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An experimental investigation of flame retardancy and thermal stability of treated and untreated kenaf fiber reinforced epoxy composites

  • Nivedhitha Durgam Muralidharan , Jeyanthi Subramanian , Sathish Kumar Rajamanickam EMAIL logo and Venkatachalam Gopalan
Published/Copyright: November 1, 2023
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Abstract

Natural fiber reinforced polymeric composites perform poor in mechanical and thermal properties at elevated temperatures due to the cellulose and hemicellulose contents of natural fiber start degrading at elevated temperature. In this research work, flame retardancy and thermal stability of treated and untreated kenaf fiber reinforced epoxy composites have been experimentally investigated and reported. Two composite laminates, one with 6 % NaOH Alkali treated and another with untreated woven kenaf mats, were fabricated by hand lay-up technique followed by compression molding with 40 % fiber weight fractions. Flame retardancy test and various thermal characteristics studies such as thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), heat deflection temperature (HDT), and morphological analysis via scanning electron microscopy (SEM) tests were carried out. The results showed that alkali treated kenaf fiber composite achieved V0 fire retardancy grade. The major weight losses, 86 % and 75.5 % for untreated and treated composites respectively were recorded between 300 °C and 450 °C. 13.6 % increase in HDT was noted for treated composite with 0.25 mm deflection at 0.45 MPa pressure condition. Thus the composite laminate with 6 % NaOH alkali-treated kenaf fiber achieved the best thermal stability with less degradation which is more suitable for automobile and aerospace applications.


Corresponding author: Sathish Kumar Rajamanickam, Department of Automobile Engineering, Hindustan Institute of Technology and Science, Chennai 603103, Tamil Nadu, India, E-mail:

Acknowledgments

The authors are grateful to VIT Chennai for providing the seed fund and fully operational laboratory for carrying out the experiments.

  1. Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.

  2. Competing interests: The authors declare no conflicting financial/personal interest regarding this article.

  3. Research funding: No funding declared.

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Received: 2023-06-15
Accepted: 2023-09-29
Published Online: 2023-11-01
Published in Print: 2023-11-27

© 2023 Walter de Gruyter GmbH, Berlin/Boston

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