Hydride formation mechanisms in Zr-containing amorphous alloys during sample preparation and atom probe tomography
-
Chetarpa Yipyintum
Chetarpa Yipyintum is a PhD student in Advanced Material Analysis Research Unit, Department of Metallurgical Engineering, Chulalongkorn University, Bangkok, Thailand.
Ji Yeong Lee is working at Advanced Analysis Center, Korea Institute of Science and Technology, Seoul, Korea.
Jin-Yoo Suh is a PI at Center for Energy Materials Research, Korea Institute of Science and Technology, Seoul, Korea.
Boonrat Lohwongwatana is an Associate Professor in Biomedical Engineering Research Center, Chulalongkorn University, Bangkok, Thailand.
Abstract
Hydride formation in Zr-containing amorphous alloys as an experimental artifact was investigated utilizing atom probe tomography, transmission electron microscopy, and focused ion beam with normal and cryogenic conditions. The amount of hydrogen existing in the atom probe specimens decreased significantly by utilizing focused ion beam milling under cryogenic condition. Also, the formation of hydride was confirmed by diffraction pattern analysis in the remaining tip of the specimen after the atom probe tomography experiment. With those collected pieces of evidence, sources of hydrogen in the atom probe tomography were discussed.
Funding source: National Research Council of Science and Technology
Award Identifier / Grant number: CAP-18-04-KRISS
Funding source: Thailand Research Fund
Award Identifier / Grant number: RRI PHD56I0045
Funding source: Northwestern University
Award Identifier / Grant number: DMR-0420532
Award Identifier / Grant number: N00014-0400798
Award Identifier / Grant number: N00014-0610539
Award Identifier / Grant number: N00014-0910781
Award Identifier / Grant number: N00014-1712870
Award Identifier / Grant number: NSF DMR-1720139
Award Identifier / Grant number: NSF ECCS-1542205
About the authors
Chetarpa Yipyintum is a PhD student in Advanced Material Analysis Research Unit, Department of Metallurgical Engineering, Chulalongkorn University, Bangkok, Thailand.
Ji Yeong Lee is working at Advanced Analysis Center, Korea Institute of Science and Technology, Seoul, Korea.
Jin-Yoo Suh is a PI at Center for Energy Materials Research, Korea Institute of Science and Technology, Seoul, Korea.
Boonrat Lohwongwatana is an Associate Professor in Biomedical Engineering Research Center, Chulalongkorn University, Bangkok, Thailand.
Acknowledgment
A preliminary experiment of atom-probe tomography was performed at the Northwestern University Center for Atom-Probe Tomography (NUCAPT). The LEAP tomograph at NUCAPT was purchased and upgraded with grants from the NSF-MRI (DMR-0420532) and ONR-DURIP (N00014-0400798, N00014-0610539, N00014-0910781, N00014-1712870) programs. NUCAPT received support from the MRSEC program (NSF DMR-1720139) at the Materials Research Center, the SHyNE Resource (NSF ECCS-1542205), and the Initiative for Sustainability and Energy (ISEN) at Northwestern University.
-
Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.
-
Research funding: This work was supported by the Korea Institute of Science and Technology from the National Research Council of Science & Technology (NST) under grant No. CAP-18-04-KRISS, Research and Researchers for Industries (RRI) under grant PHD56I0045.
-
Conflict of interest statement: The authors declare no conflicts of interest regarding this article.
References
[1] H. P. van Leeuwen, “Non-uniform hydrogen distributions in notched delayed failure specimens,” Mater. Test., vol. 16, no. 9, pp. 263–269, 1974, https://doi.org/10.1515/mt-1974-160904.Suche in Google Scholar
[2] M. Türker, “Diffusible hydrogen content in submerged arc welds of a S960 type steel,” Mater. Test., vol. 58, no. 6, pp. 561–568, 2016, https://doi.org/10.3139/120.110891.Suche in Google Scholar
[3] T. Lai, H. Yin, and M. Lind, “The hydrogen permeability of Cu-Zr binary amorphous metallic membranes and the importance of thermal stability,” J. Membr. Sci., vol. 489, pp. 264–269, 2015, https://doi.org/10.1016/j.memsci.2015.03.098.Suche in Google Scholar
[4] S. N. Paglieri, N. K. Pal, M. D. Dolan et al.., “Hydrogen permeability, thermal stability and hydrogen embrittlement of Ni–Nb–Zr and Ni–Nb–Ta–Zr amorphous alloy membranes,” J. Membr. Sci., vol. 378, no. 1, pp. 42–50, 2011, https://doi.org/10.1016/j.memsci.2011.04.049.Suche in Google Scholar
[5] S. Rubanov and P. R. Munroe, “FIB-induced damage in silicon,” J. Microsc., vol. 214, no. 3, pp. 213–221, 2004, https://doi.org/10.1111/j.0022-2720.2004.01327.x.Suche in Google Scholar PubMed
[6] M. Andrzejczuk, T. Płociński, W. Zieliński, and K. j. Kurzydłowski, “TEM characterization of the artefacts induced by FIB in austenitic stainless steel,” J. Microsc., vol. 237, no. 3, pp. 439–442, 2010, https://doi.org/10.1111/j.1365-2818.2009.03288.x.Suche in Google Scholar PubMed
[7] J. Belz, A. Beyer, T. Torunski, W. Stolz, and K. Volz, “Direct investigation of (sub-) surface preparation artifacts in GaAs based materials by FIB sectioning,” Ultramicroscopy, vol. 163, pp. 19–30, 2016, https://doi.org/10.1016/j.ultramic.2016.01.001.Suche in Google Scholar PubMed
[8] H. J. Chang, E. S. Park, Y. C. Kim, and D. H. Kim, “Observation of artifact-free amorphous structure in Cu–Zr-based alloy using transmission electron microscopy,” Mater. Sci. Eng. A, vol. 406, no. 1, pp. 119–124, 2005, https://doi.org/10.1016/j.msea.2005.06.017.Suche in Google Scholar
[9] S. M. Hanlon, S. Y. Persaud, F. Long, A. Korinek, and M. R. Daymond, “A solution to FIB induced artefact hydrides in Zr alloys,” J. Nucl. Mater., vol. 515, pp. 122–134, 2019, https://doi.org/10.1016/j.jnucmat.2018.12.020.Suche in Google Scholar
[10] M. C. Dolph and C. Santeufemio, “Exploring cryogenic focused ion beam milling as a Group III–V device fabrication tool,” Nucl. Instrum. Methods Phys. Res. B, vol. 328, pp. 33–41, 2014, https://doi.org/10.1016/j.nimb.2014.02.126.Suche in Google Scholar
[11] A. McMinn, E. C. Darby, and J. S. Schofield, “The terminal solid solubility of hydrogen in zirconium alloys,” in Zirconium in the Nuclear Industry: Twelfth International Symposium, pp. 173–195, 2000, https://doi.org/10.1520/STP14300S.Suche in Google Scholar
[12] E. Zuzek, J. P. Abriata, A. San-Martin, and F. D. Manchester, “The H-Zr (hydrogen-zirconium) system,” Bull. Alloy Phase Diagr., vol. 11, no. 4, pp. 385–395, 1990, https://doi.org/10.1007/BF02843318.Suche in Google Scholar
[13] S.-D. Kim, J.-S. Kim, and J. Yoon, “Phase analysis of hydride blister in zirconium alloy,” J. Alloys Compd., vol. 735, pp. 2007–2011, 2018, https://doi.org/10.1016/j.jallcom.2017.11.359.Suche in Google Scholar
[14] K. Thompson, D. Lawrence, D. J. Larson, J. D. Olson, T. F. Kelly, and B. Gorman, “In situ site-specific specimen preparation for atom probe tomography,” Ultramicroscopy, vol. 107, no. 2, pp. 131–139, 2007, https://doi.org/10.1016/j.ultramic.2006.06.008.Suche in Google Scholar PubMed
[15] X. Wang, R.-Z. Qiu, Y.-J. Xian, Y.-T. Zhang, P.-C. Liu, and P.-C. Zhang, “New insight into the intrinsic instability of fcc ZrH2 by energy-resolved local bonding analysis,” RSC Adv., vol. 6, no. 23, pp. 19150–19154, 2016, https://doi.org/10.1039/C5RA27103G.Suche in Google Scholar
[16] J. O. Fadonougbo, J.-Y. Suh, C.-H. Shim, G.-H. Kim, E. Fleury, and Y. W. Cho, “Nanometer-scale phase separation and formation of delta ZrH2 in Cu-Zr binary amorphous alloys,” J. Alloys Compd., vol. 721, pp. 646–652, 2017, https://doi.org/10.1016/j.jallcom.2017.06.012.Suche in Google Scholar
[17] G. Sha, H. M. Zhu, J. W. Liu, C. P. Luo, Z. W. Liu, and S. P. Ringer, “Hydrogen-induced decomposition of Zr-rich cores in an Mg−6Zn−0.6Zr−0.5Cu alloy,” Acta Mater., vol. 60, no. 15, pp. 5615–5625, 2012, https://doi.org/10.1016/j.actamat.2012.07.001.Suche in Google Scholar
[18] Y.-J. Kim and D. N. Seidman, “Atom-probe tomographic analyses of hydrogen interstitial atoms in ultrahigh purity niobium,” Microsc. Microanal., vol. 21, no. 3, pp. 535–543, 2015, https://doi.org/10.1017/S143192761500032X.Suche in Google Scholar PubMed
[19] B. Gault, M. P. Moody, J. M. Cairney, and S. P. Ringer, Atom Probe Microscopy, 2012th ed. New York, Springer, 2012.10.1007/978-1-4614-3436-8Suche in Google Scholar
[20] B.-M. Lee and B.-J. Lee, “A comparative study on hydrogen diffusion in amorphous and crystalline metals using a molecular dynamics simulation,” Metall. Mater. Trans. A, vol. 45, no. 6, pp. 2906–2915, 2014, https://doi.org/10.1007/s11661-014-2230-4.Suche in Google Scholar
[21] T. Twiehaus, S. Olschok, and U. Reisgen, “Influence of residual oxygen during laser beam welding under vacuum,” Mater. Test., vol. 64, no. 7, pp. 945–953, 2022, https://doi.org/10.1515/mt-2021-2183.Suche in Google Scholar
[22] R. Ding and I. P. Jones, “In situ hydride formation in titanium during focused ion milling,” J. Electron Microsc., vol. 60, no. 1, pp. 1–9, 2011, https://doi.org/10.1093/jmicro/dfq066.Suche in Google Scholar PubMed
[23] J. D. Wnuk, J. M. Gorham, S. G. Rosenberg et al.., “Electron induced surface reactions of the organometallic precursor trimethyl-(methylcyclopentadienyl)platinum(IV),” J. Phys. Chem. C, vol. 113, no. 6, pp. 2487–2496, 2009, https://doi.org/10.1021/jp807824c.Suche in Google Scholar
[24] F. Yan, I. Mouton, L. T. Stephenson et al.., “Atomic-scale investigation of hydrogen distribution in a TiMo alloy,” Scr. Mater., vol. 162, pp. 321–325, 2019, https://doi.org/10.1016/j.scriptamat.2018.11.040.Suche in Google Scholar
[25] G. J. C. Carpenter, J. A. Jackman, J. P. McCaffrey, and R. Alani, “In situ hydride formation in zirconium and titanium during ion milling,” Microsc. Microanal., vol. 1, no. 4, pp. 175–184, 1995, https://doi.org/10.1017/S1431927695111757.Suche in Google Scholar
[26] G. J. C. Carpenter, “The precipitation of γ-zirconium hydride in zirconium,” Acta Metall., vol. 26, no. 8, pp. 1225–1235, 1978, https://doi.org/10.1016/0001-6160(78)90006-8.Suche in Google Scholar
[27] S. C. Lumley, R. W. Grimes, S. T. Murphy et al.., “The thermodynamics of hydride precipitation: the importance of entropy, enthalpy and disorder,” Acta Mater., vol. 79, pp. 351–362, 2014, https://doi.org/10.1016/j.actamat.2014.07.019.Suche in Google Scholar
[28] R. P. Kolli, “Controlling residual hydrogen gas in mass spectra during pulsed laser atom probe tomography,” Adv. Struct. Chem. Imag., vol. 3, no. 1, p. 10, 2017, https://doi.org/10.1186/s40679-017-0043-4.Suche in Google Scholar PubMed PubMed Central
[29] Y. Chang, A. J. Breen, Z. Tarzimoghadam et al.., “Characterizing solute hydrogen and hydrides in pure and alloyed titanium at the atomic scale,” Acta Mater., vol. 150, pp. 273–280, 2018, https://doi.org/10.1016/j.actamat.2018.02.064.Suche in Google Scholar
[30] H. Sato and S. Zaefferer, “A study on the formation mechanisms of butterfly-type martensite in Fe–30% Ni alloy using EBSD-based orientation microscopy,” Acta Mater., vol. 57, no. 6, pp. 1931–1937, 2009, https://doi.org/10.1016/j.actamat.2008.12.035.Suche in Google Scholar
© 2023 Walter de Gruyter GmbH, Berlin/Boston
Artikel in diesem Heft
- Frontmatter
- Effect of alloying elements on mechanical behaviour of Cu-Zn-Sn bronzes
- Effects of boron waste as a reinforcement in the production of Al composite foams
- Buckling in rectangular hybrid composite plates with angled groove-shaped cut-outs
- Experimental and numerical investigation of crashworthiness performance for optimal automobile structures using response surface methodology and oppositional based learning differential evolution algorithm
- Effects of deep cryogenic treatment with different holding times on the mechanical properties of Al 7050-T7451 alloy friction stir welding
- Additive manufacturing and characterization of a stainless steel and a nickel alloy
- Shear strain rate sensitivity and crystallisation kinetics investigation in melt spun Cu64Zr36 binary metallic glass
- Microstructure analysis, constitutive relationship, and processing map of novel pre-aged Mg-Zn-Gd-Er alloy with different deformation ranges
- Effects of process parameters on strengthening mechanisms of additively manufactured AlSi10Mg
- Comparison of notch fabrication methods on the impact strength of FDM-3D-printed PLA specimens
- Hydride formation mechanisms in Zr-containing amorphous alloys during sample preparation and atom probe tomography
- Taper connection strength of revision heads with adapter sleeves compared to standard heads made of ceramics
- Investigation of glass/epoxy laminate composites reinforced with bio-particles under mechanical loading
- Nondestructive microstructural characterization of austempered ductile iron
Artikel in diesem Heft
- Frontmatter
- Effect of alloying elements on mechanical behaviour of Cu-Zn-Sn bronzes
- Effects of boron waste as a reinforcement in the production of Al composite foams
- Buckling in rectangular hybrid composite plates with angled groove-shaped cut-outs
- Experimental and numerical investigation of crashworthiness performance for optimal automobile structures using response surface methodology and oppositional based learning differential evolution algorithm
- Effects of deep cryogenic treatment with different holding times on the mechanical properties of Al 7050-T7451 alloy friction stir welding
- Additive manufacturing and characterization of a stainless steel and a nickel alloy
- Shear strain rate sensitivity and crystallisation kinetics investigation in melt spun Cu64Zr36 binary metallic glass
- Microstructure analysis, constitutive relationship, and processing map of novel pre-aged Mg-Zn-Gd-Er alloy with different deformation ranges
- Effects of process parameters on strengthening mechanisms of additively manufactured AlSi10Mg
- Comparison of notch fabrication methods on the impact strength of FDM-3D-printed PLA specimens
- Hydride formation mechanisms in Zr-containing amorphous alloys during sample preparation and atom probe tomography
- Taper connection strength of revision heads with adapter sleeves compared to standard heads made of ceramics
- Investigation of glass/epoxy laminate composites reinforced with bio-particles under mechanical loading
- Nondestructive microstructural characterization of austempered ductile iron
