acid hydrochloride, (C₁₂H₂₂NO₄)Cl

11. Februar 2014

W. Frey, M. Henneböhle, V. Jäger

Seiten: 193-194

PDF downloaden

C 12 H 22 ClNO 4 , monoclinic, P 12 1 1 (no. 4), a = 6.2327(3) Å, b = 7.9360(3) Å, c = 14.1536(5) Å, β = 99.709(4)°, V = 690.1 Å 3 , Z = 2, R gt (F) = 0.042, wR ref (F 2 ) = 0.115, T = 293 K.
Open Access
Crystal structure of chlorodimethyl(2-aminoethanethiolato)tin(IV), (NH₂CH₂CH₂S)SnCl(CH₃)₂

11. Februar 2014

M. D. Couce, G. Faraglia, U. Russo, R. Graziani, G. Valle

Seiten: 195-196

PDF downloaden

C 4 H 12 ClNSSn, orthorhombic, Pbca (no. 61), a = 11.422(2) Å, b = 11.475(2) Å, c = 13.582(2) Å, V = 1780.2 Å 3 , Z = 8, R gt (F) = 0.057, wR ref (F 2 ) = 0.147, T = 293 K.
Open Access
Crystal structure of methyl-2-hydroxy-2-phenyl-3-(4-bromophenyl)-3- phenylamino-propanoate, C₂₂H₂₀BrNO₃

11. Februar 2014

L. Malpezzi

Seiten: 197-198

PDF downloaden

C 22 H 20 BrNO 3 , monoclinic, P 12 1 / c 1 (no. 14), a = 17.643(1) Å, b = 5.935(1) Å, c = 18.782(1) Å, β = 90.13(1)°, V = 1966.7 Å 3 , Z = 4, R gt (F) = 0.041, wR ref (F 2 ) = 0.117, T = 293 K.
Open Access
Crystal structure of (η⁴-norborna-2,5-dien)-(1,2-bis((R,R)-2,5-bis- (methoxymethyl)phospholanyl)benzene)rhodium(I) tetrafluoroborate, [Rh(C₂₂H₃₆O₄P₂)(C₇H₈)](BF₄)

11. Februar 2014

J. Holz, A. Börner, A. Spannenberg, C. Pribbenow, D. Heller, H.-J. Drexler

Seiten: 199-200

PDF downloaden

C 29 H 44 BF 4 O 4 P 2 Rh, monoclinic, P 2 1 (no. 4), a = 10.119(2) Å, b = 14.125(3) Å, c = 11.542(2) Å, β = 106.87(3)°, V = 1578.7 Å 3 , Z = 2, R gt (F) = 0.034, wR ref (F 2 ) = 0.090, T = 200 K.
Open Access
Crystal structure of (η⁴-cycloocta-1,5-dien)(1,2-bis(diethylphosphino)- ethane)rhodium(I) tetrafluoroborate, [Rh(C₈H₁₂)(C₁₀H₂₄P₂)](BF₄)

11. Februar 2014

R. Kempe, A. Spannenberg, D. Heller, H.-J. Drexler

Seiten: 201-202

PDF downloaden

C 18 H 36 BF 4 P 2 Rh, monoclinic, P 12 1 / n 1 (no. 14), a = 15.522(3) Å, b = 9.173(2) Å, c = 15.862(3) Å, β = 103.91(3)°, V = 2192.3 Å 3 , Z = 4, R gt (F) = 0.037, wR obs (F 2 ) = 0.087, T = 200 K.

Ausgaben in diesem Band

In dieser Zeitschrift suchen

Dieses Heft

Alle Hefte

Ausgaben in diesem Band