Effect of the synthesis parameters on the structural and magnetic properties of strontium hexaferrite synthesized via the Pechini method
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Alfonso Enrique Ramírez Sanabria
Abstract
Strontium hexaferrite (SrFe12O19–SF6) is a magnetic material of great interest in various research fields due to its high coercive field (Hc) and its high saturation magnetization. In this research, the effect of synthesis parameters on the structure and magnetic response was studied. It was evidenced that the parameters such as pH value and iron precursor type have a strong influence on the crystalline structure of the samples, since the pure phase of strontium hexaferrite was obtained by two different pathways (ferrous and ferric) and only at pH = 5. It was determined that there are differences in the magnetic response of both samples; the ferrous pathway generates the largest values of both saturation magnetization (74.3 emu g−1) and coercive field (5.2 kOe).
References
[1] V.G. Harris , A.Geiler, Y.Chen, S.D.Yoon, M.Wu, A.Yang, Z.Chen, P.He, P.V.Parimi, X.Zuo, C.E.Patton, M.Abe, O.Acher, C.Vittoria: J. Magn. Magn. Mater.321 (2009) 2035–2047. 10.1016/j.jmmm.2008.10.020Search in Google Scholar
[2] T. Xie , L.Xu, C.Liu: Powder Technol.232 (2012) 87–92. 10.1016/j.powtec.2012.08.015Search in Google Scholar
[3] D.V. Ruikar , P.B.Kashid, V.R.Patil, V.Puri: Appl. Surf. Sci.265 (2013) 475–479. 10.1016/j.apsusc.2012.11.031Search in Google Scholar
[4] X. Tang , Y.M.Wang, Z.Luo, L.S.Wang, R.Y.Hong, W.G.Feng: Prog. Org. Coat.75(s 1–2):124–130. 10.1016/j.porgcoat.2012.04.006Search in Google Scholar
[5] J. Kreisel , H.Vincent, F.Tasset, M.Paté, J.P.Ganne: J. Magn. Magn. Mater.224 (2001) 17–29. 10.1016/S0304-8853(00)01355-XSearch in Google Scholar
[6] M. Cernea , S.-G.Sandu, C.Galassi, R.Radu, V.Kuncser: J. Alloys Compd.561 (2013) 121–128. 10.1016/j.jallcom.2013.01.081Search in Google Scholar
[7] H. Hsiang , R.Q.Yao: Mater. Chem. Phys.104 (2007) 1–4. 10.1016/j.matchemphys.2007.02.030Search in Google Scholar
[8] W. Yongfei , L.Qiaoling, Z.Cunrui, J.Hongxia: J. Alloys Compd.467 (2009) 284–287. 10.1016/j.jallcom.2007.12.037Search in Google Scholar
[9] A.E. Ramírez , N.J.Solarte, L.H.Singh, J.A.H.Coaquira, S.Gaona J.: J. Magn. Magn. Mater.438 (2017) 100–106. 10.1016/j.jmmm.2017.04.042Search in Google Scholar
[10] Barium Titanium Citrate, Barium Titanate and processes for producing some, US Patent: 3, 231, pp. 218, (1966).Search in Google Scholar
[11] S.R. Janasi , M.Emura, F.J.G.Landgraf, D.Rodrigues: J. Magn. Magn. Mater.238 (2002) 168–172. 10.1016/S0304-8853(01)00857-5Search in Google Scholar
[12] S.R. Janasi , M.Emura, F.J.G.Landgraf, D.Rodrigues: J. Magn. Magn. Mater.238 (2002) 168–172. 10.1016/S0304-8853(01)00857-5Search in Google Scholar
[13] Y.H.O. Muñoz , M.Ponce, J.E.R.Páez: Powder Technol.279 (2015), 86–95. 10.1016/j.powtec.2015.03.049Search in Google Scholar
[14] H. Zhang , D.Zeng, Z.Liu: J. Magn. Magn. Mater.322 (2010) 2375–2380. 10.1016/j.jmmm.2010.02.040Search in Google Scholar
[15] F. Esper : Journal de Physique Colloques, 1977, 38 (C1), pp. C1-69-C1-72. 10.1051/jphyscol:1977114Search in Google Scholar
[16] J.H. de Araújo , J.M.Soares, M.F.Giani, F.L.A.Machado, J.B.M.da Cunha: J. Magn. Magn. Mater.343 (2013) 203–207. 10.1016/j.jmmm.2013.04.077Search in Google Scholar
[17] R.C. Pullar : Prog. Mater. Sci.57 (2012) 1191–1334. 10.1016/j.pmatsci.2012.04.001Search in Google Scholar
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- DGM News
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Articles in the same Issue
- Contents
- Contents
- Editorial
- Welcome to Prof. Joachim Bill as a new editor for IJMR
- Original Contributions
- Fabrication of highly porous merwinite scaffold using the space holder method
- Improvement of AISI 4340 steel properties by intermediate quenching – microstructure, mechanical properties, and fractography
- Hardness and corrosion properties of functionally graded AA5083/Al2O3 composites produced by powder metallurgy method
- Production and properties of functionally graded hybrid composites containing Al3Ti and TiB2
- Experimental measurement and thermodynamic model predictions of the distributions of Cu, As, Sb and Sn between liquid lead and PbO–FeO–Fe2O3–SiO2 slag
- Effect of Co substitution on the magnetic properties and magnetocaloric effects of Ni–Co–Mn–Sn alloys
- Effect of the synthesis parameters on the structural and magnetic properties of strontium hexaferrite synthesized via the Pechini method
- Investigation on microstructural and mechanical properties of sub-zero processed AISI 440C steel
- Effects of rail flash-butt welding and post-weld heat treatment processes meeting different national standards on residual stresses of welded joints
- DGM News
- DGM News