Adhesive tensile testing of atmospheric plasma sprayed zinc coating on a 1.4301 substrate
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Philipp Stögmüller
Abstract
The atmospheric plasma spray (APS) process for applying thin coatings on substrates has a lot of different process parameters. To evaluate which parameters have the most significant influence on the adhesive strength, a design of experience (DoE) investigation was performed. The data for the DoE analyses were generated with an own designed adhesive tensile strength test device according to EN 13144. For these experiments, the two component epoxy HTK Ultra Bond 100 was used for loading the interface of APS zinc coated steel samples. To provide a highly repeatable test setup, a special gluing device was developed to cope with the requirements of the Ultra Bond 100. Although the DoE analysis showed the expected results, the pull-off test has some weaknesses, which are shown and discussed in the present paper.
Kurzfassung
Der Atmosphärenplasmaspritzprozess (APS) zum Auftragen dünner Schichten wird von einer Vielzahl an Prozessparameter beeinflusst. Um jene Parameter herauszufinden, welche einen signifikanten Einfluss auf die Schichthaftung haben, wurde eine Versuchsplan-Analyse (Design of Experiments (DoE-Analyse)) durchgeführt. Zur Generierung der Daten für die DoE-Analyse wurde, in Anlehnung an die Norm EN 13144, eine Abzugsvorrichtung entwickelt, um einen Stirnabzugsversuch durchführen zu können. Für die Verbindung zwischen beschichteten Substraten und Abzugsstempel wurde ein normgerechter Zweikomponenten Epoxidklebstoff namens HTK Ultra Bond 100 verwendet. Um eine reproduzierbare Klebung zu gewährleisten und den Anforderungen des Ultra Bond gerecht zu werden, wurde eine Verklebevorrichtung entwickelt. Obwohl die DoE-Analyse die erwarteten Ergebnisse zeigte, wurden bei der Versuchsdurchführung einige Schwächen des Stirnabzugsversuches festgestellt, welche in dieser Publikation aufgezeigt und diskutiert werden.
References
1 R.Heimann, Plasma Spray Coating, 2nd Ed.Wiley-VCH, Weinheim, Germany (2008)Suche in Google Scholar
2 J. M.Lackner, W.Waldhauser, M.Schwarz, F.Collins, D.Burtner: Adhesion improvement of PVD coatings by plasma treatment with linear anode layer ion sources, D.Mattox, V.Mattox: 50th Annual Technical Conference – Society of Vacuum Coaters, Louisville (2007)Suche in Google Scholar
3 J. M.Lackner, W.Heinz, W.Waldhauser, E.Brandstätter, M.Schwarz: Haftungssteigerung von PVD-Beschichtungen durch Plasmabehandlung mit gitterlosen Anode-Layer-Source-Ionenquellen, Jahrbuch-Oberflächentechnik (2007), pp. 1–21Suche in Google Scholar
4 J.Großmann: Einfluß von Plasmabehandlungen auf die Haftfestigkeit vakuumtechnisch hergestellter Polymer-Metall-Verbunde, Dissertation, TU Erlangen-Nürnberg, Germany (2009)Suche in Google Scholar
5 J. F.Coulon, N.Tournerie, H.Maillard: Adhesion enhancement of Al coatings on carbon/epoxy composite surfaces by atmospheric plasma, Applied Surface Science283 (2013), pp. 843–85010.1016/j.apsusc.2013.07.028Suche in Google Scholar
6 EN ISO 2409: Paints and varnishes – Cross-cut test, Austrian Standards Institute, Vienna (2013)Suche in Google Scholar
7 J.Valli: A review of adhesion test methods for thin hard coatings, Journal of Vacuum Science & Technology A: Vacuum, Surfaces and Films4 (1986), pp. 3007–301410.1116/1.573616Suche in Google Scholar
8 EN 13144: Metallic and other inorganic coatings – Method for quantitative measurements of adhesion by tensile test, Austrian Standards Institute, Vienna (2003)Suche in Google Scholar
9 EN ISO 4624: Paints and varnishes – Pull-off test for adhesion, Austrian Standards Institute, Vienna (2003)Suche in Google Scholar
10 EN 582: Thermal spraying – Determination of tensile adhesive, Austrian Standards Institute, Vienna (1993)Suche in Google Scholar
11 M.Mellali, P.Fauchais, A.Grimaud: Influence of substrate roughness and temperature on the adhesion/cohesion of alumina coatings, Surface and Coatings Technology81 (1996), pp. 275–28610.1016/0257-8972(95)02540-5Suche in Google Scholar
12 F.-W.Bach, A.Laarmann, K.Möhwald, T.Wenz: Moderne Beschichtungsverfahren, 2nd Ed.Wiley-VCH, Weinheim, Germany (2005)10.1002/3527604278Suche in Google Scholar
13 L.Pawlowski: The Science and Engineering of Thermal Spray Coatings, 2nd Ed., John Wiley and Sons, West Sussex, UK (2008) 10.1002/9780470754085Suche in Google Scholar
14 F.-W.Bach, K.Möhwald, T.Bause: Untersuchung der Einflüsse von Substratrauheit und Spritzpartikelgröße auf die Haftung thermisch gespritzter Schichten, Materialwissenschaft und Werkstofftechnik39 (2008), pp. 45–4710.1002/mawe.200700221Suche in Google Scholar
15 S.Amada, T.Hirose: Influence of grit blasting pre-treatment on the adhesion strength of plasma sprayed coatings: Fractal analysis of roughness, Surface and Coatings Technology102 (1998), pp. 132–13710.1016/S0257-8972(97)00628-2Suche in Google Scholar
16 J.Sickfeld: Pull-off test, an internationally standardized method for adhesion testing – Assessment of the relevance of test results, K. L.Mittal (Ed.): Adhesion Aspects of Polymeric Coatings SE – 32, Springer, New York, USA (1983), pp. 543–56710.1007/978-1-4613-3658-7_32Suche in Google Scholar
17 L. W.Meyer: Werkstoffverhalten Band 004: Erfassung und Beschreibung des skalierten Fließ-, Verfestigungs- und Versagensverhaltens ausgewählter metallischer Werkstoffe, Eigenverlag TU Chemnitz, Chemnitz, Germany (2008)Suche in Google Scholar
18 F.Ghadami, M. H.Sohi, S.Ghadami: Effect of bond coat and post-heat treatment on the adhesion of air plasma sprayed WC-Co coatings, Surface and Coatings Technololy261 (2015), pp. 289–29410.1016/j.surfcoat.2014.11.016Suche in Google Scholar
19 U.Rietz, D.Lerche, S.Hielscher, U.Beck: Determination of bonding and adhesive strength by means of the centrifuge technology, In-cosmetics (2014), http://www.in-cosmetics.com/_novadocuments/19960?v=634940995363030000, accessed: 17-Mar-2015Suche in Google Scholar
© 2015, Carl Hanser Verlag, München
Artikel in diesem Heft
- Inhalt/Contents
- Inhalt
- Fachbeiträge/Technical Contributions
- Adhesive tensile testing of atmospheric plasma sprayed zinc coating on a 1.4301 substrate
- Fatigue strength of nodular cast iron with regard to heavy-wall applications
- Mechanical and corrosion properties of friction stir welded joints of Al-Cu alloy 2219-T87
- The effect of using heat treated ulexite and cashew in automotive friction materials
- Residual stress relaxation in welded large components
- Variation regulation of the acoustic emission energy parameter during the failure process of granite under uniaxial compression
- Iznik tiles: A new production technology and respective characterization
- Quality during milling of a glass fiber reinforced polymer composite
- Effect of abrasive water jet turning process parameters on surface roughness and material removal rate of AISI 1050 steel
- Influence of cutting parameters on the chip-tool interface temperature during the turning of Waspaloy
- Effects of the thixocasting injection velocity on tensile properties of an A357 Al alloy
- Solid mold investment casting – A replication process for open-cell foam metal production
- Design of an impact testing machine for polymer films by the free falling dart procedure
- Mechanical and electrical properties of Sb-Ga50Au10In40 alloys
- CFD simulation of particulate flow in a spiral concentrator
Artikel in diesem Heft
- Inhalt/Contents
- Inhalt
- Fachbeiträge/Technical Contributions
- Adhesive tensile testing of atmospheric plasma sprayed zinc coating on a 1.4301 substrate
- Fatigue strength of nodular cast iron with regard to heavy-wall applications
- Mechanical and corrosion properties of friction stir welded joints of Al-Cu alloy 2219-T87
- The effect of using heat treated ulexite and cashew in automotive friction materials
- Residual stress relaxation in welded large components
- Variation regulation of the acoustic emission energy parameter during the failure process of granite under uniaxial compression
- Iznik tiles: A new production technology and respective characterization
- Quality during milling of a glass fiber reinforced polymer composite
- Effect of abrasive water jet turning process parameters on surface roughness and material removal rate of AISI 1050 steel
- Influence of cutting parameters on the chip-tool interface temperature during the turning of Waspaloy
- Effects of the thixocasting injection velocity on tensile properties of an A357 Al alloy
- Solid mold investment casting – A replication process for open-cell foam metal production
- Design of an impact testing machine for polymer films by the free falling dart procedure
- Mechanical and electrical properties of Sb-Ga50Au10In40 alloys
- CFD simulation of particulate flow in a spiral concentrator
