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The crystal structure of manganese(II) succinate tetrahydrate
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August 25, 2010
Abstract
The crystal structure of manganese(II) succinate tetrahydrate, Mn(C4H4O4) · 4H2O, has been determined from single crystal X-ray diffraction data. The crystals are triclinic, space group P[unk] with a = 5.50(1), b = 9.05(2), c = 5.26(1) Å, α = 96.1(5), β = 98.9(5), γ = 120.5(5)°, Z = 1. The structure was solved by the heavy-atom method and refined to a final R-value of 0.11 for all the 501 observed reflexions. The Mn2+ ion is coordinated with six oxygen atoms with distances ranging from 2.18 to 2.24 Å. Both the carboxyl groups in the succinate anion are twisted out of the plane of the four carbon atoms by 7.7°.
Published Online: 2010-8-25
Published in Print: 1983-1-1
© 2015 Oldenbourg Wissenschaftsverlag GmbH, Rosenheimer Str. 145, 81671 München
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Articles in the same Issue
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- The crystal structure of C.I. Pigment Yellow 3, α-(1-hydroxyethylidene)-2-chloro-acetanilide-α-azo-(4′-chloro-2′-nitrobenzene)
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- Effects of symmetry and atomic heterogeneity on X-ray intensities – a case of hypercentric distribution*
- Refinement of a partially disordered natrolite, Na2Al2Si3O10 · 2H2O
- The crystal structures of 1-(3′,5′-dinitrobenzoyloxy)-bicyclo[3.3.1]-9-oxanonane and 5-(3′,5′-dinitrobenzoyloxy)-cyclooctanone1
- The crystal structure of methoxymethoxy-2,4-dinitrobenzene1
- The crystal structure of 2-(3′,5′-dinitrobenzoyloxy)-tetrahydropyran Cyclohexane Solvate1
- The crystal structure of 2-(N-phthalimidomethoxy)-tetrahydropyran1
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