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Synthesis of nickel oxide nanoparticles as an agent for antibacterial and wastewater remediation applications by calcination

  • Ayşegül Şenocak ORCID logo EMAIL logo , Rızvan İmamoğlu ORCID logo and Sefa Yılmaz ORCID logo
Published/Copyright: February 15, 2023
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International Journal of Materials Research
From the journal International Journal of Materials Research Volume 114 Issue 3

Abstract

In this paper, a nickel complex with the general formula [Ni(HST)(OAc)] (HST: 1-salicylaldehydethiosemicarbazone, OAc: acetate) was subjected to thermal decomposition to produce nanoparticles at three different temperatures. The semiconductor nanoparticles have a particle size of 22.18 nm and a band gap of 2.68 eV. Furthermore, it was observed that the nanoparticles exhibiting a zeta-potential value of −26.1 are stable in colloidal media. The produced nanoparticles have the potential to be used as wastewater treatment agents under optimized conditions, as evidenced by the photocatalytic activity on methylene blue degradation with a 69.30% decomposition. Although all the synthesized compounds exhibit high antibacterial activity with low minimal inhibitory concentration values, the nanoparticles obtained by calcination at 400 °C had the highest activity, which is consistent with the literature.

Keywords: Methylene blue degradation; Nanostructures; Schiff bases; Semiconductor; Solid-state thermal decomposition
Corresponding author: Ayşegül Şenocak, Department of Chemistry, Collage of Art and Science, Tokat Gaziosmanpaşa University, 60240, Tokat, Türkiye, E-mail:

  1. Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.

  2. Research funding: None declared.

  3. Conflict of interest statement: The authors declare no conflicts of interest regarding this article.

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Received: 2022-06-02
Accepted: 2022-10-07
Published Online: 2023-02-15
Published in Print: 2023-03-28

© 2023 Walter de Gruyter GmbH, Berlin/Boston

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https://doi.org/10.1515/ijmr-2022-0260
Keywords for this article
Methylene blue degradation; Nanostructures; Schiff bases; Semiconductor; Solid-state thermal decomposition

Articles in the same Issue

  1. Frontmatter
  2. Original Papers
  3. Modeling the band gap of spinel nano-ferrite material using a genetic algorithm based support vector regression computational method
  4. Influence of surfactant concentration on structural properties and corrosion behaviour of electrodeposited Ni–SiO2 nanocomposite coatings
  5. Synthesis of RGO/γ-Fe2O3 nanocomposite for the removal of heavy metals from aqueous solutions
  6. Synthesis of nickel oxide nanoparticles as an agent for antibacterial and wastewater remediation applications by calcination
  7. Synthesis and efficient electrocatalytic performance of Bi2O3/Dy2O3 nanoflakes
  8. Finite element assisted self-consistent simulations to capture texture heterogeneity during hot compression
  9. Improving mechanical properties of additive manufactured AZ31 by mechanical rolling
  10. News
  11. DGM – Deutsche Gesellschaft für Materialkunde
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