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Röntgenaufnahmen mit der Buergerschen Präzessionskamera bei Temperaturen zwischen 1000°C und 2000°C
Published/Copyright:
July 28, 2010
Abstract
Single crystal photographs at temperatures between 1000°C and 2000°C using a Buerger precession camera can be obtained by heating the crystal with a small gas flame. The temperature of exposure may be controlled by gas pressure and gas flow (pressure regulator and needle valve). Advantages and disadvantages of the device are discussed.
X-ray exposures at high temperatures of anorthite (CaAl2Si2O8) demonstrate the application of the apparatus. The lattice angle α* and the intensity ratios of some reflections show a continuous change at temperatures between 300°C and 1400°C.
Published Online: 2010-07-28
Published in Print: 1963-12
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Articles in the same Issue
- Structure defects in kaolinite
- Dehydration of goethite and diaspore*
- Contributions to the crystal chemistry of normal and defect tetrahedral structures*
- The crystal and molecular structure of a synthetic imidazo-purine
- The crystal structure of the anhydrous cadmium and mercuric sulfates
- The crystal structure of dimethyl sulfone
- Hydrogen bonding and conformations in echitamine salts
- Ein einfacher Heizaufsatz für die Präzessionskamera
- Röntgenaufnahmen mit der Buergerschen Präzessionskamera bei Temperaturen zwischen 1000°C und 2000°C
- Die Kristallstruktur des Phenols
- Crystal structure of bis-(hydrazine)manganese(II) chloride
- On the crystal structure of biotites
- A three-dimensional refinement of crystalline structure of trioxane*
- Über die Orientierung des durch Erhitzen aus Manganit entstehenden Pyrolusits
