Home The use of color etching to study the microstructure of laser welded steel used in the automotive industry
Article
Licensed
Unlicensed Requires Authentication

The use of color etching to study the microstructure of laser welded steel used in the automotive industry

  • Daniel Dobras and Małgorzata Rutkowska-Gorczyca
Published/Copyright: October 30, 2019
Become an author with De Gruyter Brill

Abstract

In the present article the results of a microstructure study of dual phase, multiphase (with transformation induced plasticity effect) and manganese-boron steel have been presented in the as-delivered state and after laser fusion by means of color metallography, which, up to now, has not been applied in those types of joints. In order to reveal the components of the microstructure of the steel types studied, five reagents were applied: nital, pikral, Klemm, LePera and sodium metabisulfite, in different combinations. Various phases were revealed in the material in the as-delivered state and after fusion, and this would not have been possible using standard procedures by means of a light microscope. In the as-delivered state all basic phases were observed. In the state after laser remelting, the observed microstructures were completely different than in the received state giving bainite and martensite an advantage. Measurements of the hardness of the as-received material and the welds of the tested steels were performed, showing a significant increase in weld hardness.


*Correspondence Address, Daniel Dobras, Wrocław University of Science and Technology, Department of Metal Forming and Metrology, Faculty of Mechanical Engineering, 7−9 I. Łukasiewicza Street, 50−371 Wrocław, Poland, E-mail: daniel.dobras@pwr.edu.pl

M. Sc. Eng. Daniel Dobras, born 1993, is a PhD student at Wrocław University of Science and Technology, Poland, Faculty of Mechanical Engineering, in the discipline Construction and Operation of Machines. From October 2018 to February 2019 he was had a research internship in the Department of Industrial Engineering at University of Padova, Italy.

Dr Eng. Małgorzata Rutkowska-Gorczyca, born 1981, has been employed as a Teaching and Research Adjunct at the Wroclaw University of Science and Technology, Poland, since 2009, with a specialization in the field of Mechanical Engineering and Material Science research. She received her Master's Degree at Wrocław University of Technology, Faculty of Fundamental Problems of Technology in 2007. This was followed by a PhD from the same university, Faculty of Mechanical Engineering, in the discipline Construction and Operation of Machines, in 2012


References

1 R.Kuziak, R.Kawalla, S.Waengler: Advanced high strength steels for automotive industry, Archives of Civil and Mechanical Engineering8 (2008), pp. 10311710.1016/S1644-9665(12)60197-6Search in Google Scholar

2 Z.Gronostajski, A.Niechajowicz, S.Polak: Prospects for the use of new-generation steels of the AHSS type for collision energy absorbing components, Archives of Metallurgy and Materials55 (2010), pp. 221230Search in Google Scholar

3 S.Keeler, M.Kimchi: Advanced High-Strength Steels Application Guidelines Version 5, WorldAutoSteels, Middletown (OH) (2014)Search in Google Scholar

4 H.Karbasian, A. E.Tekkaya: A review on hot stamping, Journal of Materials Processing Technology210 (2010), pp. 2103211810.1016/j.jmatprotec.2010.07.019Search in Google Scholar

5 N.Farabi, D. L.Chena, J.Li, Y.Zhou, S. J.Dong: Microstructure and mechanical properties of laser welded DP600 steel joints, Materials Science & Engineering A527 (2010), pp. 1215122210.1016/j.msea.2009.09.051Search in Google Scholar

6 L.Zhao, M. K.Wibowo, M. J. M.Hermans, S. M. C.Van Bohemen, J.Sietsma: Retention of austenite in the welded microstructure of a 0.16C–1.6Mn–1.5Si (wt.%) TRIP steel, Journal of Materials Processing Technology209 (2009), pp. 5286529210.1016/j.jmatprotec.2009.03.017Search in Google Scholar

7 K. I.Yaakob, M. I.Ishak, M. M.Quazi, M. N. M.Salleh: Optimizing the pulse wave mode low power fibre laser welding parameters of 22MnB5 boron steel using response surface methodology, Measurement135 (2018), pp. 45246610.1016/j.measurement.2018.10.035Search in Google Scholar

8 A. K.De, J. G.Speer, D. K.Matlock: Color Tint-Etching for Multiphase Steels, Advanced Materials & Processes2 (2003), pp. 2730Search in Google Scholar

9 F.Hairer, A.Karelová, C.Krempaszky: Etching techniques for the microstructural characterization of complex phase steels by light microscopy, in: International Doctoral Seminar, Smolenice Castle (2008), pp. 5054Search in Google Scholar

10 G. F.Vander Voort: ASM Handbook, Volume 9: Metallography and Microstructures, 5th Ed., ASM International Novelty (OH) (2004)10.31399/asm.hb.v09.9781627081771Search in Google Scholar

11 E.Leunis, D.Hanlon, A.Rijkenberg, C.Scott, J.Drillet, R.Hackl: Quantitative phase analysis of multi-phase steels — PHAST, European Communities, Luxembourg (2006)Search in Google Scholar

12 E.Weck, E.Leistner: Metallographic Instructions for Colour Etching by Immersion Part I: Klemm Colour Etching, D. V. S. Verlag GmbH, Dusseldorf (1982)Search in Google Scholar

13 Z.Gronostajski, A.Niechajowicz, R.Kuziak, J.Krawczyk, S.Polak: The effect of the strain rate on the stress-strain curve and microstructure of AHSS, Journal of Materials Processing Technology242 (2017), pp. 24625910.1016/j.jmatprotec.2016.11.023Search in Google Scholar

14 D.Dobras, M.Rutkowska-Gorczyca: Application of color etching to study the microstructure of TRIP steel after laser remelting, Welding Technology Review90 (2018), pp. 141910.26628/wtr.v90i12.984Search in Google Scholar

15 R.Haimann: Metaloznawstwo, Oficyna Wydawnicza Politechniki Wrocławskiej, Wrocław (1980)Search in Google Scholar

16 S.Staub: Atlas mikrostruktur stali: mikroskop elektronowy, Śląsk, Katowice (1970)Search in Google Scholar

17 A.Krajczyk: Podręczny atlas mikrostruktur metali i stopów, Oficyna Wydawnicza Politechniki Wrocławskiej, Wrocław (2005)Search in Google Scholar

18 S.Zajac, V.Schwinn, K. H.Tacke: Characterisation and quantification of complex bainitic microstructures in high and ultra-high strength line pipe steels, Materials Science Forum500-501 (2005), pp. 38739510.4028/www.scientific.net/MSF.500-501.387Search in Google Scholar

19 M. S.Węglowski, S.Stano, G. MichtaG, W.Osuch: Structural characterization of Nd:YAG laser welded joint of dual phase steel, Archives of Metallurgy and Materials55 (2010), pp. 211220Search in Google Scholar

20 G.Krauss, S. W.Thompson: Ferritic microstructures in continuously cooled low- and ultralow- carbon steels, ISIJ International35 (1995), pp. 93794510.2355/isijinternational.35.937Search in Google Scholar

21 D.Rutkowski, A.Ambroziak: Effect of laser strengthening on the mechanical properties of car body steels presently used in automotive industry, Biuletyn Instytutu Spawalnictwa58 (2014), pp. 4957Search in Google Scholar

Published Online: 2019-10-30
Published in Print: 2019-11-04

© 2019, Carl Hanser Verlag, München

Downloaded on 25.9.2025 from https://www.degruyterbrill.com/document/doi/10.3139/120.111424/html
Scroll to top button