The Investigation of Graphite Distribution on Diffusion Bonding of the AISI 1030 Low Carbon Steel with Nodular Cast Iron
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Ugur Caligulu
Abstract
The joining of Nodular Cast Iron with the conventional methods presents many problems due to the presence of high carbon content and low ductility. Therefore it is necessary to use heat treatment or to take some precautions before and after bonding. In this study, the graphite distribution on both sides of the interface of diffusion bonding of the AISI 1030 low carbon steel with Nodular Cast Iron was investigated. In order to observe the behavior of the graphite nodules in diffusion bonding, AISI 1030 was used as the comparison of alloy. Diffusion bonding experiments were carried out in an argon atmosphere at the temperatures of 900–950 and 1000 °C and 15 MPa under a dynamic load for 50–100 and 150 min. holding times. The properties of microstructure and graphite distribution that formed in the interface zone of the joints were examined by optic microscope, SEM, EDS, and X-Ray analysis. The hardness values from the interface were measured with the HV hardness scale. The strength of the joint was tested by lap-shear tests. The result of all observations indicated a homogenous graphite distribution. On the other hand, as a function of the process temperature elevation, an increase in the amount of graphite atoms that migrated towards the interface and a decrease in the nodule diameters were observed.
Kurzfassung
Das Verbinden von Gusseisen mit Kugelgraphit mittels konventioneller Verfahren bringt aufgrund des hohen Kohlenstoffgehaltes und der niedrigen Duktilität viele Schwierigkeiten mit sich. Daher ist es notwendig, eine Wärmebehandlung durchzuführen oder andere Vorkehrungen vor oder nach dem Fügen zu treffen. Für die diesem Beitrag zugrunde liegende Studie wurde die Graphitverteilung auf beiden Seiten der Grenzfläche beim Diffusionsverbinden des kohlenstoffarmen Stahles AISI 1030 mit Kugelgraphit-Gusseisen untersucht. Um das Verhalten des Kugelgrphits während des Bonding-Prozesses zu beobachten, wurde der Stahl AISI als Vergleichswerkstoff verwendet. Die Bonding-Versuche wurden in einer Argon-Atmosphäre bei Temperaturen von 900, 950 und 1000 °C und einer dynamischen Beanspruchung mit 15 MPa bei Haltezeiten von 50, 100 und 150 min. durchgeführt. Die mikrostrukturellen Eigenschaften und die Graphitverteilung an der Grenzfläche der der Verbindungen wurden mittels Lichtmikroskop, REM, EDS und Röntgenanalyse untersucht. Ebenso wurde die Vickershärte bestimmt. Die Festigkeit der Verbindung wurde mit Scherversuchen geprüft. Im Ergebnis aller Untersuchungen zeigte sich eine homogene Graphitverteilung, eine Zunahme der Anzahl von Kohlenstoffatomen, die in Richtung der Grenzfläche migrierten, und eine Abnahme des Durchmessers der Graphitkugeln.
References
1 N.Ozdemir, C.Ozek: An investigation on machinability of Nodular Cast Iron by WEDM, International Journal of Advanced Manufacturing Technology288 (2006), pp. 869–87210.1007/s00170-004-2446-3Suche in Google Scholar
2 M.Taskin, A.Orhan, R.Samur: Investigation of the effect of temperature on the bonding in TLP diffusion bonding of Nodular Cast Iron with a Cu interlayer, Proc. of the 10th International Materials Symposium, Denizli (2004), pp. 478–482Suche in Google Scholar
3 M. M.Yildirim, M.Pakdil, Z. S.Dogantan, A.Cakan: Engineering Materials I, Mustafa Kemal Univ. Publication, No. 9, Iskenderun, Turkey (2001)Suche in Google Scholar
4 M.Taskin, S.Ozan, S.Kolukisa: The effect of the process temperature on the bondability in diffusion bonding of AISI 430 with Nodular Cast Iron, Practical Metallography43 (2006), No. 6, pp. 293–305Suche in Google Scholar
5 S.Ozan, M.Taskin, S.Kolukisa: The effect of the process temperature on the bondability in transient liquid pahse (TLP) diffusion bonding of AISI 430 ferritic stainless steel with Nodular (spheroid) Cast Iron using a Copper interlayer, Practical Metallography43 (2006), No. 11, pp. 575–585Suche in Google Scholar
6 A.Sunwoo: Diffusion bonding of Al alloy 8090, Scripta Metall. Mater.31 (1994), No. 4, pp. 407–41210.1016/0956-716X(94)90009-4Suche in Google Scholar
7 N.Ozdemir, M.Aksoy, N.Orhan: Effect of Graphite Shape in Vacuum-Free Diffusion Bonding of Nodular Cast Iron with Gray Cast Iron, Journal of Materials Processing Technology, 141 (2003) pp. 228–23310.1016/S0924-0136(03)00154-7Suche in Google Scholar
8 H.Kejanli, M.Taksin, S.Kolukisa, P.Topuz: Transient liquid phase (TLP) diffusion bonding of Ti P/M components using Cu interlayer Ti45Ni49Cu6, Int J Adv Manuf Tech.44 (2009), pp. 695–69910.1007/s00170-008-1860-3Suche in Google Scholar
9 C. S.Lee, H.Li, R. S.Chandel: Vacuum-free diffusion bonding of Aluminum metal matrix composite, Journal of Material Process Technology89–90 (1999), pp. 326–33010.1016/S0924-0136(99)00144-2Suche in Google Scholar
10 H.Kejanli, U.Caligulu, S.Kolukisa: The investigation of the effect of the joining temperature and period on the Cu-Ni foils diffusion bonding at 910-940-970 °C Temperatures of Ti45.2Ni49.1Cu5.7 composite, e-Journal of New World Sciences Academy3 (2008), No. 3, pp. 515–523Suche in Google Scholar
11 M.Taskin, H.Dikbas, U.Caligulu: Artificial neural network (ANN) approach to prediction of diffusion bonding behavior (shear strength) of Ni-Ti Alloys manufactured by powder metallurgy method, Mathematical and Computational Applications13 (2008), No. 3, pp. 183–191Suche in Google Scholar
12 M.Taskin, U.Caligulu, H.Dikbas: Artificial neural network (ANN) approach to prediction of diffusion bonding behavior (shear strength) of SiCp reinforced metal matrix composites, e-Journal of Yasar University12 (2008), No. 3, pp. 1811–1825Suche in Google Scholar
13 G.Garmong, N. E.Paton, A. S.Argon: Attainment of full interfacial contact during diffusion bonding, Met. Trans.6A (1975), pp. 1269–1279Suche in Google Scholar
14 I.Dutta, M. W.Chen, K.Peterson, T.Shultz: Plastic deformation and interfacial sliding in Al and Cu thin film: Si substrate systems due to thermal cycling, J. Electron. Mater. P. (2001), p. 1537–1548Suche in Google Scholar
15 K. A.Peterson; C.Park, I.Dutta: Interfacial sliding in back-end interconnect structures in microelectronic devices, Journal of Electronic Materials32 (2003), No. 10, pp. 1059–107110.1007/s11664-003-0089-zSuche in Google Scholar
16 H.Kejanli, M.Taksin, U.Caligulu: The effect on the connecting characteristic of welding temperatures on the joining with the diffusion bonding using Ni and Cu interlayer of Ni-Ti-Cu composites manufactured by powder metallurgy method, e-Journal of New World Sciences Academy3 (2008), No. 4, pp. 556–568Suche in Google Scholar
17 Y.Takahashi, K.Inoue, K.Nishiguchi: A new model for diffusion bonding and its application to duplex alloys, Mater. Sci. Eng. A271 (1999), pp. 458–46810.1016/S0921-5093(99)00315-9Suche in Google Scholar
18 S.Güleç, A.Aran: Material Science, Tubitak Publications, Gebze, (1986)Suche in Google Scholar
19 R. A.Bushey: Welding of Cast Irons, ASM Hand Book6 (1993)10.31399/asm.hb.v06.a0001435Suche in Google Scholar
20 M.Aydın: TR2002 02710 U Patented Diffusion Bonding Machine, Department of Machine Engineering, Faculty of Engineering, University of Dumlipinar, Kutahya, Turkey (2002)Suche in Google Scholar
21 H.Kejanli: Investigation of Ni-Ti-Cu alloys compatibility that produced dust metallurgy method with liquid phase diffusion welding, PhD Thesis, Elazig (2007)Suche in Google Scholar
22 A.Ozel: Importance and properties of austempered Nodular Cast Irons, 4th Materials Seymposium, Denizli (1991), pp. 307–316Suche in Google Scholar
23 G. E.Dieter: Mechanical Metallurgy, McGraw-Hill, USA, (1986)Suche in Google Scholar
24 W. D.Callister Jr: Materials Science and Engineering: An Introduction, Wiley, USA (2000)10.1108/acmm.2000.12847aae.001Suche in Google Scholar
© 2011, Carl Hanser Verlag, München
Artikel in diesem Heft
- Inhalt/Contents
- Inhalt
- Fachbeiträge/Technical Contributions
- DIN EN ISO 6892-1:2009 Der Zugversuch — Erste Erfahrungen aus der praktischen Umsetzung der neuen Norm*
- EN ISO 6892-1:2009 Tensile Testing: Initial Experience from the Practical Implementation of the New Standard*
- Weld Metal Grain Refinement of Aluminium Alloy 5083 through Controlled Additions of Ti and B
- TIG Riveting of Temperature Sheath Microprobe
- Einfluss der Mikrostruktur auf den Druck- und Zug-E-Modul teilkristalliner Kunststoffe
- A Novel Approach for Quantitative Measurement of the Slag Penetration Area in Refractories by Using Computer Aided Image Analysis
- Effects of Thermal Oxidation and Subsequent Pickling on Pitting Geometry of Austentitic Stainless Steels in Chloride Solutions
- Plasmagestützte Ionisations-spektroskopie (PGIS) zur Materialanalyse
- Arbeitswalzen aus Keramik zum Walzen von dünnen Stahlfolien im 20-Walzen-Sendzimirgerüst
- Magnesium Applications for Fuel Economy and Energy Production
- The Investigation of Graphite Distribution on Diffusion Bonding of the AISI 1030 Low Carbon Steel with Nodular Cast Iron
- Kalender/Calendar
- Kalender
- Vorschau/Preview
- Vorschau
Artikel in diesem Heft
- Inhalt/Contents
- Inhalt
- Fachbeiträge/Technical Contributions
- DIN EN ISO 6892-1:2009 Der Zugversuch — Erste Erfahrungen aus der praktischen Umsetzung der neuen Norm*
- EN ISO 6892-1:2009 Tensile Testing: Initial Experience from the Practical Implementation of the New Standard*
- Weld Metal Grain Refinement of Aluminium Alloy 5083 through Controlled Additions of Ti and B
- TIG Riveting of Temperature Sheath Microprobe
- Einfluss der Mikrostruktur auf den Druck- und Zug-E-Modul teilkristalliner Kunststoffe
- A Novel Approach for Quantitative Measurement of the Slag Penetration Area in Refractories by Using Computer Aided Image Analysis
- Effects of Thermal Oxidation and Subsequent Pickling on Pitting Geometry of Austentitic Stainless Steels in Chloride Solutions
- Plasmagestützte Ionisations-spektroskopie (PGIS) zur Materialanalyse
- Arbeitswalzen aus Keramik zum Walzen von dünnen Stahlfolien im 20-Walzen-Sendzimirgerüst
- Magnesium Applications for Fuel Economy and Energy Production
- The Investigation of Graphite Distribution on Diffusion Bonding of the AISI 1030 Low Carbon Steel with Nodular Cast Iron
- Kalender/Calendar
- Kalender
- Vorschau/Preview
- Vorschau