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Mechanochemical synthesis of nanocrystalline lead selenide: industrial approach

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Veröffentlicht/Copyright: 11. Juni 2013
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International Journal of Materials Research
Aus der Zeitschrift International Journal of Materials Research Band 102 Heft 4

Abstract

Mechanochemical synthesis of lead selenide PbSe nanoparticles was performed by high-energy milling of lead and selenium powder in a laboratory planetary ball mill and in an industrial eccentric vibratory mill. Structural properties of the synthesized lead selenide were characterized using X-ray diffraction that confirmed crystalline nature of PbSe nanoparticles. The average size of PbSe crystallites of 37 nm was calculated from X-ray diffraction data using the Williamson – Hall method. The methods of particle size distribution analysis, specific surface area measurement, scanning electron microscopy and transmission electron microscopy were used for characterization of surface, mean particle size, and morphology of PbSe. An application of industrial mill verified a possibility of the synthesis of a narrow bandgap semiconductor PbSe at ambient temperature and in a relatively short reaction time.

Keywords: Mechanochemical synthesis; Laboratory mill; Industrial mill; Lead selenide
* Correspondence address, Mgr. Marcela Achimovičová, PhD., Institute of Geotechnics, Slovak Academy of Sciences, Watsonova 45, 04353 Košice, Slovakia. Tel.: +421 055 792 2606, Fax: +421 055 792 2604, E-mail:

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Received: 2010-7-14
Accepted: 2011-2-3
Published Online: 2013-06-11
Published in Print: 2011-04-01

© 2011, Carl Hanser Verlag, München

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https://doi.org/10.3139/146.110496
Schlagwörter für diesen Artikel
Mechanochemical synthesis; Laboratory mill; Industrial mill; Lead selenide

Artikel in diesem Heft

  1. Contents
  2. Contents
  3. Original Contributions
  4. On the evolution of microstructure in oxygen-free high conductivity copper during thermo-mechanical processing using rotary swaging
  5. Phase-field simulation of diffusion couples in the Ni–Al system
  6. Finnis–Sinclair potentials for fcc Au–Pd and Ag–Pt alloys
  7. Hollow pyramidal lattice truss structures
  8. Synthesis of single-phase polycrystalline Ca2Si powder and sintered compacts
  9. On the micromechanics of die compaction of composite powder materials
  10. Structural, thermal, electrical and mechanical properties of nanosilica-composite polymer electrolytes
  11. The effects of tool rotation speed and traverse speed on friction stir welding of AISI 304 austenitic stainless steel
  12. Estimation of Fe2B growth on low-carbon steel based on two diffusion models
  13. Glass-forming ability and thermal stability of gas-atomized Zr50Cu40Al10 metallic glass powders
  14. Mechanochemical synthesis of nanocrystalline lead selenide: industrial approach
  15. On abnormal grain growth in nanocrystalline materials induced by small particles
  16. High-temperature deformation behaviour of Ti3Al-11Nb intermetallic
  17. Optimization of ZnO2 nanoparticle content in binary blended concrete to enhance high strength concrete
  18. New structural and mechanical features of hexagonal materials after room temperature extrusion using the KoBo method
  19. People
  20. Yuri Estrin turns 65
  21. DGM News
  22. DGM News
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