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Production- and microstructure-based fatigue assessment of metallic AISI 304/430 multilayer materials produced by hot pack rolling

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Published/Copyright: January 27, 2017
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Abstract

Metallic multilayer materials consisting of hundreds or thousands of layers offer a high potential for broad applications in modern technology. A uniform and gradual thinning of layers can be realized by using alloys with different crystal structures in combination with the efficient and high-performance technology of hot pack rolling. However, investigations on fatigue properties, especially to evaluate the influence of the number of layers, are still missing. In the present study, the fatigue behavior of metallic multilayer materials consisting of austenitic and ferritic stainless steels AISI 304 and AISI 430 with 100 and 1400 layers are characterized by applying a time-efficient load increase procedure. Therefore, instrumented stepwise load increase tests were performed to define suitable loading parameters for a convenient comparison of fatigue properties in constant amplitude tests. A benefit of the complex production process leading to 1400 layers was verified concerning the investigated load level in the range of low cycle fatigue with a significant improvement by the factor of 3.5. The alternating current potential drop method for measurements of change in voltage was determined to be most suitable to detect microstructural changes at an early state of fatigue damage for multilayer materials. Microstructures as well as fractured surfaces were investigated using light and scanning electron microscopy to evaluate the results of the two technological manufacturing routes as well as the crack and failure behavior.

Kurzfassung

Metallische Mehrschichtwerkstoffe bestehen aus hunderten oder tausenden Schichten und bieten daher ein hohes Potential für den Einsatz in industriellen Anwendungen. Eine sukzessive und gleichmäßige Reduzierung der Schichtdicken wird über die Verwendung von Legierungen mit unterschiedlichen Kristallstrukturen in Kombination mit dem effizienten und leistungsstarken Paket-Warmwalzverfahren sichergestellt. Untersuchungen zu den Ermüdungseigenschaften, insbesondere im Hinblick auf den Einfluss der Schichtanzahl, existieren bisher nicht. Im Rahmen dieser Studie wurde das Ermüdungsverhalten von metallischen Mehrschichtwerkstoffen, die aus 100 und 1400 Schichten der austenitischen und ferritischen Edelstähle 1.4301 und 1.4016 bestehen, auf Basis eines effizienten stufenförmigen Laststeigerungsverfahrens charakterisiert. Die instrumentierten Laststeigerungsversuche wurden dazu verwendet, um geeignete Beanspruchungen für den Vergleich der beiden Mehrschichtwerkstoffe in Einstufenversuchen zu definieren. Für das untersuchte Lastniveau im LCF-Bereich konnte ein Vorteil des aufwendigeren Verfahrens zur Herstellung von 1400 Schichten mit einer signifikanten Erhöhung der Bruchlastspielzahlen um den Faktor 3,5 nachgewiesen werden. Es wurde belegt, dass die Wechselstrompotentialsonde zur Messung der elektrischen Wechselspannung exzellent geeignet ist, um verformungs- und mikrostrukturbedingte Schädigungen der Mehrschichtwerkstoffe durch zyklische Beanspruchung frühzeitig zu detektieren. Die Untersuchungen wurden durch licht- und rasterelektronenmikroskopische Analysen der Gefüge und Bruchflächen ergänzt, um eine Bewertung der mechanischen Eigenschaften sowie des Schädigungs- und Rissverhaltens hinsichtlich der zwei Prozessrouten des Paket-Warmwalzverfahrens vorzunehmen.


*Correspondence Address, Prof. Dr.-Ing. F. Walther, M.Sc. Anke Schmiedt, Institute for Design and Materials Testing (IKW), Department of Materials Test Engineering (WPT), TU Dortmund University, Baroper Str. 303, D 44227 Dortmund, Germany, E-mail:

MSc Anke Schmiedt, born in 1986, studied Mechanical Engineering with specialization in Materials Engineering at Ruhr-University Bochum, Germany. After her master degree in 2011, she worked at Siemens AG, Energy Sector in Mülheim an der Ruhr, Germany, in the Department of Materials Engineering and generated LCF material design data for power plant components. Since 2014, she has been working as a research assistant in the field of fatigue and corrosion fatigue testing of stainless steels in the Department of Materials Test Engineering (WPT) of TU Dortmund University, Germany.

Lukas Luecker, born in 1989, studies Mechanical Engineering with specialization in Machine Technology at TU Dortmund University, Germany. Since 2015, he has been working parallel to his studies as a student assistant in the Department of Materials Test Engineering (WPT) at TU Dortmund University, Germany. His research focus is on fatigue and fracture of metals.

Prof. Dr. Alexander G. Kolesnikov, born in 1947, graduated from Moscow Higher Technical School named after Bauman, Russia. After graduating from college, he worked there as an assistant, Associate Professor and Professor. In 1979, he defended his doctoral thesis. Since 1989, he has worked as Head of scientific-educational complex “Engineering technologies” and since 2002 as Head of the Department “Equipment and Technology of Rolling”. For his work on the creation of a new class of structural materials, he was awarded the Prize of the State Prize of the Russian Federation In 2001.

Dr. Andrew I. Plokhikh, born in 1961, graduated from Moscow Higher Technical School named after Bauman, Russia. In 1997, he defended his thesis on the topic of high-strength maraging steel with carbide and intermetallic hardening. Since 1997, he has been working as Associate Professor of Materials Science at Moscow State Technical University named after Bauman, and since 2001, he is Head of the faculty of the test center “Engineering technologies”. His research interests include material science of high strength steels of martensitic class, development of metallic materials with nanostructure, composites of nonmetallic materials and methods of mechanical testing.

Prof. Dr.-Ing. Frank Walther, born in 1970, studied Mechanical Engineering with majoring in Materials Science and Engineering at TU Kaiserslautern University, Germany. There he finished his PhD on the fatigue assessment of railway wheel steels at Chair of Materials Science and Engineering (WKK) in 2002. Until 2008, he headed the group Fatigue Behavior at WKK and finished his postdoctoral qualification (habilitation) in Materials Science and Engineering in 2007. He then joined Schaeffler in Herzogenaurach, Germany, and took responsibility for Public Private Partnership within Corporate Development. Since 2010, he has been Professor for Materials Test Engineering (WPT) at TU Dortmund University, Germany. His research portfolio includes determination of process-structure-property relationships of metal- and polymer-based material systems taking into account the influence of manufacturing and joining processes as well as service-relevant loading and environmental conditions. He focuses on measurement and testing approaches for fatigue assessment from LCF to VHCF regions, physically-based deformation and damage development characterization and modeling as well as (remaining) fatigue life calculation.


References

1 B.Huang, K. N.Ishihara, P. H.Shingu: Preparation of high strength bulk nano-scale Fe/Cu multilayers by repeated pressing-rolling, Materials Science Letters20 (2001), pp. 1669167010.1023/A:1012465117652Search in Google Scholar

2 K.Yasuna, M.Terauchi, A.Otsuki, K. N.Ishihara, P. H.Shingu: Formation of nanoscale Fe/Ag multilayer by repeated press-rolling and its layer thickness dependence of magnetoresistance, Materials Science & Engineering A285 (2000), pp. 41241710.1016/S0921-5093(00)00680-8Search in Google Scholar

3 D. W.Kum, T.Oyama, O. A.Ruano, O. D.Sherby: Development of ferrous laminated composites with unique microstructures by control of carbon diffusion, Metallurgical Transactions A17 (1986), pp. 1517152110.1007/BF02650087Search in Google Scholar

4 M.Pozuelo, F.Carreno, C. M.Cepeda-Jimenez, O. A.Ruano: Effect of hot rolling on bonding characteristics and impact behavior of a laminated composite material based on UHCS-1.35 Pct C, Metallurgical and Materials Transactions A39 (2008), pp. 66667110.1007/s11661-007-9441-xSearch in Google Scholar

5 Y.Saito, N.Tsuji, H.Utsunomiya, T.Sakai: Novel ultra-high straining process for bulk materials – Development of the accumulative roll-bonding (ARB) process, Acta Materialia47 (1999), pp. 57958310.1016/S1359-6454(98)00365-6Search in Google Scholar

6 N.Tsuji, Y.Ito, Y.Saito, Y.Minamino: Strength and ductility of ultrafine grained aluminum and iron produced by ARB and annealing, Scripta Materialia47 (2002), pp. 89389910.1016/S1359-6462(02)00282-8Search in Google Scholar

7 A. G.Kolesnikov, A. I.Plokhikh, Yu. S.Komissarchuk, I. Yu.Mikhaltsevich: A study of special features of formation of submicro and nanosize structure in multilayer materials by the method of hot rolling, Metal Science and Heat Treatment52 (2010), pp. 27327810.1007/s11041-010-9266-xSearch in Google Scholar

8 T. I.Tabatchikova, I. L.Yakovlev, A. I.Plokhikh, S. Yu.Del'gado Reina: Studying a multilayer material based on stainless steels and produced by hot pack rolling, The Physics of Metals and Metallography115 (2014), pp. 40341210.1134/S0031918X14040152Search in Google Scholar

9 F.Walther: Microstructure-oriented fatigue assessment of construction materials and joints using short-time load increase procedure, MP Materials Testing56 (2014), pp. 51952710.3139/120.110592Search in Google Scholar

10 B.Ebel-Wolf, F.Walther, D.Eifler: Cyclic deformation behaviour and lifetime calculation of the magnesium die-cast alloys AZ91D, MRI 153M and MRI 230D, International Journal of Materials Research98 (2007), pp. 11712210.3139/146.101443Search in Google Scholar

11 D.Huelsbusch, M.Haack, A.Solbach, C.Emmelmann, F.Walther: Influence of pin size on tensile and fatigue behavior of Ti-CFRP hybrid structures produced by laser additive manufacturing, ICCM20, Proc. of the 20th International Conference on Composite Materials (2015), pp. 112Search in Google Scholar

Published Online: 2017-01-27
Published in Print: 2017-02-03

© 2017, Carl Hanser Verlag, München

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