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A Novel Approach for Quantitative Measurement of the Slag Penetration Area in Refractories by Using Computer Aided Image Analysis

  • Cem Emre Kurban , Eray Erzi and Suat Yilmaz
Published/Copyright: May 26, 2013
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Abstract

The Crucible Method is a standard method to determine the corrosion between slag and refractory. According to this method refractory samples are heated to experimental temperature with the active slag powder inside the crucible. The aim of the experiment is to corrode the refractory by slag penetration and cutting the refractory to analyze the corroded surface to determine the slag-refractory interaction. In this study, this method was used and supported by a computer aided surface analyze system which recently has several application areas in material science. The image of the corroded surface of the refractory was transferred to a computer. Image settings and calibrations of complex shaped slag penetration areas were done by Photoshop. Quantitative analysis was done by MVH-ImagePCv7 image analysis software. It was found that the qualitative and quantitative analysis of the Crucible Method was enhanced by the help of computer aided surface display and image analysis techniques.

Kurzfassung

Die sogenannte Crucible Method (Schmelztiegelverfahren) ist ein Standardverfahren, um die Korrosion zwischen Schlacke und feuerfesten Materialien zu untersuchen. Entsprechend diesem Test wurden für die diesem Beitrag zugrunde liegende Studie Proben aus feuerfesten Materialien auf die Experimenttemperatur mit dem aktiven Schlackepulver innerhalb des Schmelztiegels erhitzt. Das Ziel dieses Versuches ist es, das feuerfeste Material durch Eindringen von Schlacke zu korrodieren und dann das feuerfeste Material zu zerschneiden, um die korrodierte Oberfläche hinsichtlich der Wechselwirkung zwischen der Schlacke und dem feuerfesten Material zu analysieren. In der Studie wurde dieses Verfahren zusammen mit einem computergestützten Oberflächenanalyse-System angewendet, das kürzlich in verschiedenen Bereichen der Materialwissenschaften angewendet wurde. Die Bildbearbeitung und die Kalibrierung der komplex geformten Bereiche der eingedrungenen Schlacke wurden mittels Photoshop realisiert. Die quantitative Analyse wurde mit der Software MVH-ImagePCv7 ausgeführt. Es stellte sich heraus, dass die qualitative und die quantitative Analyse mit dem Schmelztiegelverfahren mit der computergestützten Darstellung der Oberfläche und den enstprechenden Bildanalysetechniken erheblich verbessert werden kann.


Cem Emre Kurban, born 1981, graduated in 2008 from Istanbul University, at the Metallurgical and Materials Engineering Department.

Dr. Eray Erzi, born 1978, took the BSc degree in 2001, the MSc degree in 2003, and the PhD degree in 2011 at the Istanbul University, Metallurgical and Materials Engineering Department. He is working at the same university as a research assistant since 2001.

Prof. Dr. Suat Yilmaz, born 1968, took the BSc degree, the MSc degree, and the PhD degree at the Istanbul Technical University, Metallurgical and Materials Engineering Department in 1989, 1992, and 1998 respectively. He is working at the same department at the Istanbul University as a full professor since 2001.


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Published Online: 2013-05-26
Published in Print: 2011-10-01

© 2011, Carl Hanser Verlag, München

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