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A single-crystal investigation of the solid solution NiB48.5 of β-rhombohedral boron type structure
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August 25, 2010
Abstract
A solid solution of nickel in β-rhombohedral boron of composition NiB48.5 has been investigated using X-ray single-crystal diffractometry. The space group is R[unk]m (No. 166) and the hexagonal unit cell dimensions a = 10.9615(5) Å and c = 23.8544(7) Å. The boron atoms occupy 16 atomic positions, of which two are partially occupied. The nickel atoms are distributed on four partially occupied atomic positions with occupancies ranging from 0.58% to 44.7%. The conventional R value was 2.9%, based on 3434 non-equivalent reflections with a positive net intensity (no sigma restriction, 87 reflections with as measured negative intensities excluded).
Published Online: 2010-08-25
Published in Print: 1984
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- Crystal structure of Te(OH)6 ·2KNO3 ·2H2O: an addition compound of telluric acid
- Die Kristallstrukturen von KCo(CO)4 und RbCo(CO)4
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