In-line Ultrasonic Monitoring of Filler Dispersion during Extrusion
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J. Tatibouët
Abstract
Mechanical and rheological properties of filled polymers are very sensitive to the filler dispersion. Classical methods for evaluating dispersion are based on optical or scanning electron microscopy observations on extruded specimens. They cannot be used in-line and are generally time consuming. We present here an in-line characterisation technique to evaluate the dispersion of calcium carbonate, CaCO3, in polypropylene. The technique is based on the monitoring of velocity and attenuation of ultrasounds in the flowing material. These properties are measured in a specially instrumented die placed at the end of a single screw extruder. Measurements were made for filler concentrations up to 60 wt.%. In-line data are compared to dispersion indexes measured by an optical method on 25 micron thick films.
© 2002, Carl Hanser Verlag, Munich
Artikel in diesem Heft
- Editorial
- Twelfth of a Series: Father of Synthetic Fiber Industry Wallace Hume Carothers
- Special Paper
- The Matching of Experimental Polymer Processing Flows to Viscoelastic Numerical Simulation
- Single and Twin Screw Extrusion
- Polymer Pellet Flow out of the Hopper into the First Section of a Single Screw
- Estimation of Residence Time Distribution in two Elements of a Ko-Kneader
- Flow Characteristics of Screws and Special Mixing Enhancers in a Co-rotating Twin Screw Extruder
- Reactive Extrusion
- Bulk Polymerization of ε-Caprolactone in an Internal Mixer and in a Twin Screw Extruder
- Die Extrusion
- Flow Instabilities of Linear PE in Capillary Dies
- In-line Ultrasonic Monitoring of Filler Dispersion during Extrusion
- Fibers and Film
- Birefringence and Mechanical Property Development in Melt Spinning Cyclopolyolefin Filaments
- Injection Molding
- An Empirical Study of the Surface Blush in Gas-Assisted Injection Molded Parts
- Use of the Fast-cool pVT Data for Shrinkage Analysis in Injection Molding
- Composite Processing
- Impregnation Behaviors in Composite Processing
Artikel in diesem Heft
- Editorial
- Twelfth of a Series: Father of Synthetic Fiber Industry Wallace Hume Carothers
- Special Paper
- The Matching of Experimental Polymer Processing Flows to Viscoelastic Numerical Simulation
- Single and Twin Screw Extrusion
- Polymer Pellet Flow out of the Hopper into the First Section of a Single Screw
- Estimation of Residence Time Distribution in two Elements of a Ko-Kneader
- Flow Characteristics of Screws and Special Mixing Enhancers in a Co-rotating Twin Screw Extruder
- Reactive Extrusion
- Bulk Polymerization of ε-Caprolactone in an Internal Mixer and in a Twin Screw Extruder
- Die Extrusion
- Flow Instabilities of Linear PE in Capillary Dies
- In-line Ultrasonic Monitoring of Filler Dispersion during Extrusion
- Fibers and Film
- Birefringence and Mechanical Property Development in Melt Spinning Cyclopolyolefin Filaments
- Injection Molding
- An Empirical Study of the Surface Blush in Gas-Assisted Injection Molded Parts
- Use of the Fast-cool pVT Data for Shrinkage Analysis in Injection Molding
- Composite Processing
- Impregnation Behaviors in Composite Processing
