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Synthesis and Characterization of Ammonium Acesulfamate

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Published/Copyright: June 2, 2014
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Zeitschrift für Naturforschung B
From the journal Zeitschrift für Naturforschung B Volume 69 Issue 6

Ammonium acesulfamate, (NH4)C4H4NO4S, was prepared by the reaction of acesulfamic acid and ammonium carbonate in aqueous solution, and characterized by elemental analysis and 1H and 13C NMR spectroscopy. Its crystal and molecular structure was determined by single-crystal X-ray diffraction methods. The substance crystallizes in the orthorhombic space group Pnma with Z = 4 molecules per unit cell. The NH4+ ion generates medium to strong hydrogen bonds with the carbonylic oxygen, the iminic nitrogen and the sulfonyl oxygen atoms of the acesulfamate anion. The FTIR spectrum of the compound was also recorded and is briefly discussed.

Graphical Abstract

Synthesis and Characterization of Ammonium Acesulfamate

Synthesis and Characterization of Ammonium Acesulfamate

Keywords: Ammonium Acesulfamate; Synthesis; Crystal Structure; FTIR Spectra
Received: 2014-3-3
Published Online: 2014-6-2
Published in Print: 2014-6-1

© 1946 – 2014: Verlag der Zeitschrift für Naturforschung

Articles in the same Issue

  1. Synthesis and Crystal Structure of a “High-temperature” Phase of Li[H2NC(O)NH], the Missing Alkali-Metal Ureate
  2. Strukturen von polaren Magnesiumorganylen: Synthese und Struktur von Basen-Addukten des Bis(pentamethylcyclopentadienyl)magnesiums
  3. The Mixed-valent Mercury(I/II) Compounds Hg3(HAsO4)2 and Hg6As2O10
  4. New Intermetallic Zinc Compounds with Ordering Variants of the KHg2 and LT-SrZn5 Type
  5. Effects of Metal Ions and N-Donor Ligands with Different Coordination Characters on the Construction of d10 Metal-organic Complexes with Selective Photocatalytic Activities
  6. Synthesis and Characterization of Novel Re(BIAN)(CO)3Cl Derivatives Including the First Example of a Water-soluble Tricarbonyl Rhenium(I) Complex with Bis(imino)acenaphthene Ligands
  7. Hydrothermal Synthesis and Crystal Structure of a One-dimensional Cobalt (II) Coordination Polymer with Two Organic Ligands
  8. Vinylsilylferrocenes and Ethynyl(vinyl)silylferrocenes. Synthesis, Multinuclear Magnetic Resonance Study and DFT Calculations
  9. One-pot Multi-component Synthesis of Mono- and Bis-indolylimidazole Derivatives Using Zn2+@KSF and Their Antibacterial Activity
  10. Catalyst-free, Solvent-promoted and Scalable Multicomponent Synthesis of 3-Aminoalkylated Indoles via a Mannich-type Reaction
  11. Synthesis and Reactions of New Chiral Linear Dipeptide Candidates Using Nalidixic Acid as Starting Material
  12. Synthesis and Characterization of Ammonium Acesulfamate
  13. Two Rare Hydroazulene-type Sesquiterpenes from the Roots of Aristolochia yunnanensis
  14. Spiroalkaloids and Coumarins from the Stem Bark of Pauridiantha callicarpoides
https://doi.org/10.5560/znb.2014-4061
Keywords for this article
Ammonium Acesulfamate; Synthesis; Crystal Structure; FTIR Spectra

Articles in the same Issue

  1. Synthesis and Crystal Structure of a “High-temperature” Phase of Li[H2NC(O)NH], the Missing Alkali-Metal Ureate
  2. Strukturen von polaren Magnesiumorganylen: Synthese und Struktur von Basen-Addukten des Bis(pentamethylcyclopentadienyl)magnesiums
  3. The Mixed-valent Mercury(I/II) Compounds Hg3(HAsO4)2 and Hg6As2O10
  4. New Intermetallic Zinc Compounds with Ordering Variants of the KHg2 and LT-SrZn5 Type
  5. Effects of Metal Ions and N-Donor Ligands with Different Coordination Characters on the Construction of d10 Metal-organic Complexes with Selective Photocatalytic Activities
  6. Synthesis and Characterization of Novel Re(BIAN)(CO)3Cl Derivatives Including the First Example of a Water-soluble Tricarbonyl Rhenium(I) Complex with Bis(imino)acenaphthene Ligands
  7. Hydrothermal Synthesis and Crystal Structure of a One-dimensional Cobalt (II) Coordination Polymer with Two Organic Ligands
  8. Vinylsilylferrocenes and Ethynyl(vinyl)silylferrocenes. Synthesis, Multinuclear Magnetic Resonance Study and DFT Calculations
  9. One-pot Multi-component Synthesis of Mono- and Bis-indolylimidazole Derivatives Using Zn2+@KSF and Their Antibacterial Activity
  10. Catalyst-free, Solvent-promoted and Scalable Multicomponent Synthesis of 3-Aminoalkylated Indoles via a Mannich-type Reaction
  11. Synthesis and Reactions of New Chiral Linear Dipeptide Candidates Using Nalidixic Acid as Starting Material
  12. Synthesis and Characterization of Ammonium Acesulfamate
  13. Two Rare Hydroazulene-type Sesquiterpenes from the Roots of Aristolochia yunnanensis
  14. Spiroalkaloids and Coumarins from the Stem Bark of Pauridiantha callicarpoides
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