A Novel Approach for Quantitative Measurement of the Slag Penetration Area in Refractories by Using Computer Aided Image Analysis
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Cem Emre Kurban
Abstract
The Crucible Method is a standard method to determine the corrosion between slag and refractory. According to this method refractory samples are heated to experimental temperature with the active slag powder inside the crucible. The aim of the experiment is to corrode the refractory by slag penetration and cutting the refractory to analyze the corroded surface to determine the slag-refractory interaction. In this study, this method was used and supported by a computer aided surface analyze system which recently has several application areas in material science. The image of the corroded surface of the refractory was transferred to a computer. Image settings and calibrations of complex shaped slag penetration areas were done by Photoshop. Quantitative analysis was done by MVH-ImagePCv7 image analysis software. It was found that the qualitative and quantitative analysis of the Crucible Method was enhanced by the help of computer aided surface display and image analysis techniques.
Kurzfassung
Die sogenannte Crucible Method (Schmelztiegelverfahren) ist ein Standardverfahren, um die Korrosion zwischen Schlacke und feuerfesten Materialien zu untersuchen. Entsprechend diesem Test wurden für die diesem Beitrag zugrunde liegende Studie Proben aus feuerfesten Materialien auf die Experimenttemperatur mit dem aktiven Schlackepulver innerhalb des Schmelztiegels erhitzt. Das Ziel dieses Versuches ist es, das feuerfeste Material durch Eindringen von Schlacke zu korrodieren und dann das feuerfeste Material zu zerschneiden, um die korrodierte Oberfläche hinsichtlich der Wechselwirkung zwischen der Schlacke und dem feuerfesten Material zu analysieren. In der Studie wurde dieses Verfahren zusammen mit einem computergestützten Oberflächenanalyse-System angewendet, das kürzlich in verschiedenen Bereichen der Materialwissenschaften angewendet wurde. Die Bildbearbeitung und die Kalibrierung der komplex geformten Bereiche der eingedrungenen Schlacke wurden mittels Photoshop realisiert. Die quantitative Analyse wurde mit der Software MVH-ImagePCv7 ausgeführt. Es stellte sich heraus, dass die qualitative und die quantitative Analyse mit dem Schmelztiegelverfahren mit der computergestützten Darstellung der Oberfläche und den enstprechenden Bildanalysetechniken erheblich verbessert werden kann.
References
1 S.Yilmaz: Corrosion of high alumina spinel castables by steel ladle slag, Ironmaking and Steelmaking33 (2006), pp. 151–15610.1179/174328106X80109Search in Google Scholar
2 S.Yilmaz: Vergleich zwischen MgO-C-Steinen und MgO-AlO3-Spinellgießmassen als Verschleißfutter für Stahlgießpfannen, Kerami-sche Zeitschrift51 (1999), pp. 636–638Search in Google Scholar
3 Y. K.Kalpakli, S.Yilmaz: Effect of Magnesia addition on physical properties and slag attack resistance of ultra-low cement castables (ULC), Can. Metall. Quar.48 (2009), pp. 177–18610.1179/000844309794239071Search in Google Scholar
4 E.Yilmaz, S.Yilmaz: Investigation of properties of the boehmitic sol coated graphite added alumina-low cement castables, J. Ceram. Process. Res.11 (2010), pp. 56–60Search in Google Scholar
5 Y. K.Kalpakli: Comparative study for physical properties and corrosion mechanism of synthetic and in situ MgAl2O4 spinel formation zero cement refractory castables, Ironmaking and Steelmaking37 (2010), pp. 414–42410.1179/030192309X12506804200546Search in Google Scholar
6 H.J.Klischat, H.Liever, H.Wirsing: Alkali-resistant linings for the security and preheating zones in rotary cement and lime kilns subject to chemical attack, ZKG Int.55 (2002), pp. 66–72Search in Google Scholar
7 H.Sorpoolaky, S. W.Zhang, B. B.Argent, W. E.Lee: Influence of grain phase on slag corrosion of low-cement castable refractories, J. Amer. Ceram. Soc.84 (2001), pp. 426–43410.1111/j.1151-2916.2001.tb00672.xSearch in Google Scholar
8 E.Prestes, A.S.Chinelatto, A.W.D.Resende: Slag attack resistance of castable refractories for the short rotary furnace of secondary lead smelting application, Ind. Ceram.28 (2008), pp. 213–220 (special issue)Search in Google Scholar
9 W.Yan, N.Li, B.Q.Han: Influence of Microsilica Content on the Slag Resistance of Castables Containing Porous Corundum-Spinel Aggregates, Int. J. App. Ceram. Tech.5 (2008), pp. 633–64010.1111/j.1744-7402.2008.02240.xSearch in Google Scholar
10 M. H.Amin, A.Kazemzadeh, M.Amin-Ebrahimabadi, N.Saha-Chaudhury, V.Sahajwalla: Interactions of magnesia castables used in steelmaking with calcium aluminate slag, Ind. Ceram.28 (2008), pp. 125–132 (special issue)Search in Google Scholar
11 Z. H.Huang, W.Pan, W. D.Xue, R. G.Sun, Y. R.Hong: Corrosion behavior of BF slag to SiAlON-Al2O3-SiC composite refractories, Rare Metal Mat. Eng.34 (2005), pp. 532–535Search in Google Scholar
12 S.Karamoutsos, I. E.Alexopoulou, D.Papanastassiou, D. C.Papamantellos: Study of the effect of Hellenic diasporic bauxite addition on blast furnace operations, Steel Res Int.75 (2004), pp. 157–162Search in Google Scholar
13 M.Rivenet, N.Ruchaud, J.C.Boivin, F.Abraham, P.Hubert: A basic gunning material interfaces study, J. Euro Ceram Soc20 (2000), pp. 1645–165110.1016/S0955-2219(00)00024-8Search in Google Scholar
14 C. F.Chan, B. B.Argent, W.Lee: EInfluence of additives on slag resistance of Al2O3-SiO2-SiC-C refractory bond phases under reducing atmosphere, J. Amer Ceram Soc81 (1998), pp. 3177–318810.1111/j.1151-2916.1998.tb02754.xSearch in Google Scholar
15 X.M.Yang, D.B.Huang, L.T.Kong, T. J.Yang, Y. S.Xie, D. G.Wang: Kinetics of reduction of iron oxide in CaO-SiO2-Al2O3-FeO slags with graphite powder, J. Iron Steel Res Int5 (1998), pp. 21–27Search in Google Scholar
16 M.A.L.Braulio, A.G.Tomba Martinez, A.P.Luz, C.Liebske, V.C.Pandolfelli: Basic slag attack of spinel-containing refractory castables, Ceramics International37 (2011), pp. 1935–194510.1016/j.ceramint.2011.02.007Search in Google Scholar
17 A.P.Luz, A.G.Tomba Martinez, M.A.L.Braulio, V.C.Pandolfelli: Thermodynamic evaluation of spinel containing refractory castables corrosion by secondary metallurgy slag, Ceramics International37 (2011), pp. 1191–120110.1016/j.ceramint.2010.11.043Search in Google Scholar
18 L.A.Diaz, R.Torrecillas, A.H.de Aza, P.Pena: Effect of spinel content on slag attack resistance of high alumina refractory castables, Journal of the European Ceramic Society27 (2007), pp. 4623–463110.1016/j.jeurceramsoc.2007.04.007Search in Google Scholar
19 S.Mukhopadhyay, P.K.Das Poddar: Effect of preformed and in situ spinels on microstructure and properties of a low cement refractory castable, Ceramics International30 (2004), pp. 369–38010.1016/S0272-8842(03)00117-2Search in Google Scholar
20 DIN 51069-2: Testing of ceramic materials; comparing test of the resistance of refractory bricks to the attack of solid and liquid materials at high temperature, crucible methodSearch in Google Scholar
21 C. E.Kurban, E.Erzi, S.Yilmaz: Determination of slag penetration area using computer aided surface image analysis, Proc. of the 2nd Int. Conference on Ceramics – ICC2, Verona, 29 June-3 July 2008Search in Google Scholar
22 Adobe® Photoshop® CS2, Image processing softwareSearch in Google Scholar
23 MVH-ImagePCv7, Free Image analysis software: http://mvh.sr.unh.edu/software/software.htm (date of visit: 10.03.2011)Search in Google Scholar
© 2011, Carl Hanser Verlag, München
Articles in the same Issue
- Inhalt/Contents
- Inhalt
- Fachbeiträge/Technical Contributions
- DIN EN ISO 6892-1:2009 Der Zugversuch — Erste Erfahrungen aus der praktischen Umsetzung der neuen Norm*
- EN ISO 6892-1:2009 Tensile Testing: Initial Experience from the Practical Implementation of the New Standard*
- Weld Metal Grain Refinement of Aluminium Alloy 5083 through Controlled Additions of Ti and B
- TIG Riveting of Temperature Sheath Microprobe
- Einfluss der Mikrostruktur auf den Druck- und Zug-E-Modul teilkristalliner Kunststoffe
- A Novel Approach for Quantitative Measurement of the Slag Penetration Area in Refractories by Using Computer Aided Image Analysis
- Effects of Thermal Oxidation and Subsequent Pickling on Pitting Geometry of Austentitic Stainless Steels in Chloride Solutions
- Plasmagestützte Ionisations-spektroskopie (PGIS) zur Materialanalyse
- Arbeitswalzen aus Keramik zum Walzen von dünnen Stahlfolien im 20-Walzen-Sendzimirgerüst
- Magnesium Applications for Fuel Economy and Energy Production
- The Investigation of Graphite Distribution on Diffusion Bonding of the AISI 1030 Low Carbon Steel with Nodular Cast Iron
- Kalender/Calendar
- Kalender
- Vorschau/Preview
- Vorschau
Articles in the same Issue
- Inhalt/Contents
- Inhalt
- Fachbeiträge/Technical Contributions
- DIN EN ISO 6892-1:2009 Der Zugversuch — Erste Erfahrungen aus der praktischen Umsetzung der neuen Norm*
- EN ISO 6892-1:2009 Tensile Testing: Initial Experience from the Practical Implementation of the New Standard*
- Weld Metal Grain Refinement of Aluminium Alloy 5083 through Controlled Additions of Ti and B
- TIG Riveting of Temperature Sheath Microprobe
- Einfluss der Mikrostruktur auf den Druck- und Zug-E-Modul teilkristalliner Kunststoffe
- A Novel Approach for Quantitative Measurement of the Slag Penetration Area in Refractories by Using Computer Aided Image Analysis
- Effects of Thermal Oxidation and Subsequent Pickling on Pitting Geometry of Austentitic Stainless Steels in Chloride Solutions
- Plasmagestützte Ionisations-spektroskopie (PGIS) zur Materialanalyse
- Arbeitswalzen aus Keramik zum Walzen von dünnen Stahlfolien im 20-Walzen-Sendzimirgerüst
- Magnesium Applications for Fuel Economy and Energy Production
- The Investigation of Graphite Distribution on Diffusion Bonding of the AISI 1030 Low Carbon Steel with Nodular Cast Iron
- Kalender/Calendar
- Kalender
- Vorschau/Preview
- Vorschau