Zeitschrift für Kristallographie - New Crystal Structures

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Volume 219, Issue 2

February 2014

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

Open Access
Crystal structure of samarium nickel tetraaluminide, SmNiAl₄

February 11, 2014

M. L. Fornasini, R. Raggio, G. Borzone

Page range: 75-76

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Al 4 NiSm, orthorhombic, Cmcm (no. 63), a = 4.0948(6) Å, b = 15.582(3) Å, c = 6.610(1) Å, V = 421.8 Å 3 , Z = 4, R gt (F) = 0.028, wR obs (F 2 ) = 0.074, T = 293 K.
Open Access
Crystal structure of samarium nickel aluminide, Sm₄Ni₆Al₂₃

February 11, 2014

M. L. Fornasini, R. Raggio, G. Borzone

Page range: 77-78

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Al 23 Ni 6 Sm 4 , monoclinic, C 12/ m 1 (no. 12), a = 15.939(3) Å, b = 4.0967(6) Å, c = 18.320(3) Å, β = 113.09(2)°, V = 1100.4 Å 3 , Z = 2, R gt (F) = 0.017, wR obs (F 2 ) = 0.040, T = 293 K.
Open Access
Crystal structure of dieuropium lithium trigermanide, Eu₂LiGe₃

February 11, 2014

Q.-X. Xie, R. Nesper

Page range: 79-80

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Eu 2 Ge 3 Li, orthorhombic, Pnnm (no. 58), a = 10.968(2) Å, b = 11.687(2) Å, c = 4.5482(7) Å, V = 583.0 Å 3 , Z = 4, R gt (F) = 0.023, wR ref (F 2 ) = 0.048, T = 293 K.
Open Access
Crystal structure of ytterbium lithium digermanide, YbLiGe₂

February 11, 2014

Q.-X. Xie, R. Nesper

Page range: 81-82

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Ge 2 LiYb, orthorhombic, Pnma (no. 62), a = 7.939(2) Å, b = 3.882(1) Å, c = 10.524(3) Å, V = 324.4 Å 3 , Z = 4, R gt (F) = 0.030, wR ref (F 2 ) = 0.064, T = 293 K.
Open Access
Crystal structure of dieuropium and distrontium di(lithium, magnesium) trigermanide, M₂Li_xMg_2–xGe₃ (M= Eu, x = 1.16;M= Sr, x = 0.94)

February 11, 2014

Q.-X. Xie, R. Nesper

Page range: 83-84

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Eu 2 Ge 3 Li 1 . 16 Mg 0.84 , orthorhombic, Cmcm (no. 63), a = 4.577(1) Å, b = 19.534(4) Å, c = 7.223(2) Å, V = 645.7 Å 3 , Z = 4, R gt (F) = 0.030, wR ref (F 2 ) = 0.072, T = 293 K. Ge3Li0.94Mg1.06Sr2, orthorhombic, Cmcm (no. 63), a = 4.6357(3) Å, b = 19.703(1) Å, c = 7.3239(5) Å, V = 669.0 Å 3 , Z = 4, R gt (F) = 0.023, wR ref (F 2 ) = 0.047, T = 293 K.
Open Access
Crystal structure of calcium zinc silicide, CaZn_xSi_2–x (x = 0.80), and strontium germanium silicide, SrGe_xSi_2–x (x = 1.20)

February 11, 2014

Q.-X. Xie, R. Nesper

Page range: 85-86

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CaSi 1.20 Zn 0.80 , hexagonal, P 6/ mmm (no. 191), a = 4.1423(3) Å, c = 4.3176(4) Å, V = 64.2 Å 3 , Z = 1, R gt (F) = 0.018, wR ref (F 2 ) = 0.042, T = 293 K. Ge 1.20 Si 0.80 Sr, hexagonal, P 6/ mmm (no. 191), a = 4.360(1) Å, c = 4.537(2) Å, V = 74.7 Å 3 , Z = 1, R gt (F) = 0.038, wR ref (F 2 ) = 0.085, T = 293 K.
Open Access
Crystal structure of pentalanthanum trilead monoiodide, La₅Pb₃I

February 11, 2014

Hj. Mattausch, A. Simon, C. Zheng

Page range: 87-88

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ILa 5 Pb 3 , hexagonal, P 63/ mcm (no. 193), a = 9.736(1) Å, c = 6.947(1) Å, V = 570.3 Å 3 , Z = 2, R gt (F) = 0.029, wR ref (F 2 ) = 0.068, T = 293 K.
Open Access
Refinement of the crystal structure of diniobium trisoxydisulfate hydrate, Nb₂O₃(SO₄)₂ · 0.25H₂O

February 11, 2014

B. Ewald, Yu. Prots, M. Boström

Page range: 89-90

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H 0.5 Nb 2 O 11.25 S 2 , trigonal, R 3̅ (no. 148), a = 10.378(2) Å, c = 26.540(5) Å, V = 2475.7 Å 3 , Z = 24, R gt (F) = 0.031, wR ref (F 2 ) = 0.072, T = 295 K.
Open Access
Crystal structure of pentabismuth heptaoxide nitrate, Bi₅O₇NO₃

February 11, 2014

P. Ziegler, M. Ströbele, H.-J. Meyer

Page range: 91-92

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Bi 5 NO 10 , monoclinic, P 12 1 / c 1 (no. 14), a = 8.5846(6) Å, b = 23.385(2) Å, c = 5.5422(4) Å, β = 108.103(8)°, V = 1057.5 Å 3 , Z = 4, R gt (F) = 0.029, wR ref (F 2 ) = 0.074, T = 210 K.
Open Access
Crystal structure of dirubidium aquapentachlorochromate(III), Rb₂[CrCl₅(H₂O)]

February 11, 2014

J.-X. Mi, X. Zhou, H. Zhang, S.-Y. Mao, J.-T. Zhao

Page range: 93-94

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Cl 5 CrH 2 ORb 2 , orthorhombic, Pnma (no. 62), a = 13.8123(5) Å, b = 9.7705(4) Å, c = 7.1522(4) Å, V = 965.2 Å 3 , Z = 4, R gt (F) = 0.038, wR ref (F 2 ) = 0.073, T = 295 K.
Open Access
Crystal structure of dicesium aquapentachlorochromate(III), Cs₂[CrCl₅(H₂O)]

February 11, 2014

J.-X. Mi, X. Zhou, H. Zhang, S.-Y. Mao, J.-T. Zhao

Page range: 95-96

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Cl 5 CrCs 2 H 2 O, orthorhombic, Cmcm (no. 63), a = 7.4297(6) Å, b = 17.234(1) Å, c = 8.0121(6) Å, V = 1025.9 Å 3 , Z = 4, R gt (F) = 0.041, wR ref (F 2 ) = 0.082, T = 295 K.
Open Access
Crystal structure of dithallium(I) octa-μ3-bromohexabromo-octahedrohexamolybdate, Tl₂[(Mo₆Br₈)Br₆]

February 11, 2014

W. Xu, Y.-Q. Zheng, P. Wang

Page range: 97-98

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Br 14 Mo 6 Tl 2 , cubic, Pn 3̅ (no. 201), a = 13.813(1) Å, V = 2635.4 Å 3 , Z = 4, R gt (F) = 0.080, wR ref (F 2 ) = 0.147, T = 295 K.
Open Access
Crystal structure of tetraaquatrissuccinatodierbium hexahydrate, Er₂(H₂O)₄(C₄H₄O₄)₃ · 6H₂O

February 11, 2014

J. Sun, Y.-Q. Zheng, J.-L. Lin

Page range: 99-100

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C 12 H 32 Er 2 O 22 , triclinic, P 1̅ (no. 2), a = 6.517(1) Å, b = 9.774(1) Å, c = 10.466(1) Å, α = 80.19(1)°, β = 89.84(1)°, γ = 71.37(1)°, V = 621.5 Å 3 , Z = 1, R gt (F) = 0.031, wR ref (F 2 ) = 0.080, T = 293 K.
Open Access
Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C₆H₅)₄]₂[VOCl₄] · 4CH₃CN, [P(C₆H₅)₄]₂[MCl₆] · 4CH₃CN (M = Sn, Mo)

February 11, 2014

Susanne Rabe, Wilfried Bubenheim, Ulrich Müller

Page range: 101-105

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C 56 H 52 Cl 4 N 4 OP 2 V, monoclinic, P 12 1 / c 1 (no. 14), a = 9.473(2) Å, b = 19.832(6) Å, c = 14.461(2) Å, β = 99.00(2)°, V = 2683.3 Å 3 , Z = 2, R gt (F) = 0.035, wR ref (F 2 ) = 0.096, T = 193 K. C 56 H 52 Cl 6 N 4 P 2 Sn, monoclinic, P 12 1 / c 1 (no. 14), a = 9.606(7) Å, b = 19.842(9) Å, c = 15.129(9) Å, β = 98.91(2)°, V = 2848.8 Å 3 , Z = 2, R gt (F) = 0.038, wR ref (F 2 ) = 0.089, T = 300 K. C 56 H 52 Cl 6 MoN 4 P 2 , monoclinic, P 12 1 / c 1 (no. 14), a = 9.505(3) Å, b = 19.624(2) Å, c = 14.759(2) Å, β = 98.72(2)°, V = 2721.1 Å 3 , Z = 2, R gt (F) = 0.062, wR ref (F 2 ) = 0.175, T = 193 K.
Open Access
Crystal structure of aquabis(4-methyl-5-formyl-imidazolfuranoylhydrazone)- (trinitrato)praseodymium(III) monohydrate, Pr(H₂O)(C₉H₁₀O₂N₄)₂(NO₃)₃·H₂O

February 11, 2014

P. M. Haba, M. Gaye, A. S. Sall, A. H. Barry, T. Jouini

Page range: 106-108

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C 20 H 24 N 11 O 15 Pr, monoclinic, P 12 1 / c 1 (no. 14), a = 18.956(4) Å, b = 8.161(2) Å, c = 22.151(3) Å, β = 114.53(2)°, V = 3117.5 Å 3 , Z = 4, R gt (F) = 0.025, wR ref (F 2 ) = 0.063, T = 293 K.
Open Access
Crystal structure of tin(II) acetate acetylacetonate, Sn(C₅H₇O₂)(C₂H₃O₂)

February 11, 2014

H. Reuter

Page range: 109-110

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C 7 H 10 O 4 Sn, monoclinic, C 12/ c 1 (no. 15), a = 12.459(3) Å, b = 9.676(2) Å, c = 16.237(3) Å, β = 99.55(2)°, V = 1930.3 Å 3 , Z = 8, R gt (F) = 0.032, wR ref (F 2 ) = 0.084, T = 293 K.
Open Access
Crystal structure of (–)-hardwickiic acid, C₁₉H₂₇OCOOH

February 11, 2014

C. Chaichantipyuth, N. Muangsin, N. Chaichit, S. Roengsumran, A. Petsom, T. Watanabe, T. Ishikawa

Page range: 111-113

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C 20 H 28 O 3 , monoclinic, P 2 1 (no. 4), a = 10.0279(2) Å, b = 11.1076(3) Å, c = 17.0856(4) Å, β = 105.522(1)°, V = 1833.7 Å 3 , Z = 4, R gt (F) = 0.058, wR ref (F 2 ) = 0.159, T = 293 K.
Open Access
Crystal structure of 3-diphenylamino-benzo[de]anthracen-7-one, C₂₉H₁₉NO

February 11, 2014

M.-X. Yu

Page range: 114-116

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C 29 H 19 NO, monoclinic, P 12 1 / c 1 (no. 14), a = 23.218(4) Å, b = 14.748(2) Å, c = 12.094(2) Å, β = 90.986(4)°, V = 4140.6 Å 3 , Z = 8, R gt (F) = 0.045, wR ref (F 2 ) = 0.085, T = 293 K.
Open Access
Crystal structure of (1,4-cyclohexanedicarboxylato)(2,2′-bipyridine)- copper(II) monohydrate, Cu(C₈H₁₀O₄)(C₁₀H₈N₂) · H₂O

February 11, 2014

A.-Q. Ma, M.-X. Yu, L.-G. Zhu

Page range: 117-118

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C 18 H 20 CuN 2 O 5 , monoclinic, P 12 1 / c 1 (no. 14), a = 9.1432(4) Å, b = 17.8251(8) Å, c = 10.1994(5) Å, β = 99.226(2)°, V = 1640.8 Å 3 , Z = 4, R gt (F) = 0.030, wR ref (F 2 ) = 0.080, T = 293 K.
Open Access
Crystal structure of 1,2,6,7,11,12-hexathia-cyclopentadecane, C₉H₁₈S₆

February 11, 2014

Y.-Q. Sun, J. Sun, Y.-W. Guo

Page range: 119-120

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C 9 H 18 S 6 , triclinic, P 1̅ (no. 2), a = 5.637(1) Å, b = 14.748(4) Å, c = 17.913(4) Å, α= 86.663(5)°, β = 82.988(4)°, γ = 83.742(4)°, V = 1467.7 Å 3 , Z = 4, R gt (F) = 0.072, wR ref (F 2 ) = 0.166, T = 293 K.
Open Access
Crystal structure of 1,2,6,7,11,12-hexathia-cyclopentadecane-4,9,14-triol, C₉H₁₈O₃S₆

February 11, 2014

Y.-Q. Sun, G. Zahn, Y.-W Guo

Page range: 121-123

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C 9 H 18 O 3 S 6 , orthorhombic, Pbca (no. 61), a = 17.419(2) Å, b = 10.6391(9) Å, c = 17.445(2) Å, V = 3232.9 Å 3 , Z = 8, R gt (F) = 0.079, wR ref (F 2 ) = 0.252, T = 293 K.
Open Access
Crystal structure of N,N′,N′′-tris(2-pyridinyl)phosphoric triamide, (NC₅H₄NH)₃PO

February 11, 2014

K. Gholivand, M. D. Alavi, M. Pourayoubi

Page range: 124-126

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C 15 H 15 N 6 OP, monoclinic, P 12 1 / n 1 (no. 14), a = 10.558(2) Å, b = 13.448(2) Å, c = 21.814(4) Å, β = 92.314(4)°, V = 3094.6 Å 3 , Z = 8, R gt (F) = 0.051, wR ref (F 2 ) = 0.101, T = 120 K.
Open Access
Crystal structure of [9,22-(bisbutyloxy)hemiporphyrazinato]nickel(II), C₃₄H₃₀N₈O₂Ni

February 11, 2014

K. Haberroth, M. Hanack, C. Maichle-Mössmer

Page range: 127-128

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C 34 H 30 N 8 NiO 2 , monoclinic, P 12 1 / n 1 (no. 14), a = 14.048(4) Å, b = 4.7256(1) Å, c = 21.491(6) Å, β = 99.10(1)°, V = 1408.7 Å 3 , Z = 2, R gt (F) = 0.054, wR ref (F) = 0.059, T = 293 K.
Open Access
Crystal structure of 5,10,15,20-tetrakis(5′-methylthien-2′-yl)porphyrin, C₄₀H₃₀N₄S₄

February 11, 2014

M. Bellizzi, P. C. D. Foss, R. Pelto, G. Crundwell, C. Brückner, J. B. Updegraff, M. Zeller, A. D. Hunter

Page range: 129-131

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C 40 H 30 N 4 S 4 , triclinic, P 1̅ (no. 2), a = 6.5126(7) Å, b = 10.499(1) Å, c = 12.635(1) Å, α = 87.818(2)°, β = 79.141(2)°, γ = 86.737(2)°, V = 846.7 Å 3 , Z = 1, R gt (F) = 0.057, wR ref (F 2 ) = 0.150, T = 100 K.
Open Access
Crystal structure of (2R,2′R,5R,5′R)-1,1′-bis[1-(2-tert-butyl-1-carboxytert- butyl-3-methyl-4-oxo-imidazolidine-5-yl)-1-methyl]ferrocene, Fe(C₂₁H₃₃N₂O₃)₂

February 11, 2014

H. Nöth, H. Dialer, T. Habereder, W. Beck

Page range: 132-134

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C 42 H 66 FeN 4 O 6 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 10.7723(9) Å, b = 11.7128(8) Å, c = 33.392(3) Å, V = 4213.2 Å 3 , Z = 4, R gt (F) = 0.071, wR ref (F 2 ) = 0.158, T = 193 K.
Open Access
Crystal structure of diaqua-bis(pyrazole)-μ2-squarato(1,3)nickel(II), Ni(C₄O₄)(C₃H₄N₂)₂(H₂O)₂

February 11, 2014

R. Kirchmaier, E. Altin, A. Lentz

Page range: 135-136

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C 10 H 12 N 4 NiO 6 , orthorhombic, Pbca (no. 61), a = 11.890(3) Å, b = 7.909(2) Å, c = 14.664(4) Å, V = 1378.9 Å 3 , Z = 4, R gt (F) = 0.028, wR ref (F 2 ) = 0.068, T = 293 K.
Open Access
Crystal structure of diaqua-bis(pyridine-2,6-dicarboxylato-O,N,O′)-(μ2- pyrazino)dicopper(II) dihydrate, [Cu₂(C₄H₄N₂)(C₇H₃NO₄)₂(H₂O)₂] · 2H₂O

February 11, 2014

E. Altin, R. Kirchmaier, A. Lentz

Page range: 137-138

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C 18 H 18 Cu 2 N 4 O 12 , monoclinic, P 12 1 / n 1 (no. 14), a = 5.808(1) Å, b = 15.541(3) Å, c = 11.962(3) Å, β = 92.79(3)°, V = 1078.3 Å 3 , Z = 2, R gt (F) = 0.028, wR ref (F 2 ) = 0.079, T = 293 K.
Open Access
Crystal structure of tetraaqua-bis(pyridine-2,6-dicarboxylato-O,N,O′)- (μ2-pyrazino)dinickel(II), [Ni₂(C₄H₄N₂)(C₇H₃NO₄)₂(H₂O)₄]

February 11, 2014

E. Altin, R. Kirchmaier, A. Lentz

Page range: 139-140

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C 18 H 18 N 4 Ni 2 O 12 , monoclinic, P 12 1 / c 1 (no. 14), a = 7.558(2) Å, b = 20.004(3) Å, c = 7.135(2) Å, β = 92.02(3)°, V = 1078.1 Å 3 , Z = 2, R gt (F) = 0.023, wR ref (F 2 ) = 0.061, T = 293 K.
Open Access
Crystal structure of aqua[1,3-bis(2-pyridylimino)isoindolinato](salicylato)- copper(II), Cu(C₇O₃H₄)(C₁₈H₁₂N₅)(H₂O)

February 11, 2014

J. Kaizer, J. Pap, G. Speier, L. Párkányi

Page range: 141-142

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C 25 H 18 CuN 5 O 4 , triclinic, P 1̅ (no. 2), a = 7.300(1) Å, b = 11.985(1) Å, c = 13.190(1) Å, α = 88.15(1)°, β = 78.68(1)°, γ = 78.62(1)°, V = 1109.3 Å 3 , Z = 2, R gt (F) = 0.048, wR ref (F 2 ) = 0.134, T = 293 K.
Open Access
Crystal structure of [N,N-bis(2-[2-pyridyl]ethyl)-2-(2-aminoethoxy)ethanol]- copper(II) bis(trifluoromethanesulfonate), (CuC₁₈H₂₅N₃O₂)(F₃CSO₃)₂

February 11, 2014

K. Selmeczi, G. Speier, M. Réglier, M. Giorgi

Page range: 143-144

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C 20 H 25 CuF 6 N 3 O 8 S 2 , triclinic, P 1̅ (no. 2), a = 8.0561(4) Å, b = 11.766(1) Å, c = 14.859(1) Å, α = 75.539(3)°, β = 84.980(5)°, γ = 82.435(5)°, V = 1349.8 Å 3 , Z = 2, R gt (F) = 0.068, wR ref (F 2 ) = 0.135, T = 293 K.
Open Access
Crystal structure of 2-hydroxyimino-3-oxo-3-phenyl-propionic acid ethyl ester, C₁₁H₁₁NO₄

February 11, 2014

M. Ramos Silva, A. Matos Beja, J. A. Paixão, S. H. Lopes, Ana M. T. D. P. V. Cabral, A. M. d′A. Rocha Gonsalves, A. J. F. N. Sobral

Page range: 145-146

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C 11 H 11 NO 4 , orthorhombic, Pna 2 1 (no. 33), a = 18.370(4) Å, b = 4.870(1) Å, c = 24.616(2) Å, V = 2202.4 Å 3 , Z = 8, R gt (F) = 0.082, wR ref (F 2 ) = 0.203, T = 293 K.
Open Access
Crystal structure of bis(8-chloro-5-(4-methylpiperazinium-1-yl)pyrido- [2,3-b][1,5]benzoxazepine) fumarate – fumaric acid solvate (1:1), (C₁₇H₁₈ClN₄O)₂(C₄H₂O₄) · C₄H₄O₄

February 11, 2014

L. Dupont, J.-F. Liégeois

Page range: 147-149

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C 42 H 42 Cl 2 N 8 O 10 , triclinic, P 1̅ (no. 2), a = 9.625(1) Å, b = 9.929(3) Å, c = 11.860(2) Å, α = 108.12(2)°, β = 73.24(1)°, γ = 87.38(1)°, V = 1019.9 Å 3 , Z = 1, R gt (F) = 0.043, wR ref (F 2 ) = 0.131, T = 293 K.
Open Access
Crystal structure of sulfatobis{2-[N-(2-hydroxyethylaminoethyl)iminomethyl] phenolatozinc(II)}, [(ZnC₁₁H₁₅N₂O₂)₂SO₄]

February 11, 2014

X.-Y. Qiu, Q.-X. Liu, Z.-G. Wang, Y.-S. Lin, W.-J. Zeng, H.-K. Fun, H.-L. Zhu

Page range: 150-152

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C 22 H 30 N 4 O 8 SZn 2 , monoclinic, P 12 1 / c 1 (no. 14), a = 8.2666(6) Å, b = 23.229(2) Å, c = 13.7531(9) Å, β = 102.329(1)°, V = 2580.1 Å 3 , Z = 4, R gt (F) = 0.050, wR ref (F 2 ) = 0.114, T = 293 K.
Open Access
Crystal structure of 1,3-di[2-(4,5-dihydrooxazole)]benzene, C₁₂H₁₂N₂O₂

February 11, 2014

S.-H. Chen, S.-F. Li, Y. Zou, L. Yang, B. Chen, H.-L. Zhu

Page range: 153-154

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C 12 H 12 N 2 O 2 , monoclinic, P 12 1 / c 1 (no. 14), a = 7.033(4) Å, b = 14.768(9) Å, c = 10.377(6) Å, β = 96.026(9)°, V = 1071.8 Å 3 , Z = 4, R gt (F) = 0.054, wR ref (F 2 ) = 0.181, T = 293 K.
Open Access
Crystal structure of bis[N-(2-(2-hydroxyethylamino)ethyl)salicylideneimine] cadmium(II) dihydrate, Cd(C₁₁H₁₇N₂O₂)₂ · 2H₂O

February 11, 2014

S. Yang, Q.-X. Liu, W.-J. Zeng, Y. Zou, Z.-G. Wang, H.-L. Zhu

Page range: 155-156

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C 22 H 34 CdN 4 O 6 , monoclinic, P 12 1 / n 1 (no. 14), a = 9.236(4) Å, b = 21.102(9) Å, c = 12.987(6) Å, β = 97.638(6)°, V = 2508.7 Å 3 , Z = 4, R gt (F) = 0.039, wR ref (F 2 ) = 0.117, T = 298 K.
Open Access
Crystal structure of bis(2-aminopyrimidine)silver(I) hexafluoroarsenate bis(2-aminopyrimidine) solvate, [Ag(C₄H₅N₃)₂]AsF₆ · 2C₄H₅N₃

February 11, 2014

H.-L. Yang, S. Yang, X.-Y. Qiu, S.-C. Shao, J.-L. Ma, L. Sun, H.-L. Zhu

Page range: 157-158

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C 16 H 20 AgAsF 6 N 12 , triclinic, P 1̅ (no. 2), a = 7.004(1) Å, b = 8.696(2) Å, c = 11.006(2) Å, α = 68.95(3)°, β = 76.49(3)°, γ = 81.90(3)°, V = 607.1 Å 3 , Z = 1, R gt (F) = 0.044, wR ref (F 2 ) = 0.111, T = 293 K.
Open Access
Crystal structure of bis(4-aminopyridine)silver(I) bis(3-nitrobenzoato)- silver(I) dihydrate, Ag(C₅H₆N₂)₂[Ag(C₇H₄NO₄)₂] · 2H₂O

February 11, 2014

J.-L. Ma, Y. Zou, F.-J. Meng, Y.-S. Lin, Z.-G. Wang, H.-L. Zhu

Page range: 159-160

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C 24 H 24 Ag 2 N 6 O 10 , triclinic, P 1̅ (no. 2), a = 3.807(3) Å, b = 11.55(1) Å, c = 16.21(1) Å, α = 74.17(1)°, β = 84.75(1)°, γ = 89.89(1)°, V = 682.6 Å 3 , Z = 1, R gt (F) = 0.045, wR ref (F 2 ) = 0.153, T = 293 K.
Open Access
Crystal structure of bis[N,N′-bis(2-fluorobenzylidene)ethylenediamine]silver( I) 4-chlorobenzoate 4-chlorobenzoic acid, Ag(C₁₆H₁₄N₂F₂)₂(C₁₄H₉O₂Cl₂)

February 11, 2014

J.-L. Ma, L. Yang, B. Chen, Y. Zou, F.-J. Meng, H.-L. Zhu

Page range: 161-162

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C 46 H 37 AgCl 2 F 4 N 4 O 4 , orthorhombic, Pccn (no. 56), a = 27.93(1) Å, b = 7.208(3) Å, c = 21.083(8) Å, V = 4244.0 Å 3 , Z = 4, R gt (F) = 0.035, wR ref (F 2 ) = 0.069, T = 298 K.
Open Access
Crystal structure of diaquatetra(3,5-dinitrobenzoato)tetrasilver(I), Ag₄(C₇H₃N₂O₆)₄(H₂O)₂

February 11, 2014

J. Xia, Z.-G. Wang, L. Yang, L.-L. Tang, H.-L. Zhu

Page range: 163-164

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C 28 H 16 Ag 4 N 8 O 26 , monoclinic, P 12 1 / c 1 (no. 14), a = 5.667(1) Å, b = 16.915(3) Å, c = 19.694(4) Å, β = 90.38(3)°, V = 1887.8 Å 3 , Z = 2, R gt (F) = 0.065, wR ref (F 2 ) = 0.177, T = 293 K.
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Crystal structure of bis[di(1,10-phenanthroline)azidocopper(II)] biphenyl- 4,4′-dicarboxylate pentahydrate, [Cu(C₁₂H₈N₂)₂N₃]₂(C₁₄H₈O₄) · 5H₂O

February 11, 2014

M.-D. Ye, Y.-Q. Cheng, X.-H. Li, M.-L. Hu

Page range: 165-167

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C 62 H 50 Cu 2 N 14 O 9 , monoclinic, P 12/ n 1 (no. 13), a = 15.7454(6) Å, b = 7.9119(3) Å, c = 22.3267(9) Å, β = 96.150(2)°, V = 2765.4 Å 3 , Z = 2, R gt (F) = 0.071, wR ref (F 2 ) = 0.144, T = 293 K.
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Crystal structure of catena-bis-μ-terephthalato[2,2′-bipyridinecobalt(II)] [aqua-2,2′-bipyridinecobalt(II)], Co₂(C₈H₄O₄)₂(C₁₀H₈N₂)₂(H₂O)

February 11, 2014

F. Chen, M.-L. Hu, M.-D. Ye, H.-P. Xiao

Page range: 168-170

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C 36 H 26 Co 2 N 4 O 9 , monoclinic, P 12 1 / c 1 (no. 14), a = 13.8648(7) Å, b = 17.1789(9) Å, c = 14.1938(7) Å, β = 104.525(1)°, V = 3272.7 Å 3 , Z = 4, R gt (F) = 0.076, wR ref (F 2 ) = 0.151, T = 298 K.
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Crystal structure of 2,3-bis(2-cyanoethylthio)-6,7-vinylenedithiotetrathiafulvalene, C₁₄H₁₀N₂S₈

February 11, 2014

G. Xue, W.-T. Yu, Q. Fang

Page range: 171-172

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C 14 H 10 N 2 S 8 , triclinic, P 1̅ (no. 2), a = 7.753(2) Å, b = 11.403(3) Å, c = 12.371(5) Å, α = 64.10(2)°, β = 84.62(2)°, γ = 77.34(2)°, V = 959.9 Å 3 , Z = 2, R gt (F) = 0.061, wR ref (F 2 ) = 0.168, T = 293 K.
Open Access
Crystal structure of {1-benzyl-2-[(4-nitrobenzyl)sulfanyl]-1H-imidazol-5-yl}- methanol, C₁₈H₁₇N₃O₃S

February 11, 2014

A. Ramazani, F. Marandi, A. Souldozi, A. R. Jalilian

Page range: 173-174

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C 18 H 17 N 3 O 3 S, monoclinic, P 12 1 / c 1 (no. 14), a = 15.705(2) Å, b = 12.083(2) Å, c = 9.368(1) Å, β = 102.404(3)°, V = 1736.3 Å 3 , Z = 4, R gt (F) = 0.078, wR ref (F 2 ) = 0.226, T = 120 K.
Open Access
Crystal structure of dimethyl 1-acetyl-1,2-dihydro-2,3-quinolinedicarboxylate, C₁₅H₁₅NO₅

February 11, 2014

A. Ramazani, L. Dolatyari, A. R. Kazemizadeh, A. Souldozi

Page range: 175-176

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C 15 H 15 NO 5 , triclinic, P 1̅ (no. 2), a = 7.366(1) Å, b = 8.884(2) Å, c = 11.242(2) Å, α = 68.640(4)°, β = 81.328(4)°, γ = 85.050(4)°, V = 676.9 Å 3 , Z = 2, R gt (F) = 0.064, wR ref (F 2 ) = 0.151, T = 120 K.
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Crystal structure of dimethyl 1,1-diacetyl-8a-hydroxy-8-oxo-1,2,8,8a-tetrahydrocyclopenta[ a]indene-2,3-dicarboxylate, C₂₀H₁₈O₈

February 11, 2014

A. Ramazani

Page range: 177-178

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C 20 H 18 O 8 , orthorhombic, Fdd 2 (no. 43), a = 19.060(4) Å, b = 35.937(7) Å, c = 10.571(2) Å, V = 7240.6 Å 3 , Z = 16, R gt (F) = 0.056, wR ref (F 2 ) = 0.139, T = 110 K.
Open Access
Crystal structure of dimethyl (Z)-2(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)- 2-butenedioate, C₁₄H₁₁NO₆

February 11, 2014

A. Ramazani, F. Marandi, E. Ahmadi, A. Morsali

Page range: 179-180

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C 14 H 11 NO 6 , monoclinic, P 12 1 / n 1 (no. 14), a = 8.068(2) Å, b = 9.679(2) Å, c = 16.961(3) Å, β = 101.69(3)°, V = 1297.1 Å 3 , Z = 4, R gt (F) = 0.076, wR ref (F 2 ) = 0.160, T = 120 K.
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Crystal structure of diethyl 2-(dibenzoylmethyl)-3-(triphenylphosphoranylidene) succinate, C₄₁H₃₇O₆P

February 11, 2014

A. Ramazani, L. Dolatyari, A. R. Kazemizadeh, E. Ahmad, A. A. Torabi, R. Welter

Page range: 181-183

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C 41 H 37 O 6 P, triclinic, P 1̅ (no. 2), a = 11.128(5) Å, b = 12.548(5) Å, c = 13.420(5) Å, α = 87.523(5)°, β = 84.819(5)°, γ = 64.188(5)°, V = 1680.0 Å 3 , Z = 2, R gt (F) = 0.058, wR ref (F 2 ) = 0.148, T = 173 K.
Open Access
Crystal structure of 2-(6-[2-(5-ethyl-5-hydroxy-6-methyl-tetrahydro-pyran- 2-yl)-15-oxo-2,10,12-trimethyl-1,6,8-trioxa-dispiro[4.1.5.3]pentadec-13-en- 9-yl]-2-hydroxy-1,3-dimethyl-4-oxo-heptyl-5-methyl-tetrahydro-pyran- 2-yl)-butyrate sodium, Na(C₄₂H₆₇O₁₁), SY-9 – antibiotic 20-oxo-salinomycin

February 11, 2014

E. F. Paulus, L. Vértesy

Page range: 184-186

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C 42 H 67 NaO 11 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 10.5617(5) Å, b = 19.1580(9) Å, c = 21.5366(9) Å, V = 4357.7 Å 3 , Z = 4, R gt (F) = 0.035, wR ref (F 2 ) = 0.082, T = 293 K.
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Crystal structure of 2-(3-methoxyphenylethynyl)-6-methylpyridine, C₁₅H₁₃NO, M-MPEP – a mGluR5 antagonist

February 11, 2014

D. Alagille, R. M. Baldwin, C. D. Incarvito, G. Tamagnan

Page range: 187-188

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C 15 H 13 NO, monoclinic, P 12 1 / c 1 (no. 14), a = 15.986(3) Å, b = 6.760(1) Å, c = 11.415(2) Å, β = 104.63(3)°, V = 1193.5 Å 3 , Z = 4, R gt (F) = 0.055, wR ref (F 2 ) = 0.139, T = 183 K.
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Crystal structure of 4-methylanilinium dihydrogenphosphate, ( p-CH₃C₆H₄NH₃)(H₂PO₄)

February 11, 2014

W. Smirani, A. Ben Slimane, M. Rzaigui

Page range: 189-190

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C 7 H 12 NO 4 P, orthorhombic, Pbca (no. 61), a = 7.790(3) Å, b = 24.645(4) Å, c = 9.867(2) Å, V = 1894.3 Å 3 , Z = 8, R gt (F) = 0.048, wR ref (F) = 0.053, T = 296 K.
Open Access
Crystal structure of (3R,1S′,2S′)-3-[1-benzyloxy-2,3-isopropylidenedioxypropyl]- 2-methyltetrahydro-1,2-oxazole, C₁₇H₂₅NO₄

February 11, 2014

W. Frey, M. Henneböhle, V. Jäger

Page range: 191-192

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C 17 H 25 NO 4 , monoclinic, P 12 1 1 (no. 4), a = 8.547(3) Å, b = 9.176(2) Å, c = 11.166(2) Å, β = 102.24(2)°, V = 855.8 Å 3 , Z = 2, R gt (F) = 0.053, wR ref (F 2 ) = 0.137, T = 293 K.
Open Access
Crystal structure of (3S,4S)-4,5-O-cyclohexylidene-4,5-dihydroxy-3- methylamino-pentanoic acid hydrochloride, (C₁₂H₂₂NO₄)Cl

February 11, 2014

W. Frey, M. Henneböhle, V. Jäger

Page range: 193-194

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C 12 H 22 ClNO 4 , monoclinic, P 12 1 1 (no. 4), a = 6.2327(3) Å, b = 7.9360(3) Å, c = 14.1536(5) Å, β = 99.709(4)°, V = 690.1 Å 3 , Z = 2, R gt (F) = 0.042, wR ref (F 2 ) = 0.115, T = 293 K.
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Crystal structure of chlorodimethyl(2-aminoethanethiolato)tin(IV), (NH₂CH₂CH₂S)SnCl(CH₃)₂

February 11, 2014

M. D. Couce, G. Faraglia, U. Russo, R. Graziani, G. Valle

Page range: 195-196

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C 4 H 12 ClNSSn, orthorhombic, Pbca (no. 61), a = 11.422(2) Å, b = 11.475(2) Å, c = 13.582(2) Å, V = 1780.2 Å 3 , Z = 8, R gt (F) = 0.057, wR ref (F 2 ) = 0.147, T = 293 K.
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Crystal structure of methyl-2-hydroxy-2-phenyl-3-(4-bromophenyl)-3- phenylamino-propanoate, C₂₂H₂₀BrNO₃

February 11, 2014

L. Malpezzi

Page range: 197-198

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C 22 H 20 BrNO 3 , monoclinic, P 12 1 / c 1 (no. 14), a = 17.643(1) Å, b = 5.935(1) Å, c = 18.782(1) Å, β = 90.13(1)°, V = 1966.7 Å 3 , Z = 4, R gt (F) = 0.041, wR ref (F 2 ) = 0.117, T = 293 K.
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Crystal structure of (η⁴-norborna-2,5-dien)-(1,2-bis((R,R)-2,5-bis- (methoxymethyl)phospholanyl)benzene)rhodium(I) tetrafluoroborate, [Rh(C₂₂H₃₆O₄P₂)(C₇H₈)](BF₄)

February 11, 2014

J. Holz, A. Börner, A. Spannenberg, C. Pribbenow, D. Heller, H.-J. Drexler

Page range: 199-200

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C 29 H 44 BF 4 O 4 P 2 Rh, monoclinic, P 2 1 (no. 4), a = 10.119(2) Å, b = 14.125(3) Å, c = 11.542(2) Å, β = 106.87(3)°, V = 1578.7 Å 3 , Z = 2, R gt (F) = 0.034, wR ref (F 2 ) = 0.090, T = 200 K.
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Crystal structure of (η⁴-cycloocta-1,5-dien)(1,2-bis(diethylphosphino)- ethane)rhodium(I) tetrafluoroborate, [Rh(C₈H₁₂)(C₁₀H₂₄P₂)](BF₄)

February 11, 2014

R. Kempe, A. Spannenberg, D. Heller, H.-J. Drexler

Page range: 201-202

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C 18 H 36 BF 4 P 2 Rh, monoclinic, P 12 1 / n 1 (no. 14), a = 15.522(3) Å, b = 9.173(2) Å, c = 15.862(3) Å, β = 103.91(3)°, V = 2192.3 Å 3 , Z = 4, R gt (F) = 0.037, wR obs (F 2 ) = 0.087, T = 200 K.

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