Zeitschrift für Kristallographie - New Crystal Structures

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Volume 230, Issue 3

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

Open Access
Crystal structure of 7-benzyloxy-5,6-dihydroxyflavone, C₂₂H₁₆O₅

September 15, 2015

Chen-Miao Kuo, Tania N. Hill, Barend C. B. Bezuidenhoudt

Page range: 193-194

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C 22 H 16 O 5 , monoclinic, P2 1 /c (no. 14), a = 4.8039(3) Å, b = 31.819(2) Å, c = 11.1993(7) Å, β = 107.350(3)°, V = 1634.0 Å 3 , Z = 4, R gt (F) = 0.0458, wR ref (F 2 ) = 0.1173, T = 100 K.
Open Access
Crystal structure of aqua(benzene-1,2-dicarboxylato-κ²O,O')bis[2-(1Hpyrazol- 3-yl)pyridine-κ²N,N']manganese(II), C₂₄H₂₀MnN₆O₅

September 15, 2015

Hua Cai, Ying Guo, Jian-Gang Li

Page range: 195-196

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C 24 H 20 MnN 6 O 5 , triclinic, P1̅ (no. 2), a = 10.442(4) Å, b = 11.450(4) Å, c = 11.487(4) Å, α = 75.534(7)°, β = 64.803(7)°, γ = 82.086(7)°, V = 1202.5 Å 3 , Z = 2, R gt (F) = 0.0598, wR ref (F 2 ) = 0.1756, T = 296 K.
Open Access
Crystal structure of two dimensional polymeric poly[bis(μ₃-chloro)-(μ²-2- aminopyrimidine-κ²N,N')-dicopper(I)], C₈H₁₀Cl₄Cu₄N₆

September 15, 2015

Jaeun Kang, KangMin Ok, Junghwan Do

Page range: 197-198

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C 8 H 10 Cl 4 Cu 4 N 6 , orthorhombic, Pnma(no. 62), a = 14.054(1) Å, b = 14.501(1) Å, c = 3.7751(4) Å, V = 769.3 Å 3 , Z = 2, R gt (F) = 0.0331, wR ref (F 2 ) = 0.0885, T = 296 K.
Open Access
Crystal structure of hexahydro-7-hydroxy-3-(2-methylpropyl)pyrrolo [1,2-a]pyrazine-1,4-dione, C₁₁H₁₈N₂O₃

September 15, 2015

Yan Zhang, Xin-Xiang Lei

Page range: 199-200

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C 11 H 18 N 2 O 3 , orthorhombic, P2 1 2 1 2 1 (no. 19), a = 6.3149(5) Å, b = 9.6242(7) Å, c = 19.671(2) Å, V = 1195.5 Å 3 , Z = 4, R gt (F) = 0.0386, wR ref (F 2 ) = 0.1061, T = 298 K.
Open Access
Crystal structure of (2,6-pyridinedicarboxylato-κ³O,N,O')[2,6-bis(benzimidazol- 2-yl)pyridine-κ³N,N',N'']copper(II)— methanol (1:1), C₂₇H₂₀CuN₆O₅

September 15, 2015

Rui Feng, Yan Yang, Zheng Lu, Fan-Yi Lu, Feng-Mei Nie

Page range: 201-202

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C 27 H 20 CuN 6 O 5 , triclinic, P 1̅ (no. 2), a = 10.4231(9) Å, b = 11.8744(11) Å, c = 13.5630(8) Å, ɑ = 96.829(6)°, β = 110.187(7)°, γ = 106.805(8)°, V = 1463.0 Å 3 , Z = 2, R gt (F) = 0.0507, wR ref (F 2 ) = 0.1312, T = 105 K.
Open Access
Crystal structure of poly[[µ₂-1,2-benzenedicarboxylato-κ⁴O,O':O'',O''']- [µ₂-2-((1H-imidazol-1-yl)-6-methyl)-1H-benzoimidazole-κ²N:N']- cadmium(II)], C₂₀H₁₅CdN₄O₄

September 15, 2015

Zhen Liang, Shou-Jun Jian, Jin-Huan Zhou, Huai-Xia Yang

Page range: 203-204

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C 20 H 15 CdN 4 O 4 , triclinic, P1̅ (no. 2), a = 9.927(2) Å, b = 9.970(2) Å, c = 11.046(2) Å, ɑ = 80.94(3)°, β = 75.54(3)°, γ = 68.27(3)°, V = 980.8(3) Å 3 , Z = 2, R gt (F) = 0.0281, wR ref (F 2 ) = 0.0703, T = 293 K.
Open Access
Crystal structure of 4-chloro-3'-methoxy-[1,1'-biphenyl]-3-carbaldehyde, C₁₄H₁₁ClO₂

September 15, 2015

Weiwei Cao, Haifeng Gan, Zhengbang Chen, Kai Guo

Page range: 205-206

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C 14 H 11 ClO 2 , orthorhombic, P2 1 2 1 2 1 (no. 19), a = 4.1210(8) Å, b = 11.363(2) Å, c = 24.982(5) Å, V = 1169.8 Å 3 , Z = 4, R gt (F) = 0.0572, wR ref (F 2 ) = 0.1287, T = 293 K.
Open Access
Crystal structure of 3-(benzoylamino)azepan-2-one, C₁₃H₁₆N₂O₂

September 15, 2015

Xiao-Lin Li, Zheng Fang, Feng Zhang, Meng-Xue Wang, Kai Guo

Page range: 207-208

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C 13 H 16 N 2 O 2 , orthorhombic, P2 1 2 1 2 1 (no. 19), a = 7.488(2) Å, b = 9.633(2) Å, c = 16.933(3) Å, V = 1221.4 Å 3 , Z = 4, R gt (F) = 0.0671, wR ref (F 2 ) = 0.1661, T = 293 K.
Open Access
Crystal structure of hexahydro-3-[(phenylmethyl)amino]-2H-azepin-2- one, C₁₃H₁₈N₂O

September 15, 2015

Zheng Fang, Zhang Feng, Kai Guo

Page range: 209-210

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C 13 H 18 N 2 O, orthorhombic, Pbca (no. 61), a = 9.933(2) Å, b = 9.941(2) Å, c = 23.754(5) Å, V = 2345.6 Å 3 , Z = 8, R gt (F) = 0.0680, wR ref (F 2 ) = 0.1217, T = 293 K.
Open Access
Crystal structure of potassium 4-(2-carboxyphenyl)-3,5-dimethyl-1,2,6- thiadiazin-2-ide 1,1-dioxide monohydrate, C₁₂H₁₃KN₂O₅S

September 15, 2015

Nilay Bhatt, Pralav Bhatt, Thavendran Govender, Hendrik G. Kruger, Glenn E. M. Maguire

Page range: 211-212

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C 12 H 13 KN 2 O 5 S, monoclinic, P2 1 /c (no. 14), a = 15.8681(4) Å, b = 7.2173(2) Å, c = 12.8527(4) Å, β = 109.6260(10)°, V = 1386.4 Å 3 , Z = 4, R gt (F) = 0.0248, wR ref (F 2 ) = 0.0858, T = 173 K.
Open Access
Crystal structure of tetraaquabis(4-carboxypyridine-2,6-dicarboxylato- κ³N,O,O')(µ₂-4,4'-bipyridine-κ²N:N')dizinc(II)dihydrate, [Zn₂(C₈H₃NO₆)₂(C₁₀H₈N₂)(H₂O)₄]·2H₂O, C₂₆H₂₆N₄O₁₈Zn₂

September 15, 2015

Youngjin Jeon, Myunghan Lee, Hyunuk Kim, Ki-Min Park

Page range: 213-214

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C 26 H 26 N 4 O 18 Zn 2 , monoclinic, P2 1 /c (no. 14), a = 11.4727(7) Å, b = 20.281(1) Å, c = 7.0745(4) Å, β = 103.328(1)°, V = 1601.8 Å 3 , Z = 2, R gt (F) = 0.0436, wR ref (F 2 ) = 0.1314, T = 203 K.
Open Access
Crystal structure of trans-diaquabis(salicylaldehydato-κ²O,O') cobalt(II), C₁₄H₁₄CoO₆

September 15, 2015

Haipeng Diao, Wen Liu, Min Zhou, Bin Jia, Jun Xie, Haojiang Wang, Tijian Sun

Page range: 215-216

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C 14 H 14 CoO 6 , monoclinic, C2/m (no. 12), a = 7.3910(5) Å, b = 7.4029(6) Å, c = 13.012(1) Å, β = 90.573(1)°, V = 711.9 Å 3 , Z = 2, R gt (F) = 0.0373, wR ref (F 2 ) = 0.1026, T = 298 K.
Open Access
Crystal structure of (E)-1-((1-(3,4-dimethoxyphenyl)ethyl)imino) guanidinium perchlorate, C₁₁H₁₇ClN₄O₆

September 15, 2015

Lin Du, Song-He Li, Yu-Heng Deng

Page range: 217-218

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C 11 H 17 ClN 4 O 6 , monoclinic, C2/c (no. 15), a = 17.870(6) Å, b = 7.885(2) Å, c = 23.105(8) Å, β = 108.139(4)°, V = 3093.9 Å 3 , Z = 8, R gt (F) = 0.0614, wR ref (F 2 ) = 0.1961, T = 293 K.
Open Access
Crystal structure of (2E)-2-[1-(4-bromophenyl)-3-(1H-imidazol-1-yl) propylidene]-N-(2,4-dichlorophenyl)hydrazinecarboxamide, C₁₉H₁₆BrCl₂N₅O

September 15, 2015

Reem I. Al-Wabli, Mohamed I. Attia, Hazem A. Ghabbour, Nahed N. E. El-Sayed, Hoong-Kun Fun

Page range: 219-220

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C 19 H 16 BrCl 2 N 5 O, triclinic, P1̅ (no. 2), a = 7.4661(3) Å, b = 10.9874(4) Å, c = 12.8619(5) Å, ɑ = 109.979(3)°, β = 92.053(3)°, γ = 95.677(3)°, V = 984.0 Å 3 , Z = 2, R gt (F) = 0.0653, wR ref (F 2 ) = 0.1906, T = 296 K.
Open Access
Crystal structure of 1-(p-methyl benzylidene)-2-(thiazolo[5,4-b]pyridin-2- yl)hydrazine, C₁₄H₁₂N₄S

September 15, 2015

Shi-Qian Wei, Shao-Bin Miao

Page range: 221-222

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C 14 H 12 N 4 S, monoclinic, P2 1 /c (no. 14), a = 17.119(5) Å, b = 6.813(2) Å, c = 11.505(3) Å, β = 98.947(4)°, V = 1325.5 Å 3 , Z = 4, R gt (F) = 0.0469, wR ref (F 2 ) = 0.1189, T = 296 K.
Open Access
Crystal structure of bis(2-trifluoromethyl-4-nitrophenyl) terephthalate — acetic acid (1:1), C₂₄H₁₄F₆N₂O₁₀

September 15, 2015

Wei Chen, Mian Ji, Shiyong Yang

Page range: 223-224

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C 24 H 14 F 6 N 2 O 10 , triclinic, P1̅ (no. 2), a = 9.985(2) Å, b = 11.496(3) Å, c = 12.721(2) Å, ɑ = 107.297(9)°, β = 112.982(9)°, γ = 94.214(14)°, V = 1253.4 Å 3 , Z = 2, R gt (F) = 0.0656, wR ref (F 2 ) = 0.1427, T = 173 K.
Open Access
Crystal structure of poly[diaqua-µ₂-(E)-5-oxo-4-((5-oxo-1,5-dihydro-4H- 1,2,4-triazol-4-yl)diazenyl)-4,5-dihydro-1,2,4-triazol-1-ide-κ³O:O:N) sodium], C₄H₇N₈NaO₄

September 15, 2015

Jiaping Zhu, Shaohua Jin, Yuehai Yu, Shusen Chen, Qinghai Shu

Page range: 225-226

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C 4 H 7 N 8 NaO 4 , monoclinic, C2/c (no. 15), a = 19.42(2) Å, b = 6.514(5) Å, c = 15.38(1) Å, β = 93.23(2)°, V = 1942.9 Å 3 , Z = 8, R gt (F) = 0.0631, wR ref (F 2 ) = 0.1660, T = 293 K.
Open Access
Crystal structure of n-butyl-chlorido-bis[benzyl(isopropyl)carbamodithioato- κ²S:S']-tin(IV), C₂₆H₃₇ClN₂S₄Sn

September 15, 2015

Amirah Faizah Abdul Muthalib, Ibrahim Baba, Siti Nadiah Abdul Halim, Edward R. T. Tiekink

Page range: 227-228

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C 26 H 37 ClN 2 S 4 Sn, monoclinic, C2/c (no. 15), a = 29.2206(11) Å, b = 10.6749(4) Å, c = 19.6877(7) Å, β = 104.411(4)°, V = 5947.9 Å 3 , Z = 8, R gt (F) = 0.0235, wR ref (F 2 ) = 0.0545, T = 100 K.
Open Access
Crystal structure of bis-(5-bromo-2-methyl-phenyl)-diazene, C₁₄H₁₂Br2N₂

September 15, 2015

Shi-Hui Li, Tian Zhang, Xun Feng, Su-Zhen Huoi

Page range: 229-230

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C 14 H 12 Br 2 N 2 , monoclinic, P2 1 /c (no. 14), a = 7.07(1) Å, b = 4.079(7) Å, c = 23.86(4) Å, β = 90.13(2)°, V = 687.6 Å 3 , Z = 2, R gt (F) = 0.0346, wR ref (F 2 ) = 0.1166, T = 296 K.
Open Access
Crystal structure of [2,2'-(1,5-diazocane-1,5-diyl)diethanamine-κ⁴N]- nickel(II) diperchlorate, C₁₀H₂₄Cl₂N₄NiO₈

September 15, 2015

Qiang Xu, Guo Qiang Li, Jiang Ping Meng

Page range: 231-232

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C 10 H 24 Cl 2 N 4 NiO 8 , orthorhombic, Cmc2 1 (no. 36), a = 9.657(2) Å, b = 14.916(4) Å, c = 24.599(8) Å, V = 3543.3 Å 3 , Z = 8, R gt (F) = 0.0351, wR ref (F 2 ) = 0.0899, T = 293 K.
Open Access
Co-Crystal structure of 1,3-phenylenediacetic acid and 2,5-bis(4-pyridyl)- 1,3,4-oxadiazole (1:1), C₂₂H₁₈N₄O₅

September 15, 2015

Ling-Yun Xin, Hai-Xia Wu, Ying-Ge Zhang, Yan-Yan Zhang

Page range: 233-234

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C 22 H 18 N 4 O 5 , monoclinic, P2 1 /c (no. 14), a = 17.153(1) Å, b = 13.4635(8) Å, c = 8.8010(6) Å, β = 90.807(2)°, V = 2032.3 Å 3 , Z = 4, R gt (F) = 0.0414, wR ref (F 2 ) = 0.1148, T = 296 K.
Open Access
Crystal structure of ethyl 4-(5-allyl-6-methyl-2-phenylpyrimidin-4-ylamino) benzoate, C₂₃H₂₃N₃O₂

September 15, 2015

Zai-Sheng Lu, Guang-Zhou Zhu

Page range: 235-236

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C 23 H 23 N 3 O 2 , triclinic, P1̅ (no. 2), a = 8.244(5) Å, b = 9.998(6) Å, c = 12.618(8) Å, ɑ = 76.654(7)°, β = 84.834(7)°, γ = 81.708(7)°, V = 999.6 Å 3 , Z = 2, R gt (F) = 0.0469, wR ref (F 2 ) = 0.1473, T = 296 K.
Open Access
Crystal structure of 5-((2,3-dihydrobenzo[b][1,4]dioxin-6-yl)methylene)- thiazolidine-2,4-dione, C₁₂H₉NO₄S

September 15, 2015

Yong-De Liu, Lu-Bing Yan, Xin-Yi Wang, Juan Sun

Page range: 237-238

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C 12 H 9 NO 4 S, triclinic, P1̅ (no. 2), a = 3.9201(5) Å, b = 11.836(2) Å, c = 13.105(2) Å, ɑ = 67.415(4)°, β = 83.375(4)°, γ = 82.156(4)°, V = 554.8 Å 3 , Z = 2, R gt (F) = 0.0401, wR ref (F 2 ) = 0.0999, T = 293 K.
Open Access
Crystal structure of catena-poly[(µ₂-chlorido)-bis(N-ethyl,N-hydroxyethylcarbamodithioato-κ²S,S')bismuth(III) monohydrate], C₁₀H₂₂BiClN₂O₃S₄

September 15, 2015

Nur Amirah Jamaluddin, Ibrahim Baba, Nadiah Abdul Halim, Edward R. T. Tiekink

Page range: 239-240

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C 10 H 22 BiClN 2 O 3 S 4 , orthorhombic, Pca2 1 (no. 29), a = 8.1121(4) Å, b = 10.8634(5) Å, c = 20.7900(9) Å, V = 1832.1 Å 3 , Z = 4, R gt (F) = 0.0278, wR ref (F 2 ) = 0.0574, T = 100 K.
Open Access
Regioselective synthesis and crystal structure of ethyl-4-acetyl-5-((2- ethoxy-2-oxoethyl)thio)-3-hydroxythiophene-2-carboxylate, C₁₃H₁₆O₆S₂

September 15, 2015

Y. N. Mabkhot, S. S. Al-Showiman, A. Barakat, S. Yousuf, M. I. Choudhary

Page range: 241-242

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C 13 H 16 O 6 S 2 , triclinic, P1̅ (no. 2), a = 7.979(1) Å, b = 9.189(1) Å, c = 10.263(1) Å, ɑ = 72.876(2)°, β = 71.485(2)°, γ = 76.655(2)°, V = 674.0 Å 3 , Z = 2, R gt (F) = 0.0360, wR ref (F 2 ) = 0.0962, T = 273 K.
Open Access
Crystal structure of 4-pyridazinecarboxylic acid, C₅H₄N₂O₂

September 15, 2015

Shengjun Deng, Jie Chen, Yijian Liu, Ning Zhang

Page range: 243-244

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C 5 H 4 N 2 O 2 , orthorhombic, Pnma (no. 62), a = 11.165(2) Å, b = 6.215(1) Å, c = 7.413(2) Å, V = 514.4 Å 3 , Z = 4, R gt (F) = 0.0567, wR ref (F 2 ) = 0.1515, T = 153 K.
Open Access
Crystal structure 2,2’-diselanediyldibenzoic acid— dimethylformamide (1/2), C₁₈H₂₂N₄O₆Se₂

September 15, 2015

De-Zhong Niu, Lin Yao, Yuwei Zhang

Page range: 245-246

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C 18 H 22 N 4 O 6 Se 2 , monoclinic, P2 1 /c (no. 14), a = 7.3648(4) Å, b = 15.2480(7) Å, c = 9.9280(5) Å, β = 101.311(3)°, V = 1093.2 Å 3 , Z = 2, R gt (F) = 0.0230, wR ref (F 2 ) = 0.0602, T = 296 K.
Open Access
Crystal structure of 2,2'-biqinoline-κ²N,N')dichloromercury(II), C₁₈H₁₂Cl₂HgN₂

September 15, 2015

Sadif A. Shirvan, Moayad Hossaini Sadr, Karim Zare

Page range: 247-248

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C 18 H 12 Cl 2 HgN 2 , monoclinic, C2/c (no. 15), a = 13.442(1) Å, b = 16.094(1) Å, c = 7.585(1) Å, β = 96.26(1)°, V = 1631.1 Å 3 , Z = 4, R gt (F) = 0.0458, wR ref (F 2 ) = 0.0813, T = 298 K.
Open Access
Crystal structure of (2E)-2-[3-(1H-imidazol-1-yl)-1-phenylpropylidene]- hydrazinecarboxamide monohydrate, C₁₃H₁₇N₅O₂

September 15, 2015

Mohamed I. Attia, Hazem A. Ghabbour, Hoong-Kun Fun

Page range: 249-250

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C 13 H 17 N 5 O 2 , monoclinic, P2 1 /c (no. 14), a = 11.1953(3) Å, b = 5.5215(2) Å, c = 22.6998(5) Å, β = 99.929(2)°, V = 1382.2 Å 3 , Z = 4, R gt (F) = 0.0373, wR ref (F 2 ) = 0.1104, T = 296 K.
Open Access
Crystal structure of 3-bromo-4,6-dibenzyloxy-2-hydroxy acetophenone, C₂₂H₁₉BrO₄

September 15, 2015

Tania N. Hill, Chen-Miao Kuo, Barend C. B. Bezuidenhoudt

Page range: 251-252

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C 22 H 19 BrO 4 , triclinic, P1̅ (no. 2), a = 8.550(2) Å, b = 11.343(2) Å, c = 11.715(2) Å, ɑ = 102.02(3)°, β = 110.47(3)°, γ = 110.84(3)°, V = 920.2 Å 3 , Z = 2, R gt (F) = 0.0368, wR ref (F 2 ) = 0.099, T = 100 K.
Open Access
Crystal structure of catena-poly[(4-bromoisophthalato-κ²O:O')-[1,1'-(1,3- propanediyl)bis(benzimidazole-κ²N:N')cobalt(II)], C₂₅H₁₉BrCoN₄O₄

September 15, 2015

Qin Wang, Hui-Ju Zhang

Page range: 253-254

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C 25 H 19 BrCoN 4 O 4 , triclinic, P1̅ (no. 2), a = 8.333(1) Å, b = 12.331(2) Å, c = 13.061(2) Å, ɑ = 62.770(2)°, β = 85.658(2)°, γ = 79.584(2)°, V = 1173.6 Å 3 , Z = 2, R gt (F) = 0.0406, wR ref (F 2 ) = 0.1063, T = 296 K.
Open Access
Crystal structure of 1-acetylimidazolidine-2,4-dione monohydrate, C₅H₈N₂O₄

September 15, 2015

Y. N. Mabkhot, S. S. Al-Showiman, A. Barakat, S. Yousuf, M. I. Choudhary

Page range: 255-256

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C 5 H 8 N 2 O 4 , monoclinic, P2 1 /m (no. 11), a = 6.385(2) Å, b = 6.150(2) Å, c = 8.771(2) Å, β = 105.698(4)°, V = 331.5 Å 3 , Z = 2, R gt (F) = 0.0358, wR ref (F 2 ) = 0.0955, T = 273 K.
Open Access
Crystal structure of (Z)-5-(3-methylbenzylidene)-2-thioxothiazolidin-4- one, C₁₃H₁₅NO₂S₃

September 15, 2015

Assem Barakat, Abdullah Mohammed Al-Majid, Yahia N. Mabkhot, Hazem A. Ghabbour, Hoong-Kun Fun

Page range: 257-258

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C 13 H 15 NO 2 S 3 , triclinic, P1̅ (no. 2), a = 7.2618(5) Å, b = 8.3190(6) Å, c = 13.2073(10) Å, ɑ = 93.117(2)°, β = 97.485(2)°, γ = 109.523(2)°, V = 741.5 Å 3 , Z = 2, R gt (F) = 0.0573, wR ref (F 2 ) = 0.1646, T = 150 K.
Open Access
Crystal structure of tetra-aqua-bis(µ₂-thiophene-3,4-dicarboxylato-κ⁴O,O’:O’’,O’’’)-bis(thiophene-3-carboxyl-4-carboxylato-κ¹O)-bis(1,10- phenantroline-κ²N,N’)disamarium(III), C₂₄H₁₇N₂O₁₀S₂Sm

September 15, 2015

Shi-Jun Chen, Shi-Hui Li

Page range: 259-260

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C 24 H 17 N 2 O 10 S 2 Sm, triclinic, P1̅ (no. 2), a = 10.135(5) Å, b = 10.697(5) Å, c = 11.823(7) Å, ɑ = 94.676(5)°, β = 98.927(5)°, γ = 101.736(4)°, V = 1231.3 Å 3 , Z = 2, R gt (F) = 0.0184, wR ref (F 2 ) = 0.0455, T = 296 K.
Open Access
Crystal structure of tetrakis(µ₂-formiato-κ²O:O')bis(4-methylpyridine-κN) dirhodium(II) (Rh–Rh), C₁₆H₁₈N₂O₈Rh₂

September 15, 2015

Qing-Song Ye, Juan Yu, Xiao-Nian Li, Qiao-Wen Chang, Jing Jiang, Cai-Xian Yan, Wei-Ping Liu

Page range: 261-262

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C 16 H 18 N 2 O 8 Rh 2 , monoclinic, P2 1 /c (no. 14), a = 10.635(2) Å, b = 11.375(3) Å, c = 7.854(2) Å, β = 90.634(3)°, V = 950.0 Å 3 , Z = 2, R gt (F) = 0.0373, wR ref (F 2 ) = 0.0930, T = 100 K.
Open Access
Crystal structure of diaqua-dinitrato-κ¹O-bis(2-(pyridin-4-ylthio)- pyrazine-κ¹N)cadmium(II), C₁₈H₁₈CdN₈O₈S₂

September 15, 2015

Deng-Wu Wang, Fang Wang

Page range: 263-264

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C 18 H 18 CdN 8 O 8 S 2 , monoclinic, P2 1 /c (no. 14), a = 12.9345(5) Å, b = 12.9120(5) Å, c = 7.2991(3) Å, β = 91.085(2)°, V = 1218.8 Å 3 , Z = 2, R gt (F) = 0.0401, wR ref (F 2 ) = 0.0939, T = 296 K.
Open Access
Crystal structure of diaqua-bis[1-cyclopropyl-7-(4-ethylpiperazin-1-yl)-6- fluor-4-oxo-1,4-dihydrochinolin-3-carboxylic acid]manganese(II)-benzene- 1-carboxyl-4-carboxylate octahydrate, C₅₄H₇₄F₂MnN₆O₂₄

September 15, 2015

Ling Zhu, Tian Zhou

Page range: 265-266

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C 54 H 74 F 2 MnN 6 O 24 , monoclinic, P2 1 /n (no. 14), a = 13.5493(4) Å, b = 13.8063(4) Å, c = 16.7349(4) Å, β = 106.935(2)°, V = 2994.8 Å 3 , Z = 2, R gt (F) = 0.0629, wR ref (F 2 ) = 0.1500, T = 296 K.
Open Access
Crystal structure of 3-{[4-(4-fluorophenyl)piperazin-1-yl]methyl}-5-(thiophen- 2-yl)-2,3-dihydro-1,3,4-oxadiazole-2-thione, C₁₇H₁₇FN₄OS₂

September 15, 2015

Fatmah A. M. Al-Omary, Haitham AlRabiah, Hazem A. Ghabbour, Ching Kheng Quah, Hoong-Kun Fun, Ali A. El-Emam

Page range: 267-268

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C 17 H 17 FN 4 OS 2 , triclinic, P1̅ (no. 2), a = 6.3278(8) Å, b = 9.6250(13) Å, c = 14.789(2) Å, α = 81.739(5)°, β = 82.226(4)°, γ = 76.611(4)°, V = 862.3 Å 3 , Z = 2, R gt (F) = 0.0798, wR ref (F 2 ) = 0.2072, T = 150 K.
Open Access
Crystal structure of bis(N,N,N-triethylammonium) bis(tetraselenido-κ²Se¹,Se⁴)palladate(II), C₁₂H₃₂N₂PdSe₈

September 15, 2015

Kang-Woo Kim, Jinhee Kim

Page range: 269-270

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C 12 H 32 N 2 PdSe 8 , orthorhombic, Pca2 1 (no. 29), a = 17.493(3) Å, b = 8.109(1) Å, c = 17.326(2) Å, V = 2457.6 Å 3 , Z = 4, R gt (F) = 0.0270, wR ref (F 2 ) = 0.0565, T = 173 K.
Open Access
Crystal structure of (2E,6E)-2,6-bis[2-(trifluoromethyl)benzylidene]cyclohexanone, C₂₂H₁₆F₆O

September 15, 2015

Ying Zhang, Kai-Ling Pan, Fan He, Ling-Feng Chen, Zhi-Guo Liu, Guang Liang

Page range: 271-272

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C 22 H 16 F 6 O, monoclinic, P2 1 /n (no. 14), a = 8.426(2) Å, b = 15.205(4) Å, c = 14.900(4) Å, β = 93.031(6)°, V = 1906.4 Å 3 , Z = 4, R gt (F) = 0.0632, wR ref (F 2 ) = 0.1826, T = 293 K.
Open Access
Crystal structure of 3,5-bis(imidazole-1-yl)pyridine, C₁₁H₉N₅

September 15, 2015

Zhou Hongyan

Page range: 273-274

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C 11 H 9 N 5 , monoclinic, P2 1 /c (no. 14), a = 14.15(1) Å, b = 3.783(3) Å, c = 18.09(2) Å, β = 92.28(2)°, V = 968.0 Å 3 , Z = 4, R gt (F) = 0.0517, wR ref (F 2 ) = 0.1504, T = 296 K.
Open Access
Crystal structure of catena-Poly[bis(µ₂-2,4-dihydroxybenzoato-κ³O1,O1':O2)-(2,9-dimethyl-1,10-phenanthroline-κ²N,N')lead(II)], C₂₈H₂₂N₂O₈Pb

September 15, 2015

Li-Bing Guo, Dong Xian, Jun-Ming Tang

Page range: 275-276

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C 28 H 22 N 2 O 8 Pb, orthorhombic, Pbcn (no. 60), a = 18.691(2) Å, b = 12.611(1) Å, c = 11.092(1) Å, V = 2614.7 Å 3 , Z = 4, R gt (F) = 0.0220, wR ref (F 2 ) = 0.0671, T = 296 K.
Open Access
Crystal structure of bis(p-nitrobenzoato-κ¹O;κ²O,O')[bis(2-benzimidazolylmethyl) amine-κ³N,N',N'']lead (II) — methanol (1:1), C₃₁H₂₇N₇O₉Pb

September 15, 2015

Xuan Chen, Yan-Peng Liu, Li-Fei Liu, Chen Wang, Feng-Mei Nie

Page range: 277-279

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C 31 H 27 N 7 O 9 Pb, triclinic, P1̅ (no. 2), a = 7.5465(3) Å, b = 10.8333(4) Å, c = 19.9801(7) Å, α = 95.476(3)°, β = 94.404(3)°, γ = 108.206(3)°, V = 1534.8 Å 3 , Z = 2, R gt (F) = 0.0271, wR ref (F 2 ) = 0.0480, T = 99 K.
Open Access
Crystal structure of catena-poly[diaqua-3-(4-fluoro-phenyl)-acrylate-κ²O,O'-bis(κ²O,O')-1,2-di(4-pyridyl)ethylene-κ²N:N'nickel(II)] 3-(4- fluoro-phenyl)-acrylate, C₃₀H₂₆F₂N₂NiO₆

September 15, 2015

Hai-Xia Kang, Yu-Hao Duan, Rui-Juan Yang, Yu-Qin Fu

Page range: 280-282

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C 30 H 26 F 2 N 2 NiO 6 , monoclinic, P2 1 /c (no. 14), a = 16.6375(6) Å, b = 6.7702(3) Å, c = 25.352(1) Å, β = 105.390(1)°, V = 2753.2 Å 3 , Z = 4, R gt (F) = 0.0325, wR ref (F 2 ) = 0.0781, T = 296 K.
Open Access
Crystal structure of (µ₂-acetato-κ²O,O’)-(µ₂-chlorido)-(µ₂-oxido)- bis(dichlorido-triphenylphosphane-rhenium(IV)), C₃₈H₃₃Cl₅O₃P₂Re₂

September 15, 2015

Janvier Mukiza, Thomas I. A. Gerber, Eric C. Hosten, Richard Betz

Page range: 283-285

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C 38 H 33 Cl 5 O 3 P 2 Re 2 , orthorhombic, Pbca (no. 61), a = 18.9747(6) Å, b = 17.6316(5) Å, c = 22.3528(6) Å, V = 7478.2 Å 3 , Z = 8, R gt (F) = 0.0278, wR ref (F 2 ) = 0.0649, T = 200 K.
Open Access
Redetermination of the crystal structure of di-(4,7,13,16,21,24-hexaoxa- 1,10-diazabicyclo[8.8.8]hexacosane-κ⁸N₂,O₆) potassium – tetrapotassium octadecagermanide – ethylenediamine (1:1:7), C₂₅H₆₄Ge₉K₃N₉O₆

September 15, 2015

Kerstin Mayer, Michael Giebel, Manuel M. Bentlohner, Wilhelm Klein, Thomas F. Fässler

Page range: 286-288

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C 25 H 64 Ge 9 K 3 N 9 O 6 , triclinic, P1̅ (no. 2), a = 9.3766(7) A, b = 13.540(1) A, c = 19.507(1) A, α = 84.527(3)°, β = 81.252(3)°, γ = 80.127(4)°, V = 2405.4 A 3 , Z = 2, R gt (F) = 0.0405, wR ref (F 2 ) = 0.1050, T = 123 K.
Open Access
Crystal structure of 6-(phenylsulfanyl)-5-propylpyrimidine-2,4(1H,3H)- dione, C₁₃H₁₄N₂O₂S

September 15, 2015

Fatmah A. M. Al-Omary, Hazem A. Ghabbour, Mohamed I. Attia, Hoong-Kun Fun, Ali A. El-Emam

Page range: 289-291

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C 13 H 14 N 2 O 2 S, triclinic, P1̅ (no. 2), a = 10.0414(5) Å, b = 11.0866(6) Å, c = 12.6400(7) Å, α = 96.149(2)°, β = 105.602(2)°, γ = 110.432(2)°, V = 1238.2 Å 3 , Z = 4, R gt (F) = 0.0553, wR ref (F 2 ) = 0.1105, T = 150 K.
Open Access
Crystal structure of [bis(benzimidazol-2-yl-methyl)amine-κ³N,N',N''] phthalato-κ²O,O' copper(II) — methanol— water (1:1:2), C₂₅H₂₇CuN₅O₇

September 15, 2015

Guo-Hua Su, Yan-Peng Liu, Xuan Chen, Feng-Mei Nie

Page range: 292-294

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C 25 H 27 CuN 5 O 7 , triclinic, P1̅ (no. 2), a = 9.3812(6) Å, b = 11.3399(6) Å, c = 13.0957(8) Å, α = 81.654(8)°, β = 71.623(6)°, γ = 69.745(6)°, V = 1239.3 Å 3 , Z = 2, R gt (F) = 0.0361, wR ref (F 2 ) = 0.0830, T = 99 K.

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