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Crystal and molecular structure of an isostere of purine ring system: 7-benzylamino-2-methylmercaptothiazolo [5,4-d] pyrimidine
Veröffentlicht/Copyright:
25. August 2010
Abstract
The crystal and molecular structure of the title compound has been established by means of the X-ray diffraction method on a single crystal using MoKα radiation. The crystals are monoclinic, space group P21/a with a = 8.745(2), b = 13.230(8), c = 11.729(2) Å, β = 94.06(2)°. The structure was solved by the heavy-atom method, and refined by full-matrix least squares to a final R value of 0.035 with 1787 ‘observed’ reflections. The five- and six-membered ring are planar and inclined to one another at 0.9°. In the five-membered ring the average C – S bond distance is 1.75 Å and the C – S – C angle is 87.9°.
Published Online: 2010-08-25
Published in Print: 1989
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- Structure of 2,10-dibromo-3-chloro-7R,8S-epoxychamigrene
- Structural determination of a lead-lithium monophosphate, LiPbPO4
- Reciprocal lattice scan modes in single crystal diffractometry: a reexamination for cases of mineralogical interest
- Experimental charge density in polythionate anions: II. X-ray study of the electron density distribution in potassium tetrathionate, K2S4O6
- An uncommon Cu[2+4]O6 coordination polyhedron in the crystal structure of KCu3(OH)2[(AsO4)H(AsO4)] (with a comparison to related structure types)
- Some aspects of information theory and phase problem: Effect of heavy atoms on information content in P[unk]
- The crystal structure of hexaaquacopper(II) bis(7-oxabicyclo[2.2.1]heptane-2,3-dicarboxylato)cuprate(II)
- Crystal and molecular structure of an isostere of purine ring system: 7-benzylamino-2-methylmercaptothiazolo [5,4-d] pyrimidine
- A novel form of molybdenum (V) phosphate: δ-KMo2P3O13
- Structure cristalline et moléculaire du camphosulfonate de l'α-(tétrahydro-4,5,6,7 thiéno (3,2-c) pyridyl-5) (chloro-2 phényl)-acétate de méthyle, C26H32NO6S2Cl. Configuration absolue
- Verfeinerung der Kristallstruktur von Holmquistit vom Brandrücken/Weinebene, Koralpe, Österreich
- Structural relationships of zeolite frameworks: “5-ring zeolites”
- Symmetry restrictions on minimal surfaces related by the Bonnet-transformation
- Crystal and molecular structure of N-p-fluorobenzoyl-l-valine
- Thermal decay of laser-induced long living metastable electronic states in Na2[Fe(CN)5NO] · 2H2O single crystals
- Crystal structures of three substituted ammonium hexachlororhenates(IV)
Artikel in diesem Heft
- Structure of 2,10-dibromo-3-chloro-7R,8S-epoxychamigrene
- Structural determination of a lead-lithium monophosphate, LiPbPO4
- Reciprocal lattice scan modes in single crystal diffractometry: a reexamination for cases of mineralogical interest
- Experimental charge density in polythionate anions: II. X-ray study of the electron density distribution in potassium tetrathionate, K2S4O6
- An uncommon Cu[2+4]O6 coordination polyhedron in the crystal structure of KCu3(OH)2[(AsO4)H(AsO4)] (with a comparison to related structure types)
- Some aspects of information theory and phase problem: Effect of heavy atoms on information content in P[unk]
- The crystal structure of hexaaquacopper(II) bis(7-oxabicyclo[2.2.1]heptane-2,3-dicarboxylato)cuprate(II)
- Crystal and molecular structure of an isostere of purine ring system: 7-benzylamino-2-methylmercaptothiazolo [5,4-d] pyrimidine
- A novel form of molybdenum (V) phosphate: δ-KMo2P3O13
- Structure cristalline et moléculaire du camphosulfonate de l'α-(tétrahydro-4,5,6,7 thiéno (3,2-c) pyridyl-5) (chloro-2 phényl)-acétate de méthyle, C26H32NO6S2Cl. Configuration absolue
- Verfeinerung der Kristallstruktur von Holmquistit vom Brandrücken/Weinebene, Koralpe, Österreich
- Structural relationships of zeolite frameworks: “5-ring zeolites”
- Symmetry restrictions on minimal surfaces related by the Bonnet-transformation
- Crystal and molecular structure of N-p-fluorobenzoyl-l-valine
- Thermal decay of laser-induced long living metastable electronic states in Na2[Fe(CN)5NO] · 2H2O single crystals
- Crystal structures of three substituted ammonium hexachlororhenates(IV)
