Startseite Effect of screw configuration on the dispersion of nanofillers in thermoset polymers
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Effect of screw configuration on the dispersion of nanofillers in thermoset polymers

  • Gangadhar Angadi , Hebbale NarayanaRao Narasimha Murthy EMAIL logo , Sridhar Ramakrishna , Salim Firdosh , Raghavendra Nagappa und Krishna Munishamaiah
Veröffentlicht/Copyright: 5. Oktober 2017
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Abstract

This paper deals with the study of screw configuration for dispersing nanofillers in thermoset polymers using an intermesh co-rotating twin screw extruder. The influence of kneading elements on the dispersion of nanoclay in epoxy was examined using 10 different screw configurations. Nanoclay was dispersed in epoxy at a barrel temperature of 5°C and a screw speed of 100 rpm. The combination of right hand kneading block and three/four lobed kneading blocks resulted in uniform dispersion of nanofiller. Positive staggered angle with right hand kneading elements yielded uniform dispersion of the nanofiller. Mechanical properties of epoxy nanocomposites processed with these configurations were better than those of neat epoxy. Excessive shear was associated with four lobed kneading block (4KB)/4KB configuration and hence degradation of polymers leading to shorter chains, whereas inadequate shearing in neutral kneading block (NKB)/NKB configuration led to agglomerations. These observations were evidenced by scanning electron microscopy (SEM) and X-ray diffraction (XRD).

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Received: 2015-10-19
Accepted: 2016-12-23
Published Online: 2017-10-5
Published in Print: 2017-10-26

©2017 Walter de Gruyter GmbH, Berlin/Boston

Heruntergeladen am 3.12.2025 von https://www.degruyterbrill.com/document/doi/10.1515/polyeng-2015-0427/pdf
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