Phase stability analysis of shocked ammonium dihydrogen phosphate by X-ray and Raman scattering studies

Sivakumar Aswathappa; Arumugam Saranraj; Sahaya Jude Dhas Sathiyadhas; Kondaviti Showrilu; Martin Britto Dhas Sathiyadhas Amalapushpam

doi:10.1515/zkri-2020-0072

Article

Phase stability analysis of shocked ammonium dihydrogen phosphate by X-ray and Raman scattering studies

Sivakumar Aswathappa , Arumugam Saranraj , Sahaya Jude Dhas Sathiyadhas , Kondaviti Showrilu and Martin Britto Dhas Sathiyadhas Amalapushpam

Published/Copyright: December 18, 2020

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From the journal Zeitschrift für Kristallographie - Crystalline Materials Volume 236 Issue 1-2

Abstract

Impact of shock waves on non-linear optical materials bring about a lot of unknown behaviors of materials and such kinds of shock wave recovery experiments are highly required for the better understanding of material-property relationship. In the present context, we have performed experiments on the impact of structural properties of ammonium dihydrogen phosphate (ADP) samples under shock wave loaded conditions and the results of the test samples have been evaluated by X-ray diffraction (XRD), Raman spectroscopy, diffused reflectance spectroscopy (DRS) and field emission scanning electron microscopic (FESEM) technique. Interestingly, prismatic face of ADP shows loss of degree of crystallinity whereas pyramidal face shows enhancement of crystalline nature with respect to number of shock pulses due to shock wave induced dynamic re-crystallization. Hence, the present problem is worthy enough to unearth and understand the anisotropic nature of the ADP crystal and their structural modifications at shock wave loaded conditions.

Keywords: ADP crystal; dynamic re-crystallization; shock waves; structural defects

Corresponding author: Martin Britto Dhas Sathiyadhas Amalapushpam, Department of Physics, Abdul Kalam Research Center, Sacred Heart College, Tirupattur, Vellore, Tamil Nadu, 635 601, India, E-mail: martinbritto@shctpt.edu

Author contribution: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.
Research funding: None declared.
Conflict of interest statement: The authors declare no conflicts of interest regarding this article.

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Received: 2020-08-06

Accepted: 2020-11-20

Published Online: 2020-12-18

Published in Print: 2021-02-23

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https://doi.org/10.1515/zkri-2020-0072

Keywords for this article

ADP crystal; dynamic re-crystallization; shock waves; structural defects