On the evolution of microstructure in oxygen-free high conductivity copper during thermo-mechanical processing using rotary swaging
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Frederik Otto
, Jan Frenzel und Gunther Eggeler
Abstract
In the present work, the processing parameters which govern the evolution of microstructure during rotary swaging and intermediate/subsequent heat treatments in copper rods were studied. Copper ingots with an initial diameter of 40 mm were reduced to a final diameter of 11.7 mm by rotary swaging. Processing sequences were applied with different intermediate anneals and various final heat treatments. The resulting microstructures were characterized using orientation imaging microscopy, optical microscopy and hardness measurements. Special emphasis was placed on the evolution of microstructure with respect to the radial and longitudinal position in the rod. Most importantly, microstructural evidence for torsional loading during swaging was found, and a spiral grain morphology was observed. Moreover, localized deformation events were identified and evidence for abnormal grain growth was found. Finally, a combination of swaging and heat treatment parameters was identified which allowed a homogeneous grain structure to be produced.
References
[1] S.-J.Lim, K.-H.Na, H.-J.Choi, Y.-B.Park, C.-H.Lee: Proc. Inst. Mech. Eng., Part B221 (2007) 1401.10.1243/09544054JEM883Suche in Google Scholar
[2] F.Müller: Dissertation, Berichte aus Produktion und Umformtechnik 36, Shaker Verlag, Aachen (1997).Suche in Google Scholar
[3] G.E.Dieter: Mechanical Metallurgy, SI Metric Ed., McGraw-Hill, London (1988).Suche in Google Scholar
[4] F.J.Humphreys, M.Hatherly: Recrystallization and Related Annealing Phenomena, 1st Ed., Elsevier, Oxford (1976).Suche in Google Scholar
[5] D.Hull, D.E.Rimmer: Philos. Mag.4 (1959) 673.10.1080/14786435908243264Suche in Google Scholar
[6] V.M.Andronov, V.A.Gritskik: Phys. Met. Metallogr.33 (1972) 145.Suche in Google Scholar
[7] B.Ortner, H.P.Stüwe: Z. Metallkd.67 (1976) 672.Suche in Google Scholar
[8] F.Ackermann, L.P.Kubin, J.Lepinoux, H.Mughrabi: Acta Metall.32 (1984) 715.10.1016/0001-6160(84)90145-7Suche in Google Scholar
[9] A.Berger, P.J.Wilbrandt, F.Ernst, U.Klement, P.Haasen: Prog. Mater. Sci.32 (1988) 1.10.1016/0079-6425(88)90009-6Suche in Google Scholar
[10] H.Mughrabi: Acta Metall.31 (1983) 1367.10.1016/0001-6160(83)90007-XSuche in Google Scholar
[11] H.Conrad: Metall. Mater. Trans. A35 (2004) 2681.10.1007/s11661-004-0214-5Suche in Google Scholar
[12] H.Conrad: Mater. Sci. Eng. A341 (2003) 216.10.1016/S0921-5093(02)00238-1Suche in Google Scholar
[13] T.Hebesberger, H.P.Stüwe, A.Vorhauer, F.Wetscher, R.Pippan: Acta Mater.53 (2005) 393.10.1016/j.actamat.2004.09.043Suche in Google Scholar
[14] A.Grabianowski, B.Danda, B.Ortner, H.P.Stüwe: Mech. Res. Commun.7 (1980) 125.Suche in Google Scholar
[15] J.Schrank, B.Ortner, H.P.Stüwe, A.Grabianowski: Mater. Sci. Technol.1 (1985) 544.Suche in Google Scholar
[16] J.Schrank, H.P.Stüwe: Z. Metallkd.77 (1986) 107.Suche in Google Scholar
[17] B.Ortner, A.Grabianowski, A.Danda: Aluminium58 (1982) 657.Suche in Google Scholar
[18] M.F.Hupalo, A.F.Padilha, H.R.Z.Sandim, A.M.Kliauga: ISIJ Int.44 (2004) 1894.Suche in Google Scholar
[19] H.R.Z.Sandim, H.J.McQueen, W.Blum: Scr. Mater.42 (2000) 151.10.1016/S1359-6462(99)00331-0Suche in Google Scholar
[20] M.F.Hupalo, H.R.Z.Sandim: Mater. Sci. Eng. A318 (2001) 216.10.1016/S0921-5093(01)01323-5Suche in Google Scholar
[21] A.O.F.Hayama, H.R.Z.Sandim, J.F.C.Lins, M.F.Hupalo, A.F.Padilha: Mater. Sci. Eng. A371 (2004) 198.10.1016/j.msea.2003.11.052Suche in Google Scholar
[22] J.Frenzel, J.Pfetzing, K.Neuking, G.Eggeler: Mater. Sci. Eng. A481 (2008) 635.10.1016/j.msea.2007.03.115Suche in Google Scholar
[23] M.F.Hupalo, A.F.Padilha, H.R.Z.Sandim, A.M.Kliauga: ISIJ Int.44 (2004) 1902.Suche in Google Scholar
[24] E.Weck, E.Leistner: Metallographic Instructions for Colour Etching by Immersion Part I: Klemm Colour Etching, DVS, Düsseldorf (1982).Suche in Google Scholar
[25] B.Bacroix, P.Gerber, O.Castelnau, in: G. Gottstein, D.A. Molodov (Eds.), Recrystallisation and Grain Growth, Proceedings of the First Joint International Conference, Springer-Verlag, Berlin (2001) 623.Suche in Google Scholar
[26] J.B.Koo, D.Y.Yoon, M.F.Henry: Metall. Mater. Trans. A31 (2000) 1489.10.1007/s11661-000-0267-zSuche in Google Scholar
[27] J.B.Koo, D.Y.Yoon: Metall. Mater. Trans A32 (2001) 1911.10.1007/s11661-001-0004-2Suche in Google Scholar
[28] J.B.Koo, D.Y.Yoon, M.F.Henry: Metall. Mater. Trans A33 (2002) 3803.10.1007/s11661-002-0253-8Suche in Google Scholar
[29] N.Rajmohan, J.A.Szpunar: Scr. Mater.44 (2001) 2387.10.1016/S1359-6462(01)00941-1Suche in Google Scholar
[30] G.Abbruzzese, K.Lücke: Acta Metall.34 (1986) 905.10.1016/0001-6160(86)90064-7Suche in Google Scholar
[31] A.D.Rollett, W.W.Mullins: Scr. Mater.36 (1997) 975.10.1016/S1359-6462(96)00501-5Suche in Google Scholar
[32] H.Afer, N.Rouag, R.Penelle: J. Cryst. Growth268 (2004) 320.10.1016/j.jcrysgro.2004.05.001Suche in Google Scholar
[33] H.-C.Kim, C.-G.Kang, M.-Y.Huh, O.Engler: Scr. Mater.57 (2007) 325.10.1016/j.scriptamat.2007.04.023Suche in Google Scholar
[34] O.M.Ivasishin, S.V.Shevchenko, S.L.Semiatin: Scr. Mater.50 (2004) 1241.10.1016/j.scriptamat.2004.01.036Suche in Google Scholar
[35] C.S.Barrett, T.B.Massalski: Structure of Metals, 3rd Ed., McGraw-Hill, New York (1966).Suche in Google Scholar
[36] R.O.Williams: Acta Metall.13 (1965) 163.10.1016/0001-6160(65)90192-6Suche in Google Scholar
[37] A.W.Thompson, B.C.Wonsiewicz: Metall. Trans. A12 (1981) 531.10.1007/BF02648552Suche in Google Scholar
© 2011, Carl Hanser Verlag, München
Artikel in diesem Heft
- Contents
- Contents
- Original Contributions
- On the evolution of microstructure in oxygen-free high conductivity copper during thermo-mechanical processing using rotary swaging
- Phase-field simulation of diffusion couples in the Ni–Al system
- Finnis–Sinclair potentials for fcc Au–Pd and Ag–Pt alloys
- Hollow pyramidal lattice truss structures
- Synthesis of single-phase polycrystalline Ca2Si powder and sintered compacts
- On the micromechanics of die compaction of composite powder materials
- Structural, thermal, electrical and mechanical properties of nanosilica-composite polymer electrolytes
- The effects of tool rotation speed and traverse speed on friction stir welding of AISI 304 austenitic stainless steel
- Estimation of Fe2B growth on low-carbon steel based on two diffusion models
- Glass-forming ability and thermal stability of gas-atomized Zr50Cu40Al10 metallic glass powders
- Mechanochemical synthesis of nanocrystalline lead selenide: industrial approach
- On abnormal grain growth in nanocrystalline materials induced by small particles
- High-temperature deformation behaviour of Ti3Al-11Nb intermetallic
- Optimization of ZnO2 nanoparticle content in binary blended concrete to enhance high strength concrete
- New structural and mechanical features of hexagonal materials after room temperature extrusion using the KoBo method
- People
- Yuri Estrin turns 65
- DGM News
- DGM News
Artikel in diesem Heft
- Contents
- Contents
- Original Contributions
- On the evolution of microstructure in oxygen-free high conductivity copper during thermo-mechanical processing using rotary swaging
- Phase-field simulation of diffusion couples in the Ni–Al system
- Finnis–Sinclair potentials for fcc Au–Pd and Ag–Pt alloys
- Hollow pyramidal lattice truss structures
- Synthesis of single-phase polycrystalline Ca2Si powder and sintered compacts
- On the micromechanics of die compaction of composite powder materials
- Structural, thermal, electrical and mechanical properties of nanosilica-composite polymer electrolytes
- The effects of tool rotation speed and traverse speed on friction stir welding of AISI 304 austenitic stainless steel
- Estimation of Fe2B growth on low-carbon steel based on two diffusion models
- Glass-forming ability and thermal stability of gas-atomized Zr50Cu40Al10 metallic glass powders
- Mechanochemical synthesis of nanocrystalline lead selenide: industrial approach
- On abnormal grain growth in nanocrystalline materials induced by small particles
- High-temperature deformation behaviour of Ti3Al-11Nb intermetallic
- Optimization of ZnO2 nanoparticle content in binary blended concrete to enhance high strength concrete
- New structural and mechanical features of hexagonal materials after room temperature extrusion using the KoBo method
- People
- Yuri Estrin turns 65
- DGM News
- DGM News