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Structural determination of a lead-lithium monophosphate, LiPbPO4

Published/Copyright: August 25, 2010
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Zeitschrift für Kristallographie
From the journal Zeitschrift für Kristallographie Volume 188 Issue 1-2

Abstract

The crystal structure of lead-lithium monophosphate has been solved by single crystal X-ray techniques. The cell constants are: a = 7.945(6), b = 18.46(2), c = 4.928(4) Å, Pna21, Z = 8. The least squares refinement leads to a final R value of 0.032 for 1315 reflections. The three-dimensional framework built up by LiO4 and PO4 sharing vertice tetrahedra aligned in the same c direction is a non-common arrangement. The Pb atoms are distributed in the polyhedral cavities of this polar framework.

Published Online: 2010-08-25
Published in Print: 1989

Articles in the same Issue

  1. Structure of 2,10-dibromo-3-chloro-7R,8S-epoxychamigrene
  2. Structural determination of a lead-lithium monophosphate, LiPbPO4
  3. Reciprocal lattice scan modes in single crystal diffractometry: a reexamination for cases of mineralogical interest
  4. Experimental charge density in polythionate anions: II. X-ray study of the electron density distribution in potassium tetrathionate, K2S4O6
  5. An uncommon Cu[2+4]O6 coordination polyhedron in the crystal structure of KCu3(OH)2[(AsO4)H(AsO4)] (with a comparison to related structure types)
  6. Some aspects of information theory and phase problem: Effect of heavy atoms on information content in P[unk]
  7. The crystal structure of hexaaquacopper(II) bis(7-oxabicyclo[2.2.1]heptane-2,3-dicarboxylato)cuprate(II)
  8. Crystal and molecular structure of an isostere of purine ring system: 7-benzylamino-2-methylmercaptothiazolo [5,4-d] pyrimidine
  9. A novel form of molybdenum (V) phosphate: δ-KMo2P3O13
  10. Structure cristalline et moléculaire du camphosulfonate de l'α-(tétrahydro-4,5,6,7 thiéno (3,2-c) pyridyl-5) (chloro-2 phényl)-acétate de méthyle, C26H32NO6S2Cl. Configuration absolue
  11. Verfeinerung der Kristallstruktur von Holmquistit vom Brandrücken/Weinebene, Koralpe, Österreich
  12. Structural relationships of zeolite frameworks: “5-ring zeolites”
  13. Symmetry restrictions on minimal surfaces related by the Bonnet-transformation
  14. Crystal and molecular structure of N-p-fluorobenzoyl-l-valine
  15. Thermal decay of laser-induced long living metastable electronic states in Na2[Fe(CN)5NO] · 2H2O single crystals
  16. Crystal structures of three substituted ammonium hexachlororhenates(IV)
https://doi.org/10.1524/zkri.1989.188.1-2.5

Articles in the same Issue

  1. Structure of 2,10-dibromo-3-chloro-7R,8S-epoxychamigrene
  2. Structural determination of a lead-lithium monophosphate, LiPbPO4
  3. Reciprocal lattice scan modes in single crystal diffractometry: a reexamination for cases of mineralogical interest
  4. Experimental charge density in polythionate anions: II. X-ray study of the electron density distribution in potassium tetrathionate, K2S4O6
  5. An uncommon Cu[2+4]O6 coordination polyhedron in the crystal structure of KCu3(OH)2[(AsO4)H(AsO4)] (with a comparison to related structure types)
  6. Some aspects of information theory and phase problem: Effect of heavy atoms on information content in P[unk]
  7. The crystal structure of hexaaquacopper(II) bis(7-oxabicyclo[2.2.1]heptane-2,3-dicarboxylato)cuprate(II)
  8. Crystal and molecular structure of an isostere of purine ring system: 7-benzylamino-2-methylmercaptothiazolo [5,4-d] pyrimidine
  9. A novel form of molybdenum (V) phosphate: δ-KMo2P3O13
  10. Structure cristalline et moléculaire du camphosulfonate de l'α-(tétrahydro-4,5,6,7 thiéno (3,2-c) pyridyl-5) (chloro-2 phényl)-acétate de méthyle, C26H32NO6S2Cl. Configuration absolue
  11. Verfeinerung der Kristallstruktur von Holmquistit vom Brandrücken/Weinebene, Koralpe, Österreich
  12. Structural relationships of zeolite frameworks: “5-ring zeolites”
  13. Symmetry restrictions on minimal surfaces related by the Bonnet-transformation
  14. Crystal and molecular structure of N-p-fluorobenzoyl-l-valine
  15. Thermal decay of laser-induced long living metastable electronic states in Na2[Fe(CN)5NO] · 2H2O single crystals
  16. Crystal structures of three substituted ammonium hexachlororhenates(IV)
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