Zeitschrift für Kristallographie - New Crystal Structures

Heft Open Access

Band 221, Heft 3

Februar 2014

Veröffentlicht von

Veröffentlichen auch Sie bei De Gruyter Brill

Manuskript einreichen Informationen für Autor*innen

Heft der Zeitschrift

Zeitschrift für Kristallographie - New Crystal Structures

Inhalt

Open Access
Re-investigation of the crystal structure of dodecasodium dodecaniobomanganate( IV) hydrate (1:52), Na₁₂[Mn(Nb₆O₁₉)₂] · 52H₂O

18. Februar 2014

J.-P. Wang, P.-T. Ma, J.-Y. Niu

Seiten: 235-237

PDF downloaden

H 114 MnNa 6 Nb 12 O 92 , monoclinic, P 12 1 / n 1 (no. 14), a = 14.165(2) Å, b = 12.694(2) Å, c = 24.202(3) Å, β = 92.500(2)°, V = 4347.7 Å 3 , Z = 2, R gt (F) = 0.030, wR ref (F 2 ) = 0.084, T = 293 K.
Open Access
Crystal structures of trigadolinium tetraphosphidoheptapalladate, Gd₃Pd₇P₄, and triterbium tetraphosphidoheptapalladate, Tb₃Pd₇P₄

18. Februar 2014

S. Budnyk, Yu. Prots, Yu. B. Kuz'ma, Yu. Grin

Seiten: 238-240

PDF downloaden

Gd 3 P 4 Pd 7 , monoclinic, C 12/ m 1 (no. 12), a = 15.348(3) Å, b = 3.999(1) Å, c = 9.386(2) Å, β = 125.86(1)°, V = 466.9 Å 3 , Z = 2, R gt (F) = 0.024, wR ref (F 2 ) = 0.056, T = 293 K. P 4 Pd 7 Tb 3 , monoclinic, C 12/ m 1 (no. 12), a = 15.297(3) Å, b = 3.985(1) Å, c = 9.364(2) Å, β = 125.72(1)°, V = 463.4 Å 3 , Z = 2, R gt (F) = 0.026, wR ref (F 2 ) = 0.065, T = 293 K.
Open Access
Crystal structure of dicalcium sodium monohydrogen diarsenate hexahydrate, Ca₂Na[HAsO₄][AsO₄] · ₆H₂O

18. Februar 2014

A. Jiménez, J. D. Rodríguez, L. Torre-Fernández, M. Prieto, S. García-Granda

Seiten: 241-242

PDF downloaden

As 2 Ca 2 H 13 NaO 14 , triclinic, P 1̅ (no. 2), a = 6.680(5) Å, b = 8.223(4) Å, c = 12.537(3) Å, α = 73.46(5)°, β = 78.89(4)°, γ = 87.47(5)°, V = 647.7 Å 3 , Z = 2, R gt (F) = 0.062, wR ref (F 2 ) = 0.197, T = 293 K.
Open Access
Crystal structure of bismuth triiodate dihydrate, Bi[IO₃]₃ · 2H₂O

18. Februar 2014

D. Phanon, I. Gautier-Luneau

Seiten: 243-244

PDF downloaden

BiH 4 I 3 O 11 , triclinic, P 1̅ (no. 2), a = 7.056(2) Å, b = 7.337(1) Å, c = 10.740(1) Å, α = 95.06(1)°, β = 106.16(1)°, γ = 109.56(1)°, V = 493.0 Å 3 , Z = 2, R gt (F) = 0.035, wR ref (F 2 ) = 0.090, T = 293 K.
Open Access
Crystal structure of ytterbium triiodate dihydrate, Yb[IO₃]₃ · 2H₂O

18. Februar 2014

D. Phanon, I. Gautier-Luneau

Seiten: 245-246

PDF downloaden

H 4 I 3 O 11 Yb, triclinic, P 1̅ (no. 2), a = 7.268(1) Å, b = 7.441(1) Å, c = 9.319(1) Å, α = 79.54(1)°, β = 85.18(1)°, γ = 71.90(1)°, V = 470.9 Å 3 , Z = 2, R gt (F) = 0.028, wR ref (F 2 ) = 0.070, T = 293 K.
Open Access
Crystal structure of indium triiodate dihydrate, In[IO₃]₃ · 2H₂O

18. Februar 2014

D. Phanon, I. Gautier-Luneau

Seiten: 247-248

PDF downloaden

H 4 I 3 InO 11 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 5.038(2) Å, b = 12.154(2) Å, c = 16.041(3) Å, V = 982.2 Å 3 , Z = 4, R gt (F) = 0.022, wR ref (F 2 ) = 0.042, T = 293 K.
Open Access
Crystal structure of indium triiodate trihydrate, In[IO₃]₃ · 3H₂O

18. Februar 2014

D. Phanon, I. Gautier-Luneau

Seiten: 249-250

PDF downloaden

H 6 I 3 InO 12 , triclinic, P 1̅ (no. 2), a = 6.862(1) Å, b = 7.282(2) Å, c = 11.137(3) Å, α = 94.01(2)°, β = 107.75(1)°, γ = 93.59(1)°, V = 526.7 Å 3 , Z = 2, R gt (F) = 0.034, wR ref (F 2 ) = 0.089, T = 293 K.
Open Access
Crystal structure of potassium scandium (monophosphate-hydrogenmonoborate- monophosphate), KSc[BP₂O₈(OH)]

18. Februar 2014

P. W. Menezes, S. Hoffmann, Yu. Prots, R. Kniep

Seiten: 251-252

PDF downloaden

BHKO 9 P 2 Sc, triclinic, P 1̅ (no. 2), a = 5.2696(2) Å, b = 8.2739(8) Å, c = 8.3890(5) Å, α = 88.22(1)°, β = 79.701(6)°, γ = 86.67(1)°, V = 359.2 Å 3 , Z = 2, R gt (F) = 0.032, wR ref (F 2 ) = 0.075, T = 295 K.
Open Access
Crystal structure of rubidium scandium (monophosphate-hydrogenmonoborate- monophosphate), RbSc[BP₂O₈(OH)]

18. Februar 2014

P. W. Menezes, S. Hoffmann, Yu. Prots, R. Kniep

Seiten: 253-254

PDF downloaden

BHO 9 P 2 RbSc, triclinic, P 1̅ (no. 2), a = 5.3296(2) Å, b = 8.3919(8) Å, c = 8.4319(5) Å, α = 87.27(1)°, β = 80.124(6)°, γ = 86.60(1)°, V = 370.6 Å 3 , Z = 2, R gt (F) = 0.024, wR ref (F 2 ) = 0.066, T = 293 K.
Open Access
Crystal structure of tetraytterbium septarhodium hexaantimony, Yb₄Rh₇Sb₆

18. Februar 2014

A. Leithe-Jasper, R. Cardoso-Gil, R. Ramlau, U. Burkhardt

Seiten: 255-256

PDF downloaden

Rh 7 Sb 6 Yb 4 , Im 3̅ m (no. 229), a = 8.6524(2) Å, V = 647.8 Å 3 , Z = 2, R gt (F) = 0.011, wR ref (F 2 ) = 0.019, T = 293 K.
Open Access
Crystal structure of tristrontium octagallide, Sr_3-xGa_8+3x (x = 0.15)

18. Februar 2014

F. Haarmann, Yu. Prots, S. Göbel, H. G. von Schnering

Seiten: 257-258

PDF downloaden

Ga 8.45 Sr 2.85 , orthorhombic, Immm (no. 71), a = 4.3958(9) Å, b = 4.5298(6) Å, c = 26.002(4) Å, V = 517.8 Å 3 , Z = 2, R gt (F) = 0.038, wR ref (F 2 ) = 0.091, T = 293 K.
Open Access
Crystal structure of yttrium nickel phosphide, Y₂₀Ni₄₂P_30.34

18. Februar 2014

S. Stoyko, S. Oryshchyn, V. Babizhetskyy, R. Guérin

Seiten: 259-260

PDF downloaden

Ni 42 P 30.34 Y 20 , hexagonal, P 6 3 / m (no. 176), a = 20.270(1) Å, c = 3.8030(2) Å, V = 1353.2 Å 3 , Z = 1, R gt (F) = 0.053, wR ref (F 2 ) = 0.122, T = 293 K.
Open Access
Refinement of the crystal structure of europium digallide, EuGa₂

18. Februar 2014

O. Sichevych, R. Cardoso-Gil, Yu. Grin

Seiten: 261-262

PDF downloaden

EuGa 2 , orthorhombic, Imma (no. 74), a = 4.6459(3) Å, b = 7.6255(5) Å, c = 7.6379(3) Å, V = 270.6 Å 3 , Z = 4, R gt (F) = 0.017, wR ref (F) = 0.023, T = 293 K.
Open Access
Crystal structure of dieuropium trigallium iridium, Eu₂Ga₃Ir

18. Februar 2014

O. Sichevych, Yu. Prots, W. Schnelle, M. Schmidt, Yu. Grin

Seiten: 263-264

PDF downloaden

Eu 2 Ga 3 Ir, hexagonal, P 6 3 / mmc (no. 194), a = 5.6785(2) Å, c = 8.6911(5) Å, V = 242.7 Å 3 , Z = 2, R gt (F) = 0.032, wR ref (F) = 0.028, T = 293 K.
Open Access
Re-investigation of the crystal structure of trieuropium octagallide, Eu_3-xGa_8+3x (x = 0.12)

18. Februar 2014

O. Sichevych, Yu. Prots, Yu. Grin

Seiten: 265-266

PDF downloaden

Eu 2.88 Ga 8.36 , orthorhombic, Immm (no. 71), a = 4.4105(3) Å, b = 4.3732(2) Å, c = 25.852(1) Å, V = 498.6 Å 3 , Z = 2, R gt (F) = 0.025, wR ref (F) = 0.062, T = 295 K.
Open Access
Crystal structure of praseodymium dimolybdenum disilicide carbide, PrMo₂Si₂C

18. Februar 2014

E. Dashjav, W. Schnelle, F. R. Wagner, G. Kreiner, R. Kniep

Seiten: 267-268

PDF downloaden

CMo 2 PrSi 2 , tetragonal, P 4/ mmm (no. 123), a = 4.2139(3) Å, c = 5.4093(4) Å, V = 96.1 Å 3 , Z = 1, R gt (F) = 0.020, wR ref (F 2 ) = 0.042, T = 295 K.
Open Access
Crystal structure of niobium chromium nickel, Nb(Cr_1-xNi_x)₂ (x = 0.49)

18. Februar 2014

D. Grüner, A. Ormeci, G. Kreiner

Seiten: 269-270

PDF downloaden

Cr 1.02 NbNi 0.98 , hexagonal, P 63/ mmc (no. 194), a = 4.8692(5) Å, c = 7.9628(8) Å, V = 163.5 Å 3 , Z = 4, R gt (F) = 0.052, wR ref (F 2 ) = 0.111, T = 293 K.
Open Access
Crystal structure of distrontium oxide diiodide, Sr₂OI₂

18. Februar 2014

O. Reckeweg, F. J. DiSalvo

Seiten: 271-272

PDF downloaden

I 2 OSr 2 , orthorhombic, Ibam (no. 72), a = 7.412(1) Å, b = 12.955(3) Å, c = 6.475(1) Å, V = 621.8 Å 3 , Z = 4, R gt (F) = 0.031, wR ref (F 2 ) = 0.060, T = 173 K.
Open Access
Crystal structure of diaquadidysprosium triglutarate tetrahydrate, Dy₂(H₂O)₂[O₂C(CH₂)₃CO₂]₃ · 4H₂O

18. Februar 2014

D.-Y. Wei, S.-J. Huang, J. Sun, Y.-Q. Zheng

Seiten: 273-274

PDF downloaden

C 15 H 26 Dy 2 O 18 , monoclinic, C 12/ c 1 (no. 15), a = 7.918(2) Å, b = 14.912(3) Å, c = 19.617(4) Å, β = 94.66(3)°, V = 2308.6 Å 3 , Z = 4, R gt (F) = 0.027, wR ref (F 2 ) = 0.066, T = 293 K.
Open Access
Crystal structure of trans-dichloro-1,3-propanediamine-bis[(2-methoxyethyl) diphenylphosphine]ruthenium(II), RuCl₂(C₃H₁₀N₂)(C₁₅H₁₇OP)₂

18. Februar 2014

I. Warad, S. Al-Resayes, K. Eichele

Seiten: 275-277

PDF downloaden

C 33 H 44 Cl 2 N 2 O 2 P 2 Ru, monoclinic, P 12 1 / c 1 (no. 14), a = 13.278(1) Å, b = 10.315(1) Å, c = 24.825(3) Å, β = 90.340(8)°, V = 3400.1 Å 3 , Z = 4, R gt (F) = 0.023, wR ref (F 2 ) = 0.059, T = 173 K.
Open Access
Crystal structure of 2-bromo-1,4,5,7,8-pentamethoxynaphthalene, C₁₀H₂Br(OCH₃)₅

18. Februar 2014

S. Sörgel, I. Brüdgam, H. Hartl, H.-U. Reißig

Seiten: 278-280

PDF downloaden

C 15 H 17 BrO 5 , monoclinic, P 12 1 / n 1 (no. 14), a = 11.295(2) Å, b = 23.628(5) Å, c = 16.610(3) Å, β = 92.145(5)°, V = 4429.7 Å 3 , Z = 12, R gt (F) = 0.038, wR ref (F 2 ) = 0.105, T = 173 K.
Open Access
Crystal structure of carbohydrazidium(1+) p-toluenesulfonate, (NH₂NHCONHNH₃)[CH₃C₆H₄SO₃]

18. Februar 2014

L. Yang, W. Yu, T. Wu, T.-L. Zhang, J.-G. Zhang, J.-Y. Guo, R.-F. Wu, F.-J. Ren

Seiten: 281-282

PDF downloaden

C 16 H 28 N 8 O 8 S 2 , orthorhombic, Pbca (no. 61), a = 10.646(1) Å, b = 8.185(1) Å, c = 26.402(4) Å, V = 2300.6 Å 3 , Z = 4, R gt (F) = 0.038, wR ref (F 2 ) = 0.093, T = 293 K.
Open Access
Crystal structure of (2,6-diisopropyl-phenyl)[N-tris(pentafluorophenyl)- boronyl-pyridin-2-yl]amine, (C₆F₅)₃B(C₅H₄N)(C₁₂H₁₈N)

18. Februar 2014

A. Noor, T. Irrgang, R. Kempe

Seiten: 283-284

PDF downloaden

C 35 H 22 BF 15 N 2 , triclinic, P 1̅ (no. 2), a = 9.800(1) Å, b = 12.022(1) Å, c = 14.326(1) Å, α = 99.486(5)°, β = 102.673(5)°, γ = 94.591(5)°, V = 1612.3 Å 3 , Z = 2, R gt (F) = 0.046, wR ref (F 2 ) = 0.124, T = 193 K.
Open Access
Crystal structure of (1,8-diethyl-1,3,4,9-tetrahydro-pyrano[3,4-b]indol- 1-yl)acetic acid (2-hydroxy-benzylidene)hydrazide, C₂₄H₂₇N₃O₃

18. Februar 2014

Q.-B. Song, J. Zhang

Seiten: 285-286

PDF downloaden

C 24 H 27 N 3 O 3 , monoclinic, P 12 1 / c 1 (no. 14), a = 11.376(1) Å, b = 15.955(2) Å, c = 12.254(1) Å, β = 97.352(2)°, V = 2205.8 Å 3 , Z = 4, R gt (F) = 0.051, wR ref (F 2 ) = 0.152, T = 293 K.
Open Access
Crystal structure of aqua-bis(acrylato-O,O′)(1,10-phenanthroline- N,N′)zinc(II) hydrate, Zn(C₃H₃O₂)₂(H₂O)(C₁₂H₁₀N₂) · H₂O

18. Februar 2014

Q. Deng, W.-J. Jiang, Z.-S. Peng, Y.-F. Long, T.-J. Cai

Seiten: 287-288

PDF downloaden

C 18 H 18 N 2 O 6 Zn, triclinic, P 1̅ (no. 2), a = 9.2816(7) Å, b = 10.5205(8) Å, c = 11.0378(7) Å, α = 103.144(4)°, β = 99.428(4)°, γ = 111.743(3)°, V = 937.6 Å 3 , Z = 2, R gt (F) = 0.029, wR ref (F 2 ) = 0.080, T = 293 K.
Open Access
Crystal structure of bis(6,6-dimethylcyclohexadienyl)vanadium, V(C₈H₁₁)₂

18. Februar 2014

R. D. Ernst, R. Basta, A. M. Arif

Seiten: 289-290

PDF downloaden

C 16 H 22 V, monoclinic, P 12 1 / a 1 (no. 14), a = 12.1600(3) Å, b = 9.0848(3) Å, c = 13.2123(4) Å, β = 104.822(2)°, V = 1411.0 Å 3 , Z = 4, R gt (F) = 0.046, wR ref (F 2 ) = 0.110, T = 200 K.
Open Access
Crystal structure of (hydrido)(η³-butenyl)bis(η⁵-pentamethylcyclopentadienyl) zirconium, Zr(C₄H₇)[C₅(CH₃)₅]₂(H)

18. Februar 2014

R. D. Ernst, B. G. Harvey, A. M. Arif

Seiten: 291-292

PDF downloaden

C 24 H 38 Zr, triclinic, P 1̅ (no. 2), a = 8.6524(3) Å, b = 9.3669(2) Å, c = 14.2269(5) Å, α = 81.977(2)°, β = 88.117(2)°, γ = 72.557(2)°, V = 1089.2 Å 3 , Z = 2, R gt (F) = 0.034, wR ref (F 2 ) = 0.079, T = 150 K.
Open Access
Crystal structure of (η⁵-2,4-dimethylpentadienyl)[η²-rel-(aR)-a-[[(1R,5E)- 5-[(1,1-dimethylethyl)imino]-1,3-dimethyl-2-cyclopenten-1-yl]methyl]-N- (1-methylethyl)benzenemethanaminato-κN][2-(isocyano-κC)-2- methylpropane]zirconium, Zr(C₇H₁₁)(C₂₂H₃₃N₂)(C₄H₉NC)

18. Februar 2014

R. D. Ernst, V. Kulsomphob, A. M. Arif

Seiten: 293-295

PDF downloaden

C 34 H 53 N 3 Zr, triclinic, P 1̅ (no. 2), a = 10.752(4) Å, b = 12.245(3) Å, c = 12.720(5) Å, α = 82.60(2)°, β = 82.88(3)°, γ = 86.66(2)°, V = 1646.4 Å 3 , Z = 2, R gt (F) = 0.060, wR ref (F 2 ) = 0.077, T = 173 K.
Open Access
Crystal structure of bis(N-(2-aminoethyl)salicylaldiminato)iron(III) isothiocyanide, [Fe(C₉H₁₁N₂O)₂][NCS]

18. Februar 2014

X. Feng, X. Han, L.-Y. Wang

Seiten: 296-298

PDF downloaden

C 19 H 22 FeN 5 O 2 S, triclinic, P 1̅ (no. 2), a = 9.613(1) Å, b = 9.913(1) Å, c = 10.869(2) Å, α = 84.958(2)°, β = 89.047(2)°, γ = 86.098(1)°, V = 1029.3 Å 3 , Z = 2, R gt (F) = 0.038, wR ref (F 2 ) = 0.099, T = 291 K.
Open Access
Crystal structure of catena-[(1,10-phenanthroline-N,N′)- bis(μ-acetato-O,O′)lead(II)], Pb(C₁₂H₈N₂)(CH₃COO)₂

18. Februar 2014

M.-Q. Cheng, L.-F. Ma, L.-Y. Wang

Seiten: 299-300

PDF downloaden

C 16 H 14 N 2 O 4 Pb, monoclinic, C 12/ c 1 (no. 15), a = 10.945(1) Å, b = 20.499(2) Å, c = 7.4643(7) Å, β = 107.653(1)°, V = 1595.8 Å 3 , Z = 4, R gt (F) = 0.019, wR ref (F 2 ) = 0.051, T = 291 K.
Open Access
Crystal structure of dichlorobis[N-(2,6-diisopropylphenyl)- benzimidimidazolide]palladium(II), PdCl₂(C₂₂H₂₅N₃)₂

18. Februar 2014

G. Steiner, K. Wurst, B. Bildstein, H. Kopacka

Seiten: 301-302

PDF downloaden

C 44 H 50 Cl 2 N 6 Pd, monoclinic, P 12 1 / c 1 (no. 14), a = 8.9983(2) Å, b = 12.9387(3) Å, c = 18.6706(4) Å, β = 101.365(2)°, V = 2131.1 Å 3 , Z = 2, R gt (F) = 0.027, wR ref (F 2 ) = 0.072, T = 233 K.
Open Access
Crystal structure of dichloro-(3-cyclopentadienyl-3-methyl-1-phenylbutyliden- 2,6-dimethylphenylamino)chromium(III), CrCl₂(C₂₄H₂₆N)

18. Februar 2014

G. Steiner, K. Wurst, B. Bildstein, H. Kopacka

Seiten: 303-304

PDF downloaden

C 24 H 26 Cl 2 CrN, monoclinic, P 12 1 / c 1 (no. 14), a = 11.5168(5) Å, b = 13.9721(6) Å, c = 14.1146(4) Å, β = 104.628(2)°, V = 2197.6 Å 3 , Z = 4, R gt (F) = 0.039, wR ref (F 2 ) = 0.095, T = 233 K.
Open Access
Crystal structure of 2-bromobenzoic acid hydrazide, C₇H₇BrN₂O

18. Februar 2014

M. Zareef, R. Iqbal, G. Qadeer, W.-Y. Wong, H. Akhtar, M. Arfan

Seiten: 305-306

PDF downloaden

C 7 H 7 BrN 2O , monoclinic, P 12 1 / c 1 (no. 14), a = 12.769(3) Å, b = 12.754(3) Å, c = 5.026(1) Å, β = 99.874(4)°, V = 806.5 Å 3 , Z = 4, R gt (F) = 0.028, wR ref (F 2 ) = 0.074, T = 293 K.
Open Access
Crystal structure of picolinic acid hydrazide, C₆H₇N₃O

18. Februar 2014

M. Zareef, R. Iqbal, J. H. Zaidi, G. Qadeer, W.-Y. Wong, H. Akhtar

Seiten: 307-308

PDF downloaden

C 6 H 7 N 3 O, monoclinic, C 12/ c 1 (no. 15), a = 19.222(2) Å, b = 3.8987(4) Å, c = 18.115(2) Å, β = 107.095(2)°, V = 1297.6 Å 3 , Z = 8, R gt (F) = 0.038, wR ref (F 2 ) = 0.122, T = 293 K.
Open Access
Crystal structure of hexakis(μ₂-acetato)-tris(acetonitrile-κN)-μ₃-oxotrialuminum( III) tetrachloroaluminate, [Al₃(C₂H₃O₂)₆(C₂H₃N)₃O][AlCl₄]

18. Februar 2014

P. Lemoine, A. Bekaert, J. D. Brion, B. Viossat

Seiten: 309-310

PDF downloaden

C 18 H 27 Al 4 Cl 4 N 3 O 13 , orthorhombic, C 222 1 (no. 20), a = 11.867(5) Å, b = 15.421(5) Å, c = 19.181(5) Å, V = 3510.1 Å 3 , Z = 4, R gt (F) = 0.049, wR ref (F 2 ) = 0.140, T = 293 K.
Open Access
Crystal structure of 2-phenylsulfinyl-cyclohexanone, C₁₂H₁₄O₂S

18. Februar 2014

J. Zukerman-Schpector, R. Oliveira da Silva, P. R. Olivato, E. Vinhato, A. Rodrigues, C. R. Cerqueira

Seiten: 311-312

PDF downloaden

C 12 H 14 O 2 S, monoclinic, P 12 1 / a 1 (no. 14), a = 10.787(1) Å, b = 10.3955(9) Å, c = 10.888(1) Å, β = 108.928(5)°, V = 1154.9 Å 3 , Z = 4, R gt (F) = 0.047, wR ref (F 2 ) = 0.142, T = 293 K.
Open Access
Crystal structure of tetrakis(melaminium) 1,2,4,5-benzenetetracarboxylate octahydrate, (C₃H₇N₆)₄[C₆H₂(COO)₄] · 8H₂O

18. Februar 2014

Z.-X. Du, M.-L. Han, X. Feng

Seiten: 313-315

PDF downloaden

C 22 H 46 N 24 O 16 , triclinic, P 1̅ (no. 2), a = 7.0706(6) Å, b = 9.7952(8) Å, c = 14.790(1) Å, α = 105.879(1)°, β = 91.608(1)°, γ = 96.254(1)°, V = 977.6 Å 3 , Z = 1, R gt (F) = 0.049, wR ref (F 2 ) = 0.150, T = 295 K.
Open Access
Crystal structure of diiodo-bis[(4R,5R)-trans-4,5-bis[(diphenylphosphinomethyl)- 2,2-dimethyl-1,3-dioxalane]dicopper(I), Cu₂I₂(C₃₁H₃₂O₂P₂)₂

18. Februar 2014

Y.-H. Deng, Y.-L. Yang, X.-J. Yang

Seiten: 316-318

PDF downloaden

C 62 H 64 Cu 2 I 2 O 4 P 4 , triclinic, P 1̅ (no. 1), a = 10.0989(2) Å, b = 12.8084(1) Å, c = 12.8423(2) Å, α = 65.074(1)°, β = 84.31°, γ = 87.854(1)°, V = 1499.0 Å 3 , Z = 1, R gt (F) = 0.036, wR ref (F 2 ) = 0.098, T = 293 K.
Open Access
Refinement of the crystal structure of bis(2-hydroxy-1,10- phenanthroline)dicopper(I), Cu₂(C₁₂H₇N₂O)₂

18. Februar 2014

L. Yu, P.-T. Ma, J. Li, J.-P. Wang

Seiten: 319-320

PDF downloaden

C 24 H 14 Cu 2 N 4 O 2 , monoclinic, P 12 1 / n 1 (no. 14), a = 4.7747(4) Å, b = 12.688(1) Å, c = 15.446(1) Å, β = 95.316(1)°, V = 931.7 Å 3 , Z = 2, R gt (F) = 0.023, wR ref (F 2 ) = 0.062, T = 293 K.
Open Access
Crystal structure of 8-bromo-6-chloro-1′,3′,3′-trimethylspiro[2H-1-benzopyran-2,2′-indoline], C₁₉H₁₇BrClNO

18. Februar 2014

A.-Q. Wang, Y. Wu, H. Guo

Seiten: 321-322

PDF downloaden

C 19 H 17 BrClNO, tetragonal, P 4 3 (no. 78), a = 8.1499(8) Å, c = 26.863(5) Å, V = 1784.3 Å 3 , Z = 4, R gt (F) = 0.061, wR ref (F 2 ) = 0.202, T = 294 K.
Open Access
Refinement of the crystal structure of (E)-1,3-diphenyl-2-propen-1-one, C₁₅H₁₂O

18. Februar 2014

M.-H. Wu, X.-H. Yang, W.-D. Zou, W.-J. Liu, C. Li

Seiten: 323-324

PDF downloaden

C 15 H 12 O, orthorhombic, Pbcn (no. 60), a = 10.932(1) Å, b = 11.860(1) Å, c = 17.996(2) Å, V = 2333.3 Å 3 , Z = 8, R gt (F) = 0.060, wR ref (F 2 ) = 0.173, T = 292 K.
Open Access
Crystal structure of bis(cyclopropyl-4-bromosalicylaldiminato)cobalt(II), Co(C₂₀H₁₈BrNO)₂

18. Februar 2014

Y.-J. Wei, F.-W. Wang

Seiten: 325-326

PDF downloaden

C 20 H 18 Br 2 CoN 2 O 2 , orthorhombic, Pbca (no. 61), a = 13.295(2) Å, b = 13.113(2) Å, c = 23.252(3) Å, V = 4053.7 Å 3 , Z = 8, R gt (F) = 0.051, wR ref (F 2 ) = 0.151, T = 298 K.
Open Access
Crystal structure of 5,11,17,23-tetrabromo-25,27-dihydroxy- 26,28-dimethoxycalix[4]arene, C₃₀H₂₄Br₄O₄

18. Februar 2014

Y.-H. Luo, X.-J. Hu, J.-K. Liu, H. Zhang, Y. Li, H.-J. Yang, R.-J. Wang

Seiten: 327-328

PDF downloaden

C 30 H 24 Br 4 O 4 , monoclinic, P 12 1 / c 1 (no. 14), a = 9.810(1) Å, b = 27.121(6) Å, c = 11.410(3) Å, β = 110.31(1)°, V = 2846.9 Å 3 , Z = 4, R gt (F) = 0.068, wR ref (F 2 ) = 0.126, T = 295 K.
Open Access
Crystal structure of 5,17-bis(N-tert-butylhydroxyamine)-25,26,27,28- tetrapropoxycalix[4]arene, C₄₈H₆₆N₂O₆

18. Februar 2014

X.-J. Hu, H.-J. Yang, J.-K. Liu, H. Zhang, Y. Li, Y.-H. Luo, R.-J. Wang

Seiten: 329-331

PDF downloaden

C 48 H 66 N 2 O 6 , monoclinic, P 12 1 / c 1 (no. 14), a = 14.636(2) Å, b = 16.807(2) Å, c = 19.131(2) Å, β = 102.981(1)°, V = 4585.8 Å 3 , Z = 4, R gt (F) = 0.070, wR ref (F 2 ) = 0.160, T = 295 K.
Open Access
Crystal structure of catena-poly[(μ-2-aminopyrimidine-N,N′)bis(μ-chloro)- bis(triphenylphosphine)dicopper(I)], Cu₂Cl₂[P(C₆H₅)₃]₂(C₄H₅N₃)

18. Februar 2014

Q.-H. Jin, J.-C. Dong, H.-W. Gao, X.-L. Xin, L. Yang, P.-Z. Li

Seiten: 332-334

PDF downloaden

C 40 H 35 Cl 2 Cu 2 N 3 P 2 , triclinic, P 1̅ (no. 2), a = 9.5428(2) Å, b = 14.5428(3) Å, c = 15.2025(3) Å, α = 66.797(1)°, β = 72.523(1)°, γ = 78.859(1)°, V = 1842.8 Å 3 , Z = 2, R gt (F) = 0.036, wR ref (F 2 ) = 0.081, T = 273 K.
Open Access
Refinement of the crystal structure of catena-[(1,10-phenanthroline-N,N′)- (μ₃-molybdato(VI))copper(II)] monohydrate, Cu(C₁₂H₁₀N₂)(MoO₄) · H₂O

18. Februar 2014

Z.-S. Peng, W.-J. Jiang, Q. Deng, Y.-F. Long, T.-J. Cai

Seiten: 335-336

PDF downloaden

C 12 H 10 CuMoN 2 O 5 , monoclinic, P 12 1 / n 1 (no. 14), a = 14.147(3) Å, b = 5.890(1) Å, c = 16.221(3) Å, β = 103.27(1)°, V = 1315.5 Å 3 , Z = 4, R gt (F) = 0.023, wR ref (F 2 ) = 0.061, T = 298 K.
Open Access
Crystal structure of 2-(2-propynyloxy)benzaldehyde, C₁₀H₈O₂

18. Februar 2014

D. B. Werz, S. Balalaie, F. Rominger, Z. Oloumi

Seiten: 337-338

PDF downloaden

C 10 H 8 O 2 , triclinic, P 1̅ (no. 2), a = 4.3814(5) Å, b = 10.021(1) Å, c = 10.040(1) Å, α = 67.097(3)°, β = 87.762(3)°, γ = 80.576(4)°, V = 400.4 Å 3 , Z = 2, R gt (F) = 0.040, wR ref (F 2 ) = 0.089, T = 200 K.
Open Access
Crystal structure of 2-[6-(2-formylphenoxy)-2,4-hexadiynyloxy]- benzaldehyde, C₂₀H₁₄O₄

18. Februar 2014

D. B. Werz, S. Balalaie, F. Rominger, Z. Oloumi

Seiten: 339-340

PDF downloaden

C 20 H 14 O 4 , monoclinic, P 12 1 / c 1 (no. 14), a = 12.5632(6) Å, b = 4.3769(2) Å, c = 14.8059(8) Å, β = 104.213(2)°, V = 789.2 Å 3 , Z = 2, R gt (F) = 0.053, wR ref (F 2 ) = 0.145, T = 200 K.
Open Access
Crystal structure of 2′-hydroxyacetophenone nicotinoylhydrazone monohydrate, C₁₄H₁₅N₃O₃ · H₂O

18. Februar 2014

X.-S. Tai, F.-Y. Kong

Seiten: 341-342

PDF downloaden

C 14 H 15 N 3 O 3 , triclinic, P 1̅ (no. 2), a = 8.680(2) Å, b = 8.877(2) Å, c = 9.273(2) Å, α = 81.28(3)°, β = 86.26(3)°, γ = 70.48(3)°, V = 665.5 Å 3 , Z = 2, R gt (F) = 0.064, wR ref (F 2 ) = 0.177, T = 291 K.
Open Access
Crystal structure of ethanolammonium dioxo-(N-(2-ethanolato)- 2-oxy-3-methoxybenzaldiminato-O,N,O′)vanadate(V), (NH₃CH₂CH₂OH)[VO₂{(C₆H₄(OCH₃)(O)CHNCCH₂CH₂O}]

18. Februar 2014

J.-N. Feng, Y.-Z. Zhou, H.-J. Zhu, S.-J. Tu

Seiten: 343-344

PDF downloaden

C 12 H 19 N 2 O 6 V, monoclinic, P 12 1 / c 1 (no. 14), a = 8.986(2) Å, b = 13.168(2) Å, c = 13.243(2) Å, β = 108.677(2)°, V = 1484.6 Å 3 , Z = 4, R gt (F) = 0.031, wR ref (F 2 ) = 0.083, T = 294 K.
Open Access
Crystal structure of ethylenediammonium-N,N′-di-3-propionic acid tetrachloroplatinate(II), (CH₂NH₂(CH₂)₂COOH)₂[PtCl₄]

18. Februar 2014

G. N. Kaluðerović, G. A. Bogdanović, T. J. Sabo

Seiten: 345-346

PDF downloaden

C 8 H 18 Cl 4 N 2 O 4 Pt, monoclinic, P 12 1 / n 1 (no. 14), a = 8.181(3) Å, b = 10.303(5) Å, c = 9.073(6) Å, β = 103.2(1)°, V = 744.6 Å 3 , Z = 2, R gt (F) = 0.080, wR ref (F 2 ) = 0.247, T = 293 K.
Open Access
Crystal structure of rel-(3aR,4S,6aS)-4-chloromethyl-6-methyl-3,6adiphenyl- 3a,4,6,6a-tetrahydro-isoxazolo[5,4-c]isoxazole, C₁₈H₁₇ClN₂O₂

18. Februar 2014

W. Frey, S. Shiva, V. Jäger

Seiten: 347-348

PDF downloaden

C 18 H 17 ClN 2 O 2 , monoclinic, P 12 1 / c 1 (no. 14), a = 12.2900(9) Å, b = 13.325(1) Å, c = 10.482(1) Å, β = 102.69(1)°, V = 1674.7 Å 3 , Z = 4, R gt (F) = 0.053, wR ref (F 2 ) = 0.162, T = 293 K.
Open Access
Crystal structure of rel-(3aR,6aS)-6-methyl-3,6a-diphenyl-3a,4,6,6atetrahydro- isoxazolo[5,4-c]isoxazole, C₁₇H₁₆N₂O₂

18. Februar 2014

W. Frey, S. Shiva, V. Jäger

Seiten: 349-351

PDF downloaden

C 17 H 16 N 2 O 2 , orthorhombic, Pca 2 1 (no. 29), a = 5.6406(8) Å, b = 30.292(4) Å, c = 16.925(3) Å, V = 2891.9 Å 3 , Z = 8, R gt (F) = 0.084, wR ref (F 2 ) = 0.236, T = 293 K.
Open Access
Crystal structure of bis(1,10-phenanthroline-N,N′)bis(2-chlorobenzoato)- lead(II) hydrate (1:2.5), [Pb(C₇H₄O₂Cl)₂(C₁₂H₈N₂)₂] · 2.5H₂O

18. Februar 2014

H.-M. Guo, B.-S. Zhang, Y.-H. Wang

Seiten: 352-354

PDF downloaden

C 38 H 29 Cl 2 N 4 O 6.5 Pb, triclinic, P 1̅ (no. 2), a = 11.548(2) Å, b = 12.532(3) Å, c = 13.661(3) Å, α = 95.34(3)°, β = 112.60(3)°, γ = 103.23(3)°, V = 1740.4 Å 3 , Z = 2, R gt (F) = 0.037, wR ref (F 2 ) = 0.082, T = 293 K.
Open Access
Crystal structure of (2,2′-bipyridine-N,N′)bis(2-fluorobenzoato)lead(II), Pb(C₇H₄O₂F)₂(C₁₀H₈N₂)

18. Februar 2014

B.-S. Zhang

Seiten: 355-356

PDF downloaden

C 24 H 16 F 2 N 2 O 4 Pb, triclinic, P 1̅ (no. 2), a = 9.494(2) Å, b = 10.231(2) Å, c = 11.996(2) Å, α = 82.84(3)°, β = 85.53(3)°, γ = 70.25(3)°, V = 1087.3 Å 3 , Z = 2, R gt (F) = 0.027, wR ref (F 2 ) = 0.063, T = 293 K.
Open Access
Crystal structure of 4-butyl-6-nitro-2H-1,4-benzothiazin-3-one, C₁₂H₁₄N₂O₃S

18. Februar 2014

C. A. De Simone, V. L. M. Guarda, S. L. Galdino, I. R. Pitta

Seiten: 357-358

PDF downloaden

C 12 H 14 N 2 O 3 S, monoclinic, P 12 1 / n 1 (no. 14), a = 8.542(2) Å, b = 11.643(1) Å, c = 13.658(2) Å, β = 107.95(1)°, V = 1292.2 Å 3 , Z = 4, R gt (F) = 0.035, wR ref (F 2 ) = 0.094, T = 293 K.
Open Access
Crystal structure of 6-(4-difluoromethoxy-3-methoxyphenyl)-3(2H)- pyridazinone, C₁₂H₁₀F₂N₂O₃

18. Februar 2014

C. R. Doyle, M. D. Zimmerman, M. Chruszcz, M. Cymborowski, A. Gawlicka-Chruszcz, W. Minor

Seiten: 359-360

PDF downloaden

C 12 H 10 F 2 N 2 O 3 , monoclinic, P 12 1 / n 1 (no. 14), a = 7.239(1) Å, b = 15.838(1) Å, c = 10.099(1) Å, β = 91.991(6)°, V = 1157.2 Å 3 , Z = 4, R gt (F) = 0.033, wR ref (F 2 ) = 0.093, T = 109 K.
Open Access
Refinement of the crystal structure of sinoacutine, C₁₉H₂₁NO₄

18. Februar 2014

X.-L. Wang

Seiten: 361-362

PDF downloaden

C 19 H 21 NO 4 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 10.817(2) Å, b = 11.463(2) Å, c = 13.025(2) Å, V = 1615.0 Å 3 , Z = 4, R gt (F) = 0.038, wR ref (F 2 ) = 0.083, T = 297 K.
Open Access
Crystal structure of aquachloro[N,N′-bis(3-ethoxysalicylidene)ethylenediiminato] manganese(III) dihydrate, [Mn(C₂₀H₂₂N₂O₄)Cl(H₂O)] · 2H₂O

18. Februar 2014

I.-C. Hwang, K. Ha

Seiten: 363-364

PDF downloaden

C 20 H 28 ClMnN 2 O 7 , monoclinic, P 12 1 / n 1 (no. 14), a = 11.863(1) Å, b = 13.960(2) Å, c = 14.005(2) Å, β = 103.990(2)°, V = 2250.4 Å 3 , Z = 4, R gt (F) = 0.061, wR ref (F 2 ) = 0.170, T = 293 K.
Open Access
Crystal structure of aquachloro[N,N′-bis(3-ethoxysalicylidene)propylenediiminato] manganese(III) dihydrate, [Mn(C₂₁H₂₄N₂O₄)Cl(H₂O)] · 2H₂O

18. Februar 2014

I.-C. Hwang, K. Ha

Seiten: 365-366

PDF downloaden

C 21 H 30 ClMnN 2 O 7 , triclinic, P 1̅ (no. 2), a = 10.029(2) Å, b = 11.561(2) Å, c = 11.689(2) Å, α = 106.331(3)°, β = 107.874(3)°, γ = 99.092(3)°, V = 1192.8 Å 3 , Z = 2, R gt (F) = 0.071, wR ref (F 2 ) = 0.238, T = 293 K.
Open Access
Crystal structure of N-benzoyl-4,4-dimethyl-2-methylamino-2-thiazoline, C₁₃H₁₆N₂OS

18. Februar 2014

Y. B. Lee, T. H. Kim, I.-C. Hwang, K. Ha

Seiten: 367-368

PDF downloaden

C 13 H 16 N 2 OS, monoclinic, C 12/ c 1 (no. 15), a = 21.908(2) Å, b = 13.932(2) Å, c = 8.7971(9) Å, β = 101.952(2)°, V = 2626.9 Å 3 , Z = 8, R gt (F) = 0.041, wR ref (F 2 ) = 0.113, T = 293 K.
Open Access
Crystal structure of (phenanthroline-N,N′)-N-carbamoylmethyl-iminodiacetato- copper(II) dihydrate, [Cu(C₆H₈N₂)(C₁₂H₈N₂)] · 2H₂O

18. Februar 2014

M.-Q. Cheng, L.-F. Ma, L.-Y. Wang

Seiten: 369-371

PDF downloaden

C 18 H 20 CuN 4 O 7 , monoclinic, P 12 1 / c 1 (no. 14), a = 8.802(1) Å, b = 22.493(3) Å, c = 9.885(1) Å, β = 97.163(2)°, V = 1941.8Å 3 , Z = 4, R gt (F) = 0.033, wR ref (F 2 ) = 0.096, T = 291 K.
Open Access
Crystal structure of tetraaqua-bis(norfloxacin)barium(II) 1,4-benzenedicarboxylate hydrate, [Ba(H₂O)₄(C₁₆H₁₇FN₃O₃)₂][C₆H₄(COO)₂] · H₂O

18. Februar 2014

Z. An, R.-S. Wang

Seiten: 372-374

PDF downloaden

C 40 H 48 BaF 2 N 6 O 15 , triclinic, P 1̅ (no. 2), a = 12.305(1) Å, b = 12.472(1) Å, c = 16.591(2) Å, α = 101.920(2)°, β = 104.630(2)°, γ = 111.703(1)°, V = 2157.9 Å 3 , Z = 2, R gt (F) = 0.054, wR ref (F 2 ) = 0.170, T = 295 K.
Open Access
Crystal structure of caffeinium perchlorate monohydrate, (C₈H₁₁N₄O₂)[ClO₄] · H₂O

18. Februar 2014

W.-D. Wang, H. Wang, W.-J. Feng, Z.-M. Jin, M.-L. Hu

Seiten: 375-376

PDF downloaden

C 8 H 13 ClN 4 O 7 , monoclinic, P 12 1 / c 1 (no. 14), a = 13.061(2) Å, b = 6.508(1) Å, c = 16.963(4) Å, β = 112.20(1)°, V = 1335.0Å 3 , Z = 4, R gt (F) = 0.068, wR ref (F 2 ) = 0.228, T = 290 K.
Open Access
Crystal structure of (acetonitrile-N)copper(I) cyanide, [Cu(CH₃CN)][CN]

18. Februar 2014

H.-L. Keller, T. Oldag

Seiten: 377-378

PDF downloaden

C 3 H 3 CuN 2 , monoclinic, P 12 1 / c 1 (no. 14), a = 8.399(2) Å, b = 8.144(2) Å, c = 7.836(2) Å, β = 116.56(3)°, V = 479.4 Å 3 , Z = 4, R gt (F) = 0.024, wR ref (F 2 ) = 0.059, T = 120 K.
Open Access
Crystal structure of dicyano(N-(1-iminoethyl)acetamidine)palladium(II), Pd(CN)₂(C₄H₉N₃)

18. Februar 2014

H.-L. Keller, T. Oldag

Seiten: 379-380

PDF downloaden

C 6 H 9 N 5 Pd, triclinic, P 1̅ (no. 2), a = 6.906(1) Å, b = 7.371(2) Å, c = 8.784(2) Å, α = 80.67(3)°, β = 82.27(3)°, γ = 73.30(3)°, V = 420.7 Å 3 , Z = 2, R gt (F) = 0.057, wR ref (F 2 ) = 0.078, T = 150 K.
Open Access
Crystal structure of cyclonovobiocin, C₄₄H₄₂N₂O₁₂

18. Februar 2014

G. Le Bras, A. Bekaert, B. Viossat, J.-F. Peyrat, M. Alami, J. D. Brion, P. Lemoine

Seiten: 381-382

PDF downloaden

C 44 H 42 N 2 O 12 , monoclinic, P 12 1 / c 1 (no. 14), a = 5.437(5) Å, b = 32.564(5) Å, c = 10.922(5) Å, β = 99.818(5)°, V = 1905.4 Å 3 , Z = 2, R gt (F) = 0.052, wR ref (F 2 ) = 0.174, T = 293 K.
Open Access
Crystal structure of aqua(phenanthroline-N,N′)(glycinato-N,O)copper(II) bromide hydrate, [Cu(NH₂CH₂COO)(C₁₂H₈N₂)(H₂O)]Br · H₂O

18. Februar 2014

Q.-H. Jin, L. Yang, X.-L. Xin, H.-W. Gao, J.-C. Dong, P.-Z. Li

Seiten: 383-384

PDF downloaden

C 14 H 16 BrCuN 3 O 4 , monoclinic, P 12 1 / c 1 (no. 14), a = 7.1063(2) Å, b = 21.0421(7) Å, c = 11.0447(4) Å, β = 95.974(2)°, V = 1642.6 Å 3 , Z = 4, R gt (F) = 0.028, wR ref (F 2 ) = 0.078, T = 273 K.
Open Access
Refinement of the crystal structure of aquabis(2,2′-bipyridine)- bis(terephtalato)dicopper(II), Cu₂(H₂O)(C₁₀H₈N₂)₂(C₈H₄O₄)₂

18. Februar 2014

C.-C. Wang

Seiten: 385-387

PDF downloaden

C 36 H 26 Cu 2 N 4 O 9 , monoclinic, P 12 1 / c 1 (no. 14), a = 13.732(3) Å, b = 17.188(3) Å, c = 14.127(3) Å, β = 104.57(3)°, V = 3227.1 Å 3 , Z = 4, R gt (F) = 0.032, wR ref (F 2 ) = 0.089, T = 293 K.
Open Access
Crystal structure of bis[(1,3-bis(4-pyridinium)propane)]- [β-hexacosaoxooctamolybdate(VI)], (C₁₃H₁₆N₂)₂[Mo₈O₂₆]

18. Februar 2014

C.-C. Wang

Seiten: 388-390

PDF downloaden

C 26 H 32 Mo 8 N 4 O 26 , monoclinic, P 12 1 / c 1 (no. 14), a = 10.589(2) Å, b = 10.007(2) Å, c = 19.662(4) Å, β = 100.85(3)°, V = 2046.2 Å 3 , Z = 2, R gt (F) = 0.023, wR ref (F 2 ) = 0.056, T = 293 K.
Open Access
Crystal structure of bis(1,10-phenanthroline-N,N′)silver(I) mononitrate, [Ag(C₁₂H₈N₂)₂][NO₃]

18. Februar 2014

P.-G. Li, Q.-L. Wang, D.-S. Li, F. Fu, G.-C. Qi

Seiten: 391-392

PDF downloaden

C 24 H 16 AgN 5 O 3 , orthorhombic, Fddd (no. 70), a = 3.668(1) Å, b = 30.046(9) Å, c = 38.88(1) Å, V = 4284.2 Å 3 , Z = 8, R gt (F) = 0.064, wR ref (F 2 ) = 0.198, T = 273 K.
Open Access
Crystal structure of pentamethylpyrylium triiodide, [(CH₃)₅C₅O][I₃]

18. Februar 2014

S. Guo, R. Hauptmann, C. Beyer, T. Kollmann, J. J. Schneider

Seiten: 393-394

PDF downloaden

C 10 H 15 I 3 O, orthorhombic, Pnma (no. 62), a = 13.750(3) Å, b = 7.288(2) Å, c = 15.140(3) Å, V = 1517.2 Å 3 , Z = 4, R gt (F) = 0.031, wR ref (F 2 ) = 0.071, T = 150 K.
Open Access
Crystal structure of aquabis(4-aminobenzoato)cadmium dihydrate, Cd(H₂O)(NH₂C₆H₄COO)₂ · 2H₂O

18. Februar 2014

F.-Q. Cao, Y. Wang, N. Okabe, M. Odoko

Seiten: 395-397

PDF downloaden

C 14 H 18 CdN 2 O 7 , monoclinic, P 12 1 / c 1 (no. 14), a = 14.86(2) Å, b = 6.15(1) Å, c = 17.76(2) Å, β = 104.23(4)°, V = 1572.4 Å 3 , Z = 4, R gt (F) = 0.049, wR ref (F 2 ) = 0.121, T = 123 K.
Open Access
Crystal structure of (N-tert-butyl-3,4-diphenyl-1,2-oxazetidin-4-yl)methanol, C₁₉H₂₃NO₂

18. Februar 2014

S. Florio, V. Capriati, R. Luisi, A. Salomone, C. Cuocci

Seiten: 398-400

PDF downloaden

C 19 H 23 NO 2 , Pbc 21 (no. 29), a = 9.481(1) Å, b = 12.073(1) Å, c = 30.079(5) Å, V = 3443.0 Å 3 , Z = 8, R gt (F) = 0.077, wR ref (F 2 ) = 0.217, T = 293 K.
Open Access
Crystal structure of tetra(2-aminopyrimidine)dimethanolato-dicobalt(II) diperchlorate, [Co₂(CH₃O)₂(C₄H₅N₃)₄][ClO₄]₂

18. Februar 2014

S.-P. Xu, C.-H. Liu, Y. Zhu

Seiten: 401-402

PDF downloaden

C 18 H 26 Cl 2 Co 2 N 12 O 10 , monoclinic, C 12/ m 1 (no. 12), a = 16.466(5) Å, b = 14.969(5) Å, c = 12.003(4) Å, β = 132.40(1)°, V = 2184.8 Å 3 , Z = 2, R gt (F) = 0.053, wR ref (F 2 ) = 0.188, T = 293 K.
Open Access
Crystal structure of tetra(2-aminopyrimidine)dimethanolato-dinickel(II) di(tetrafluoroborate), [Ni₂(CH₃O)₂(C₄H₅N₃)₄][BF₄]₂

18. Februar 2014

S.-P. Xu, C.-H. Liu, P. Cao

Seiten: 403-404

PDF downloaden

C 18 H 26 B 2 F 8 N 12 Ni 2 O 2 , monoclinic, C 12/ m 1 (no. 12), a = 16.341(6) Å, b = 14.796(2) Å, c = 12.051(4) Å, β = 132.36(1)°, V = 2153.1 Å 3 , Z = 2, R gt (F) = 0.063, wR ref (F 2 ) = 0.201, T = 293 K.
Open Access
Crystal structure of bis(1,3-diaminepropane)carbonatomanganese(III) chloride monohydrate, [Mn(C₃H₁₀N₂)₂(CO₃)]Cl · H₂O

18. Februar 2014

S.-P. Xu, C.-H. Liu, J. Shao

Seiten: 405-406

PDF downloaden

C 7 H 22 ClMnN 4 O 4 , monoclinic, P 12 1 / n 1 (no. 14), a = 8.997(2) Å, b = 6.781(2) Å, c = 21.398(6) Å, β = 91.81(1)°, V = 1304.8 Å 3 , Z = 4, R gt (F) = 0.047, wR ref (F 2 ) = 0.132, T = 293 K.
Open Access
Crystal structure of μ-terephthalatobis[bis(1,3-diaminopropane)- manganese(II)] diperchlorate, [Mn₂{C₃H₆(NH₂)₂}₄{C₆H₄(COO)₂}][ClO₄]₂

18. Februar 2014

S.-P. Xu, C.-H. Liu, C.-H. Zhu

Seiten: 407-408

PDF downloaden

C 20 H 44 Cl 2 Mn 2 N 8 O 12 , monoclinic, P 12 1 / n 1 (no. 14), a = 10.160(3) Å, b = 10.139(4) Å, c = 16.008(3) Å, β = 93.06(1)°, V = 1646.7 Å 3 , Z = 2, R gt (F) = 0.069, wR ref (F 2 ) = 0.211, T = 293 K.
Open Access
Crystal structure of acetato-μ-N,N′-bis(salicylidene)-3-methyl- 3-aza-1,5-pentanediaminocobalt(III), Co(C₂H₃O₂)(C₂₁H₂₅N₃O₂)

18. Februar 2014

S.-P. Xu, C.-H. Liu, S.-F. Wang

Seiten: 409-410

PDF downloaden

C 23 H 28 CoN 3 O 4 , monoclinic, P 12 1 / n 1 (no. 14), a = 9.400(4) Å, b = 19.203(5) Å, c = 12.112(5) Å, β = 92.33°, V = 2184.5 Å 3 , Z = 4, R gt (F) = 0.066, wR ref (F 2 ) = 0.202, T = 293 K.
Open Access
Crystal structure of dicyclohexyl-2,2′-dipyridylamidophosphane, C₂₂H₃₀N₃P

18. Februar 2014

H. Maisel, G. Glatz, T. Irrgang, R. Kempe

Seiten: 411-412

PDF downloaden

C 22 H 30 N 3 P, monoclinic, P 12 1 / n 1 (no. 14), a = 14.0180(8) Å, b = 9.871(1) Å, c = 14.929(1) Å, β = 101.528(7)°, V = 2024.1 Å 3 , Z = 4, R gt (F) = 0.055, wR ref (F 2 ) = 0.121, T = 191 K.
Open Access
Crystal structure of bis(1,3-bis[{4-methyl-pyridin-2-yl}amido]-1,1,3,3- tetramethyldisiloxane)dichromium dichloride, [(C₁₆H₂₄N₄OSi₂)CrCl]₂

18. Februar 2014

T. Irrgang, A. Spannenberg, R. Kempe

Seiten: 413-414

PDF downloaden

C 32 H 48 Cl 2 Cr 2 N 8 O 2 Si 4 , monoclinic, P 12 1 / n 1 (no. 14), a = 12.416(2) Å, b = 13.668(3) Å, c = 13.172(3) Å, β = 113.83(3)°, V = 2044.8 Å 3 , Z = 2, R gt (F) = 0.052, wR ref (F 2 ) = 0.110, T = 200 K.
Open Access
Crystal structure of tetrakis[(4-methyl-pyridin-2-yl)-trimethylsilanylamido] zirconium(IV), Zr(C₉H₁₅N₂Si)₄

18. Februar 2014

A. Noor, T. Irrgang, R. Kempe

Seiten: 415-418

PDF downloaden

C 36 H 60 N 8 Si 4 Zr, triclinic, P 1̅ (no. 2), a = 12.0360(6) Å, b = 18.8040(9) Å, c = 21.581(1) Å, α = 69.448(4)°, β = 75.278(4)°, γ = 88.159(4)°, V = 4414.5 Å 3 , Z = 4, R gt (F) = 0.035, wR ref (F 2 ) = 0.101, T = 191 K.
Open Access
Crystal structure of 3,4,7,8-bis(1,2-dicarba-closo-dodecaborano[1,2])- 1,2,5,6-tetraselenacyclooctane benzene solvate, [(C₂B₁₀H₁₀)Se₂]₂ · C₆D₆

18. Februar 2014

Z. García-Hernández, B. Wrackmeyer, M. Herberhold, T. Irrgang, R. Kempe

Seiten: 419-420

PDF downloaden

C 10 H 26 B 20 Se 4 , monoclinic, P 12 1 / n 1 (no. 14), a = 10.3649(4) Å, b = 13.8582(7) Å, c = 18.3667(8) Å, β = 95.460(3)°, V = 2626.2 Å 3 , Z = 4, R gt (F) = 0.040, wR ref (F 2 ) = 0.097, T = 193 K.
Open Access
Crystal structure of aquabis(acrylato-O,O')(1,10-phenanthroline-N,N′)- cadmium(II), Cd(H₂O)(C₃H₃O₂)₂(C₁₂H₁₀N₂)

18. Februar 2014

T.-J. Cai, W.-J. Jiang, Z.-S. Peng, Y.-F. Long, Q. Deng

Seiten: 421-422

PDF downloaden

C 18 H 15 CdN 2 O 5 , monoclinic, P 121/ n 1 (no. 14), a = 9.9973(5) Å, b = 9.0433(4) Å, c = 19.4849(8) Å, β = 101.235(2)°, V = 1727.9 Å 3 , Z = 4, R gt (F) = 0.025, wR ref (F 2 ) = 0.065, T = 273 K.
Open Access
Crystal structure of dichloro-bis(n-pentyl)tin(IV), Sn(C₅H₁₁)₂Cl₂, tin-halide compounds - part VI

18. Februar 2014

H. Reuter, M. Izaaryene

Seiten: 423-424

PDF downloaden

C 10 H 22 Cl 2 Sn, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.5566(6) Å, b = 9.068(1) Å, c = 25.316(2) Å, V = 1505.2 Å 3 , Z = 4, R gt (F) = 0.062, wR ref (F 2 ) = 0.167, T = 258 K.

Ausgaben in diesem Band