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The Synthesis of Mesoporous Molecular Sieve MCM-41 in Glycerol System

  • Xiumei Tai , Hongxia Wang , Jian Zhang und Xiuqi Shi
Veröffentlicht/Copyright: 5. April 2013
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Tenside Surfactants Detergents
Aus der Zeitschrift Tenside Surfactants Detergents Band 43 Heft 1

Abstract

An efficient method for mesoporous molecular sieve MCM-41 was introduced in this report. In EDA/TEOS/CTAB/glycerol system, mesoporous molecular sieve MCM-41 has been synthesized at room temperature and under hydrothermal condition, respectively, characterized by X-ray power diffraction and N2 adsorption. Compared with the samples synthesized under hydrothermal condition, the samples synthesized at room temperature have better order, larger pore diameter and narrower pore diameter distribution.

Kurzfassung

Eine effiziente Methode zur Synthese mesoporöser Molekularsiebe MCM-41 wird in diesem Bericht vorgestellt. In einem EDA/TEOS/CTAB/Glycerol-System wurden mesoporöse Molekularsiebe MCM-41 bei Raumtemperatur und unter hydrothermalen Bedingungen synthetisiert und mittels Röntgenbeugungsanalyse sowie N2-Adsorption entsprechend charakterisiert. Verglichen mit den Proben die unter hydrothermalen Bedingungen synthetisiert wurden, besitzen die bei Raumtemperatur synthetisierten Proben eine bessere Ordnung, größere Porendurchmesser und eine engere Porenverteilung.

Key words:: Mesoporous molecular sieves; MCM-41; synthesis; glycerol system
Stichwörter:: Mesoporöse Molekularsiebe MCM-41; Synthese; Glycerol-System
∗ Hong-Xia Wang, China Research Institute of Daily Chemical Industry, Taiyuan 030001, Shanxi Province, P.R. China, Tel.: 0086-351-4070043. E-mail:

Xiu-Mei Tai is reading for Master degree at China Research Institute of Daily Chemical Industry. Her research fields centred at the synthesis of mesoporous molecular sieves and the application of surfactant.

Hong-Xia Wang, a professor of China Research Institute of Daily Chemical Industry, has been studying the interaction between amphiphilic molecular and mineral.

Jian Zhang is a PhD of Taiyuan University of Technology, she currently also works at China Research Institute of Daily Chemical Industry and has been engaged in surfactant research.

Xiu-Qi Shi is reading for Master degree at China Research Institute of Daily Chemical Industry. His research fields centred at the microemulsion polymerization of styrene.

References

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Received: 2005-02-22
Published Online: 2013-04-05
Published in Print: 2006-03-01

© 2006, Carl Hanser Publisher, Munich

Artikel in diesem Heft

  1. Contents/Inhalt
  2. Contents
  3. Abstracts
  4. Abstracts
  5. Analysis
  6. The Quantitative Characterization of Chemical Modification of Sodium Dodecyl Sulphate Micellar Solutions and Retention Model in Micellar Liquid Chromatography
  7. Application
  8. Testing Robustness and Compatibility of Colour Damaging Washing Tests
  9. Testing Robustness and Compatibility of Colour Damaging Washing Tests
  10. Physical Chemistry
  11. Vesicular Phase Behaviour in Ionic Surfactant Systems with Organic Counter-ions
  12. Synthesis
  13. The Synthesis of Mesoporous Molecular Sieve MCM-41 in Glycerol System
  14. Rapid Synthesis for Mesoporous Molecular Sieves MCM-41
  15. GDCh-News
  16. First European Detergents Conference Report
https://doi.org/10.3139/113.100298
Schlagwörter für diesen Artikel
Mesoporous molecular sieves; MCM-41; synthesis; glycerol system

Artikel in diesem Heft

  1. Contents/Inhalt
  2. Contents
  3. Abstracts
  4. Abstracts
  5. Analysis
  6. The Quantitative Characterization of Chemical Modification of Sodium Dodecyl Sulphate Micellar Solutions and Retention Model in Micellar Liquid Chromatography
  7. Application
  8. Testing Robustness and Compatibility of Colour Damaging Washing Tests
  9. Testing Robustness and Compatibility of Colour Damaging Washing Tests
  10. Physical Chemistry
  11. Vesicular Phase Behaviour in Ionic Surfactant Systems with Organic Counter-ions
  12. Synthesis
  13. The Synthesis of Mesoporous Molecular Sieve MCM-41 in Glycerol System
  14. Rapid Synthesis for Mesoporous Molecular Sieves MCM-41
  15. GDCh-News
  16. First European Detergents Conference Report
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