Gas chromatography/mass spectrometry techniques for the characterisation of organic materials in works of art

References

[1] Nadolny J. The first century of published scientific analyses of the materials of historical painting and polychromy, circa 1780–1880. Rev Conservation. 2003;4:39–51.10.1179/sic.2003.48.Supplement-1.39Search in Google Scholar

[2] Masschelein-Kleiner L. Perspectives de la chimie des liants picturaux anciens. Bulletin (Institut Royal du Patrimoine Artistique/Koninklijk Instituut voor het Kunstpatrimonium). 1963;6:109–26.Search in Google Scholar

[3] Mills JS. The gas chromatographic examination of paint media. Part I, Fatty acid composition and identification of dried oil films. Stud Conserv. 1966;11:92–108.10.2307/1505447Search in Google Scholar

[4] Arpino P, Moreau J-P, Oruezabal C, Flieder F. Gas chromatographic-mass spectrometric analysis of tannin hydrolysates from the ink of ancient manuscripts (XIth to XVIth century). J Chromatogr. 1977;134:433–9.10.1016/S0021-9673(00)88542-8Search in Google Scholar

[5] Mills J, White R. Organic mass-spectrometry of art materials: work in progress. Natl Gallery Tech Bull. 1982;6:3–18.Search in Google Scholar

[6] Weiss NR, Biemann K. Application of mass spectrometric techniques to the differentiation of paint media. In: Brommelle N, Smith P, editors. Conservation and restoration of pictorial art. London: Butterworths, 1976: 88–92.Search in Google Scholar

[7] Kałużna-Czaplińska J, Rosiak A, Kwapińska M, Kwapiński W. Different analytical procedures for the study of organic residues in archeological ceramic samples with the use of gas chromatography-mass spectrometry. Crit Rev Anal Chem. 2016;46:67–81.10.1080/10408347.2015.1008130Search in Google Scholar PubMed

[8] Evershed R. Organic residue analysis in archaeology: the archaeological biomarker revolution. Archaeometry. 2008;50:895–924.10.1111/j.1475-4754.2008.00446.xSearch in Google Scholar

[9] Bonaduce I, Ribechini E, Modugno F, Colombini MP. Analytical approaches based on gas chromatography mass spectrometry (GC/MS) to study organic materials in artworks and archaeological objects. Top Curr Chem. 2016;374:291–327.10.1007/978-3-319-52804-5_9Search in Google Scholar

[10] Colombini MP, Modugno F, editors. Organic mass spectrometry in art and archaeology. Chichester: John Wiley & Sons, Ltd., 2009.10.1002/9780470741917Search in Google Scholar

[11] Mills JS, White R. The organic chemistry of museum objects, 2nd ed. Oxford: Butterworth-Heinemann, 1994.Search in Google Scholar

[12] Grob RL, Barry EF, editors. Modern practice of gas chromatography, 4th ed. Hoboken: John Wiley & Sons, Inc., 2004.10.1002/0471651141Search in Google Scholar

[13] McLafferty FW, Tureček F. Interpretation of mass spectra, 4th ed. Sausalito: University Science Books, 1993.Search in Google Scholar

[14] Azemard C, Menager M, Vieillescazes C. Analysis of diterpenic compounds by GC-MS/MS: contribution to the identification of main conifer resins. Anal Bioanal Chem. 2016;408:6599–612.10.1007/s00216-016-9772-9Search in Google Scholar PubMed

[15] Kokkori M, Boon JJ, Burnstock A, McGlinchey C, Mandt P. From the streets to the canvas: on the use of bituminous asphalt in early Soviet Constructivist paintings. In: Wallert A, editor. Painting techniques: history, materials and studio practice. Amsterdam: Rijksmuseum, 2017: 280–7.Search in Google Scholar

[16] Poulin J. A new methodology for the characterisation of natural dyes on museum objects using gas chromatography-mass spectrometry. Stud Conserv. 2018;63:36–61.10.1080/00393630.2016.1271097Search in Google Scholar

[17] Gautier G, Colombini MP. GC-MS identification of proteins in wall painting samples: a fast clean-up procedure to remove copper-based pigment interferences. Talanta. 2007;73:95–102.10.1016/j.talanta.2007.03.008Search in Google Scholar PubMed

[18] Schilling M, Mazurek J. Identification of proteinaceous, oil, and plant gum binding media by quantitative GC-MS analysis: training course outline and notes. In: Sutherland K, editor. MaSC 2007 GCMS workshop handbook. Philadelphia Museum of Art, 2007:18 pp.Search in Google Scholar

[19] Van den Berg KJ, van der Horst J, Boon JJ. Recognition of copals in aged resin/oil paints and varnishes. In: Bridgland J, editor. ICOM-CC 12th Triennial Meeting, Lyon, 29 August–3 September 1999, Preprints. London: Earthscan Ltd., 1999:855–61.Search in Google Scholar

[20] Van der Doelen G, van den Berg KJ, Boon JJ. Comparative chromatographic and mass-spectrometric studies of triterpenoid varnishes: fresh material and aged samples from paintings. Stud Conserv. 1998;43:249–64.Search in Google Scholar

[21] Van den Berg KJ, Boon JJ, Pastorova I, Spetter L. Mass spectrometric methodology for the analysis of highly oxidized diterpenoid acids in Old Master paintings. J Mass Spectrom. 2000;35:512–33.10.1002/(SICI)1096-9888(200004)35:4<512::AID-JMS963>3.0.CO;2-3Search in Google Scholar PubMed

[22] Regert M, Colinart S, Degrand L, Decavallas O. Chemical alteration and use of beeswax through time: accelerated ageing tests and analysis of archaeological samples from various environmental contexts. Archaeometry. 2001;43:549–69.10.1111/1475-4754.00036Search in Google Scholar

[23] Sutherland K. Derivatisation using m-(trifluoromethyl)phenyltrimethylammonium hydroxide of organic materials in artworks for analysis by gas chromatography-mass spectrometry: unusual reaction products with alcohols. J Chromatogr A. 2007;1149:30–7.10.1016/j.chroma.2006.12.015Search in Google Scholar PubMed

[24] Lattuati-Derieux A, Ramalho O, Egasse C, Thao-Heu S, Dupont A-L. Evaluation of solid-phase microextraction on-fiber derivatization for the analysis of paper degradation compounds. e-Preservation Sci. 2015;12:38–49.Search in Google Scholar

[25] Andreotti A, Bonaduce I, Colombini MP, Gautier G, Modugno F, Ribechini E. Combined GC/MS analytical procedure for the characterization of glycerolipid, waxy, resinous, and proteinaceous materials in a unique paint microsample. Anal Chem. 2006;78:4490–500.10.1021/ac0519615Search in Google Scholar

[26] Koller J, Baumer U. An investigation of the ‘Lacquers of the West’: A methodical survey. In: Kühlenthal M, editor. Japanese and European Lacquerware. München: Karl M. Lipp Verlag, 2000:339–49.Search in Google Scholar

[27] Lluveras A, Bonaduce I, Andreotti A, Colombini MP. GC/MS analytical procedure for the characterization of glycerolipids, natural waxes, terpenoid resins, proteinaceous and polysaccharide materials in the same paint microsample avoiding interferences from inorganic media. Anal Chem. 2010;82:376–86.10.1021/ac902141mSearch in Google Scholar PubMed

[28] White R, Pilc J. Analyses of paint media. Natl Gallery Tech Bull. 1996;17:91–103.Search in Google Scholar

[29] Pitthard V, Finch P, Bayerová T. Direct chemolysis–gas chromatography–mass spectrometry for analysis of paint materials. J Sep Sci. 2004;27:200–8.10.1002/jssc.200301617Search in Google Scholar PubMed

[30] Schilling MR, Keeney J, Learner T. Characterization of alkyd paint media by gas chromatography-mass spectrometry. In: Roy A, Smith P, editors. Modern Art, New Museums: contributions to the 2004 IIC Congress, Bilbao. London: IIC, 2004: 197–201.Search in Google Scholar

[31] Izzo FC, van den Berg KJ, van Keulen H, Ferriani B, Zendri E. Modern oil paints – formulations, organic additives and degradation: some case studies. In: van den Berg KJ, Burnstock A, de Keijzer M, Krueger J, Learner T, de Tagle A, et al., editors. Issues in contemporary oil paint. Cham: Springer, 2014:75–104.10.1007/978-3-319-10100-2_5Search in Google Scholar

[32] Van den Berg JDJ, van den Berg KJ, Boon JJ. Identification of non-cross-linked compounds in methanolic extracts of cured and aged linseed oil-based paint films using gas chromatography-mass spectrometry. J Chromatogr A. 2002;950:195–211.10.1016/S0021-9673(02)00049-3Search in Google Scholar PubMed

[33] Schilling MR, Mazurek J, Learner TJS. Studies of modern oil-based artists’ paint media by gas chromatography/mass spectrometry. In: Learner TJS, editor. Modern paints uncovered. Los Angeles: Getty Conservation Institute, 2007:129–39.Search in Google Scholar

[34] Banti D, La Nasa J, Lluveras Tenorio A, Modugno F, van den Berg KJ, Lee J, et al. A molecular study of modern oil paintings: investigating the role of dicarboxylic acids in the water sensitivity of modern oil paints. RSC Adv. 2018;8:6001–12.10.1039/C7RA13364BSearch in Google Scholar

[35] Lee J, Bonaduce I, Modugno F, La Nasa J, Ormsby B, van den Berg KJ. Scientific investigation into the water sensitivity of twentieth century oil paints. Microchemical J. 2018;138:282–95.10.1016/j.microc.2018.01.017Search in Google Scholar

[36] White R, Kirby J. Rembrandt and his circle: seventeenth-century Dutch paint media re-examined. Natl Gallery Tech Bull. 1994;15:64–78.Search in Google Scholar

[37] Bonaduce I, Colombini MP. Characterisation of beeswax in works of art by gas chromatography-mass spectrometry and pyrolysis-gas chromatography-mass spectrometry procedures. J Chromatogr A. 2004;1028:297–306.10.1016/j.chroma.2003.11.086Search in Google Scholar PubMed

[38] Regert M, Langlois J, Colinart S. Characterisation of wax works of art by gas chromatographic procedures. J Chromatogr A. 2005;1091:124–36.10.1016/j.chroma.2005.07.039Search in Google Scholar PubMed

[39] Stacey R, Dyer J, Mussell C, Lluveras-Tenorio A, Colombini MP, Duce C, et al. Ancient encaustic: an experimental exploration of technology, ageing behaviour and approaches to analytical investigation. Microchemical J. 2018;138:472–87.10.1016/j.microc.2018.01.040Search in Google Scholar

[40] Languri GM, Boon JJ. Between myth and reality: on the mummy pigment from the Hafkenscheid Collection. Stud Conserv. 2005;50:161–78.10.1179/sic.2005.50.3.161Search in Google Scholar

[41] Baumer U, Dietemann P, Koller J. Identification of resinous materials on 16th and 17th century reverse-glass objects by gas chromatography/mass spectrometry. Int J Mass Spectrom. 2009;284:131–41.10.1016/j.ijms.2008.09.010Search in Google Scholar

[42] Poulin J, Helwig K. Inside amber: the structural role of succinic acid in Class Ia and Class Id resinite. Anal Chem. 2014;86:7428–35.10.1021/ac501073kSearch in Google Scholar PubMed

[43] Van der Werf ID, van den Berg KJ, Schmitt S, Boon JJ. Molecular characterization of copaiba balsam as used in painting techniques and restoration procedures. Stud Conserv. 2000;45:1–18.Search in Google Scholar

[44] White R, Kirby J. A survey of nineteenth- and early twentieth-century varnish compositions found on a selection of paintings in the National Gallery collection. Natl Gallery Tech Bull. 2001;22:64–84.Search in Google Scholar

[45] Watts S, de la Rie R. GCMS analysis of triterpenoid resins: in situ derivatization procedures using quaternary ammonium hydroxides. Stud Conserv. 2002;47:257–72.Search in Google Scholar

[46] Dietemann P, Higgitt C, Kälin M, Edelmann MJ, Knochenmuss R, Zenobi R. Aging and yellowing of triterpenoid resin varnishes – influence of aging conditions and resin composition. J Cult Heritage. 2009;10:30–40.10.1016/j.culher.2008.04.007Search in Google Scholar

[47] Colombini MP, Bonaduce I, Gautier G. Molecular pattern recognition of fresh and aged shellac. Chromatographia. 2003;58:357–64.Search in Google Scholar

[48] Sutherland K, del Río JC. Characterisation and discrimination of various types of lac resin using gas chromatography mass spectrometry techniques with quaternary ammonium reagents. J Chromatogr A. 2014;1338:149–63.10.1016/j.chroma.2014.02.063Search in Google Scholar PubMed

[49] Schilling M, Khanjian H. Gas chromatographic analysis of amino acids as ethyl chloroformate derivatives. III. Identification of proteinaceous binding media by interpretation of amino acid composition data. In: Bridgland J, editor. ICOM-CC 11th Triennial Meeting Edinburgh, 1–6 September 1996, Preprints. London: James and James, 1996: 220–7.Search in Google Scholar

[50] Chiavari G, Gandini N, Russo P, Fabbri D. Characterization of standard tempera painting layers containing proteinaceous binders by pyrolysis(/methylation)-gas chromatography-mass spectrometry. Chromatographia. 1998;47:420–6.10.1007/BF02466473Search in Google Scholar

[51] Orsini S, Parlanti F, Bonaduce I. Analytical pyrolysis of proteins in samples from artistic and archaeological objects. J Anal Appl Pyrolysis. 2017;124:643–57.10.1016/j.jaap.2016.12.017Search in Google Scholar

[52] Bleton J, Mejanelle P, Sansoulet J, Goursaud S, Tchapla A. Characterization of neutral sugars and uronic acids after methanolysis and trimethylsilylation for recognition of plant gums. J Chromatogr A. 1996;720:27–49.10.1016/0021-9673(95)00308-8Search in Google Scholar

[53] Pitthard V, Finch P. GC-MS analysis of monosaccharide mixtures as their diethyldithioacetal derivatives: application to plant gums used in art works. Chromatographia Suppl. 2001;53:S317–21.10.1007/BF02490349Search in Google Scholar

[54] Ormsby BA, Townsend JH, Singer BW, Dean JR. British watercolour cakes from the eighteenth to the early twentieth century. Stud Conserv. 2005;50:45–66.10.1179/sic.2005.50.1.45Search in Google Scholar

[55] Lluveras-Tenorio A, Mazurek J, Restivo A, Colombini MP, Bonaduce I. Analysis of plant gums and saccharide materials in paint samples: comparison of GC-MS analytical procedures and databases. Chem Cent J. 2012; 6. DOI: 10.1186/1752-153X-6-115.Search in Google Scholar PubMed

[56] Riedo C, Scalarone D, Chiantore O. Multivariate analysis of pyrolysis-GC/MS data for identification of polysaccharide binding media. Anal Methods. 2013;5:4060–7.10.1039/c3ay40474aSearch in Google Scholar

[57] Fabbri D, Chiavari G, Ling H. Analysis of anthraquinoid and indigoid dyes used in ancient artistic works by thermally assisted hydrolysis and methylation in the presence of tetramethylammonium hydroxide. J Anal Appl Pyrolysis. 2000;56:167–78.10.1016/S0165-2370(00)00092-9Search in Google Scholar

[58] Casas-Catalán MJ, Doménech Carbó MT. Identification of natural dyes used in works of art by pyrolysis-gas chromatography/mass spectrometry combined with in situ trimethylsilylation. Anal Bioanal Chem. 2005;382:259–68.10.1007/s00216-005-3064-0Search in Google Scholar PubMed

[59] Degani L, Riedo C, Gulmini M, Chiantore O. From plant extracts to historical textiles: characterization of dyestuffs by GC-MS. Chromatographia. 2014;77:1683–96.10.1007/s10337-014-2772-zSearch in Google Scholar

[60] Shedrinsky AM, Grimaldi DA, Boon JJ, Baer NS. Application of pyrolysis-gas chromatography and pyrolysis-gas chromatography/mass spectrometry to the unmasking of amber forgeries. J Anal Appl Pyrolysis. 1993;25:77–95.10.1016/0165-2370(93)80034-WSearch in Google Scholar

[61] Galletti GC, Mazzeo R. Pyrolysis/gas chromatography/mass spectrometry and Fourier-transform infrared spectroscopy of amber. Rapid Commun Mass Spectrom. 1993;7:646–50.10.1002/rcm.1290070718Search in Google Scholar

[62] Niimura N, Miyakoshi T, Onodera J, Higuchi T. Characterization of Rhus vernicifera and Rhus succedanea lacquer films and their pyrolysis mechanisms studied using two-stage pyrolysis-gas chromatography/mass spectrometry. J Anal Appl Pyrolysis. 1996;37:199–209.10.1016/0165-2370(96)00945-XSearch in Google Scholar

[63] De Witte E, Terfve A. The use of a Py-GC-MS technique for the analysis of synthetic resins. In: Brommelle NS, Thomson G, editors. Science and technology in the service of conservation: preprints of the contributions to the Washington Congress, 3–9 September 1982. London: International Institute for Conservation of Historic and Artistic Works, 1982: 16–8.Search in Google Scholar

[64] Learner T. The analysis of synthetic resins found in twentieth century paint media. In: Wright MM, Townsend JH, editors. Resins: ancient and modern. Edinburgh: Scottish Society for Conservation and Restoration, 1995: 76–84.Search in Google Scholar

[65] Learner T. The analysis of synthetic paints by pyrolysis-gas chromatography-mass spectrometry (PyGCMS). Stud Conserv. 2001;46:225–41.Search in Google Scholar

[66] La Nasa J, Orsini S, Degano I, Rava A, Modugno F, Colombini MP. A chemical study of organic materials in three murals by Keith Haring: a comparison of painting techniques. Microchemical J. 2016;124:940–8.10.1016/j.microc.2015.06.003Search in Google Scholar

[67] Defeyt C, Schilling M, Langenbacher J, Escarsega J, Rivenc R. Polyurethane coatings in twentieth century outdoor painted sculptures. Part II: comparative study of four systems by means of Py‑GC/MS. Heritage Sci. 2017;5. DOI: 10.1186/s40494-017-0129-2.Search in Google Scholar

[68] Moldoveanu SC. Analytical pyrolysis of synthetic organic polymers. Amsterdam: Elsevier B.V., 2005.Search in Google Scholar

[69] Tsuge S, Ohtani H, Watanabe C. Pyrolysis-GC/MS data book of synthetic polymers. Oxford: Elsevier, 2011.Search in Google Scholar

[70] Giachet MT, Schilling M, McCormick K, Mazurek J, Richardson E, Khanjian H, et al. Assessment of the composition and condition of animation cels made from cellulose acetate. Polym Degrad Stab. 2014;107:223–30.10.1016/j.polymdegradstab.2014.03.009Search in Google Scholar

[71] Fremout W, Verboven M, Saverwyns S. Accelerated tobacco smoke staining on waterborne acrylic paintings caused by exuding surfactants: a study with Py-GC/MS and THM-GC/MS. e-Preservation Sci. 2014;11:47–53.Search in Google Scholar

[72] Sutherland K, Schwarzinger C, Price BA. The application of pyrolysis gas chromatography mass spectrometry for the identification of degraded early plastics in a sculpture by Naum Gabo. J Anal Appl Pyrolysis. 2012;94:202–8.10.1016/j.jaap.2011.12.016Search in Google Scholar

[73] Ghelardi E, Degano I, Colombini MP, Mazurek J, Schilling M, Learner T. Py-GC/MS applied to the analysis of synthetic organic pigments: characterization and identification in paint samples. Anal Bioanal Chem. 2015;407:1415–31.10.1007/s00216-014-8370-ySearch in Google Scholar PubMed

[74] Sonoda N. Characterization of organic azo-pigments by pyrolysis-gas chromatography. Stud Conserv. 1999;44:195–208.10.1179/sic.1999.44.3.195Search in Google Scholar

[75] Bonaduce I, Andreotti A. Py-GC/MS of organic paint binders. In: Colombini MP, Modugno F, editors. Organic mass spectrometry in art and archaeology. Chichester: John Wiley & Sons, Ltd. 2009:303–26.10.1002/9780470741917.ch11Search in Google Scholar

[76] Chiavari G, Bocchini P, Galletti GC. Rapid identification of binding media in paintings using simultaneous pyrolysis methylation gas chromatography. Sci Technol Cult Heritage. 1992;1:153–8.Search in Google Scholar

[77] Schilling MR, Heginbotham A, van Keulen H, Szelewski M. Beyond the basics: A systematic approach for comprehensive analysis of organic materials in Asian lacquers. Stud Conserv. Supplementary Issue 3; 2016;61:3–27.10.1080/00393630.2016.1230978Search in Google Scholar

[78] Tamburini D, Pescitelli G, Colombini MP, Bonaduce I. The degradation of Burmese lacquer (thitsi) as observed in samples from two cultural artefacts. J Anal Appl Pyrolysis. 2017;124:51–62.10.1016/j.jaap.2017.02.023Search in Google Scholar

[79] Chiavari G, Prati S. Application of pyrolysis to the diagnostic in the artistic field. In: van Grieken R, Janssens K, Van't dack L, Meersman G, editors. Art 2002: 7th International Conference on Non-destructive Testing and Microanalysis for the Diagnostics and Conservation of the Cultural and Environmental Heritage. Antwerp: University of Antwerp, 2002:8Search in Google Scholar

[80] Wei S, Pintus V, Schreiner M. Photochemical degradation study of polyvinyl acetate paints used in artworks by Py-GC/MS. J Anal Appl Pyrolysis. 2012;97:158–63.10.1016/j.jaap.2012.05.004Search in Google Scholar PubMed PubMed Central

[81] Moffatt E, Salmon A, Poulin J, Fox A, Hay J. Characterization of varnishes on nineteenth-century Canadian furniture. J Can Assoc Conserv. 2015;40:3–18.Search in Google Scholar

[82] Pawliszyn J. Solid-phase microextraction: theory and practice. New York: Wiley-VCH, 1997.Search in Google Scholar

[83] Dyer J, Ward C, Rode N, Hacke M, Shashoua Y. Reassessment of anoxic storage of ethnographic rubber objects. In: Bridgland J, editor. ICOM-CC 16th Triennial Conference Preprints, Lisbon, 19-23 September 2011. Lisbon: Critério-Produção Grafica, Lda., 2011: 10.Search in Google Scholar

[84] Tsukada M, Rizzo A, Granzotto C. A new strategy for assessing off-gassing from museum materials: air sampling in Oddy test vessels. AIC News. 2012;37:1–7.Search in Google Scholar

[85] Desauziers V, Bourdin D, Mocho P, Plaisance H. Innovative tools and modeling methodology for impact prediction and assessment of the contribution of materials on indoor air quality. Heritage Sci. 2015;3:1–8.10.1186/s40494-015-0057-ySearch in Google Scholar

[86] Ormsby M, Johnson JS, Heald S, Chang L, Bosworth J. Investigation of solid phase microextraction sampling for organic pesticide residues on museum collections. Collection Forum. 2006;20:1–12.Search in Google Scholar

[87] Sawoszczuk T, Syguła-Cholewińska J, del Hoyo-Meléndez JM. Optimization of headspace solid phase microextraction for the analysis of microbial volatile organic compounds emitted by fungi: application to historical objects. J Chromatogr A. 2015;1409:30–45.10.1016/j.chroma.2015.07.059Search in Google Scholar PubMed

[88] Banou P, Alexopoulou A, Chranioti C, Tsimogiannis D, Terlixi A-V, Zervos S, et al. The effect of oil binders on paper supports via VOC analysis. J Cult Heritage. 2016;20:589–98.10.1016/j.culher.2016.01.003Search in Google Scholar

[89] Pedersoli Júnior JL, Ligterink FJ, van Bommel M. Non-destructive determination of acetic acid and furfural in books by solid-phase micro-extraction (SPME) and gas chromatography-mass spectrometry (GC/MS). Restaurator. 2011;32:110–34.10.1515/rest.2011.007Search in Google Scholar

[90] Weston RJ, Smith GJ, Scheele SM, Williams SH. Accelerated hydrothermal degradation of fibres of Phormium tenax (New Zealand flax). J Cult Heritage. 2012;13:413–8.10.1016/j.culher.2011.11.006Search in Google Scholar

[91] Nguyen TP, le Bourg E, Bouvet S, Rottier V. Optimisation of the quality control of cellulosic materials used for the conservation and storage of paper-based cultural heritage, based on the emissions of volatiles. In: Bridgland J, editor. ICOM-CC 16th Triennial Conference Preprints, Lisbon, 19–23 September 2011. Lisbon: Critério-Produção Grafica, Lda., 2011: 9.Search in Google Scholar

[92] Lattuati-Derieux A, Thao S, Langlois J, Regert M. First results on headspace-solid phase microextraction-gas chromatography/mass spectrometry of volatile organic compounds emitted by wax objects in museums. J Chromatogr A. 2008;1187:239–49.10.1016/j.chroma.2008.02.015Search in Google Scholar PubMed

[93] Curran K, Možir A, Underhill M, Gibson LT, Fearn T, Strlič M. Cross-infection effect of polymers of historic and heritage significance on the degradation of a cellulose reference test material. Polym Degrad Stab. 2014;107:294–306.10.1016/j.polymdegradstab.2013.12.019Search in Google Scholar

[94] Lattuati-Derieux A, Egasse C, Thao-Heu S, Balcar N, Barabant G, Lavédrine B. What do plastics emit? HS-SPME-GC/MS analyses of new standard plastics and plastic objects in museum collections. J Cult Heritage. 2013;14:238–47.10.1016/j.culher.2012.06.005Search in Google Scholar

[95] Ormsby M. Analysis of laminated documents using solid-phase microextraction. J Am Inst Conserv. 2005;44:13–26.10.1179/019713605806082400Search in Google Scholar

[96] Schilling MR, Learner T. Evolved gas analysis as a tool for characterizing plastics. In: Bridgland J, editor. ICOM-CC 16th Triennial Conference Preprints, Lisbon, 19–23 September 2011. Lisbon: Critério-Produção Grafica, Lda., 2011: 11 pp.Search in Google Scholar

[97] Samide MJ, Liggett MC, Mill J, Smith GD. Relating volatiles analysis by GC-MS to Oddy test performance for determining the suitability of museum construction materials. Heritage Sci. 2018;6:1–10.10.1186/s40494-018-0213-2Search in Google Scholar

[98] Han B, Vial J, Inaba M, Sablier M. Analytical characterization of East Asian handmade papers: a combined approach using Py-GC×GC/MS and multivariate analysis. J Anal Appl Pyrolysis. 2017;127:150–8.10.1016/j.jaap.2017.08.013Search in Google Scholar

[99] D’Arcy P, Mallard WG. AMDIS – user guide. Gaithersburg MD: National Institute of Standards and Technology, 2004.Search in Google Scholar

[100] MaSC (the Users’ Group for Mass Spectrometry and Chromatography) https://mascgroup.org/workshops-meetings/past-workshops-and-meetings/. Accessed 21 August 2018.Search in Google Scholar

[101] RAdICAL (Recent Advances in Characterizing Asian Lacquer) http://www.getty.edu/conservation/our_projects/education/radical/. Accessed 21 August 2018.Search in Google Scholar

[102] Higgitt C, Spring M, Saunders D. Pigment-medium interactions in oil paint films containing red lead or lead-tin yellow. Natl Gallery Tech Bull. 2003;24:75–95.Search in Google Scholar

[103] Calvano CD, van der Werf ID, Palmisano F, Sabbatini L. Revealing the composition of organic materials in polychrome works of art: the role of mass spectrometry-based techniques. Anal Bioanal Chem. 2016;408:6957–81.10.1007/s00216-016-9862-8Search in Google Scholar PubMed

[104] Pauk V, Barták P, Lemr K. Characterization of natural organic colorants in historical and art objects by high‐performance liquid chromatography. J Sep Sci. 2014;37:3393–410.10.1002/jssc.201400650Search in Google Scholar PubMed

[105] Frysinger G, Hall G, Gaines R, Sutherland K. Comprehensive two-dimensional gas chromatography with mass spectrometric detection (GC×GC-MS) and its application to the separation and identification of organic compounds in some natural resins and waxes. In: Sutherland K, Maines C, van den Berg KJ, Ferreira E, Higgitt C, editors. MaSC 2007 Meeting Program. Philadelphia Museum of Art: 2007:18 (abstract).Search in Google Scholar

[106] Prati S, Fuentes D, Sciutto G, Mazzeo R. The use of laser pyrolysis-GC-MS for the analysis of paint cross sections. J Anal Appl Pyrolysis. 2014;105:327–34.10.1016/j.jaap.2013.11.020Search in Google Scholar

[107] Evershed R. Compound-specific stable isotopes in organic residue analysis in archaeology. In: Colombini MP, Modugno F, editors. Organic mass spectrometry in art and archaeology. Chichester: John Wiley & Sons, Ltd. 2009:391–432.Search in Google Scholar