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Analysis of Nitrofuran Metabolites in Food by High-Performance Liquid Chromatography with Tandem Mass Spectrometry Detection

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Published/Copyright: June 1, 2005
Clinical Chemistry and Laboratory Medicine (CCLM)
From the journal Volume 41 Issue 12

Abstract

A reliable and sensitive procedure is presented for the analysis of nitrofuran metabolite residues in foods of animal origin, like poultry and shrimp. The method is based on a one-step extraction/derivatization, followed by solid-phase extraction clean-up with polymeric phase cartridges. The separations were carried out by liquid chromatography coupled with tandem mass spectroscopy detection.

Results from the full validation of the procedure and from a survey of food available from the Swiss market, with the analysis of 236 samples of shrimp, poultry, fish and rabbit, are presented and demonstrate that this method is satisfactory in order to control nitrofuran residues in foods of animal origin.

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Published Online: 2005-06-01
Published in Print: 2003-12-04

Copyright © 2003 by Walter de Gruyter GmbH & Co. KG

Articles in the same Issue

  1. Author Index
  2. Subject Index
  3. Contents
  4. Mass Spectrometry in Laboratory Medicine
  5. Mass Spectrometry-Based Proteomics: Current Status and Potential Use in Clinical Chemistry
  6. Application of Gas Chromatography-Mass Spectrometry for Analysis of Isoprostanes: Their Role in Cardiovascular Disease
  7. The Application of Clinical Proteomics to Cancer and other Diseases
  8. Therapeutic Drug Monitoring of 13 Antidepressant and Five Neuroleptic Drugs in Serum with Liquid Chromatography-Electrospray Ionization Mass Spectrometry
  9. Mass Spectrometric Analysis of Human Transferrin in Different Body Fluids
  10. Profiling and in vivo Quantification of Proteins by High Resolution Mass Spectrometry: The Example of Goserelin, an Analogue of Luteinizing Hormone-Releasing Hormone
  11. Determination of Nicotine and Its Major Metabolite Cotinine in Plasma or Serum by Gas Chromatography-Mass Spectrometry Using Ion-Trap Detection
  12. Analysis of Nitrofuran Metabolites in Food by High-Performance Liquid Chromatography with Tandem Mass Spectrometry Detection
  13. Automated LC-MS Method for the Fast Stereoselective Determination of Methadone in Plasma
  14. Proteome Analysis of Diseased Joints from Mice Suffering from Collagen-Induced Arthritis
  15. Quantitative Analysis of Bile Acids in Human Plasma by Liquid Chromatography-Electrospray Tandem Mass Spectrometry: A Simple and Rapid One-Step Method
  16. Organic Acids in the Second Morning Urine in a Healthy Swiss Paediatric Population
  17. Acknowledgement
  18. Meetings and Awards
https://doi.org/10.1515/CCLM.2003.244

Articles in the same Issue

  1. Author Index
  2. Subject Index
  3. Contents
  4. Mass Spectrometry in Laboratory Medicine
  5. Mass Spectrometry-Based Proteomics: Current Status and Potential Use in Clinical Chemistry
  6. Application of Gas Chromatography-Mass Spectrometry for Analysis of Isoprostanes: Their Role in Cardiovascular Disease
  7. The Application of Clinical Proteomics to Cancer and other Diseases
  8. Therapeutic Drug Monitoring of 13 Antidepressant and Five Neuroleptic Drugs in Serum with Liquid Chromatography-Electrospray Ionization Mass Spectrometry
  9. Mass Spectrometric Analysis of Human Transferrin in Different Body Fluids
  10. Profiling and in vivo Quantification of Proteins by High Resolution Mass Spectrometry: The Example of Goserelin, an Analogue of Luteinizing Hormone-Releasing Hormone
  11. Determination of Nicotine and Its Major Metabolite Cotinine in Plasma or Serum by Gas Chromatography-Mass Spectrometry Using Ion-Trap Detection
  12. Analysis of Nitrofuran Metabolites in Food by High-Performance Liquid Chromatography with Tandem Mass Spectrometry Detection
  13. Automated LC-MS Method for the Fast Stereoselective Determination of Methadone in Plasma
  14. Proteome Analysis of Diseased Joints from Mice Suffering from Collagen-Induced Arthritis
  15. Quantitative Analysis of Bile Acids in Human Plasma by Liquid Chromatography-Electrospray Tandem Mass Spectrometry: A Simple and Rapid One-Step Method
  16. Organic Acids in the Second Morning Urine in a Healthy Swiss Paediatric Population
  17. Acknowledgement
  18. Meetings and Awards
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