Method for the Detection of Grain Boundaries in α Ti-Based Alloys by means of Polarized Light Microscopy and Image Processing in MATLAB
-
L. Morales-Rivas
Abstract
Metallographic methods which are typically comprising chemical etching processes are applied to reveal grain boundaries in sections of metallic materials. In the case of an optically anisotropic material, grain boundaries can also be detected suing polarized light microscopy (PLM). To this end, the identification of grain boundaries, an automated image processing procedure, based on PLM, was developed. In this context, two different α Ti-based alloys were examined: a cast, non-porous rod material and a material obtained by powder metallurgy which, owing to its high porosity, places specific demands on the image processing system. The present work outlines the underlying metallographic and computer-based methods.
Kurzfassung
Um Korngrenzen in Schliffen metallischer Werkstoffe sichtbar zu machen, werden metallographische Methoden angewendet, die für gewöhnlich chemische Ätzvorgänge beinhalten. Handelt es sich um einen optisch anisotropen Werkstoff, so ist es auch möglich, Korngrenzen mittels polarisierter Lichtmikroskopie (PLM) zu detektieren. Dazu wurde eine automatisierte, auf PLM-Aufnahmen basierende Bildverarbeitungsprozedur zur Identifikation von Korngrenzen entwickelt. Hierbei wurden zwei verschiedene α-Ti-Basislegierungen untersucht: Ein gegossenes porenfreies Stabmaterial und ein pulvermetallurgisch hergestelltes Material, das aufgrund der hohen Porosität besondere Anforderungen an die Bildverarbeitung stellt. In der vorliegenden Arbeit werden die hierbei zugrunde liegenden metallographischen und computergestützten Methoden erläutert.
References / Literatur
[1] Vander Voort, G. F.: Metallography – Principles and Practice, 4. Auflage, ASM International, 2007Search in Google Scholar
[2] McCrone, W. C.; McCrone, L. B.; Delly, J. G.: Polarized light microscopy. McCrone Research Institute, Chicago, ILSearch in Google Scholar
[3] MATLAB (R2015b); MathWorks, Inc.: Natick, MA, 1984–2015Search in Google Scholar
[4] Neves, R. G.; Ferrari, B.; Sanchez-Herencia, A. J.; Gordo, E.: Mater. Lett.2013, 107, S. 75–7810.1016/j.matlet.2013.05.015Search in Google Scholar
[5] Neves, R. G.; Ferrari, B.; Sanchez-Herencia, A. J.; Gordo, E.: Design of Ti Microstructure by Addition of Ceramic Particles by Colloidal Techniques, Euro PM – Lightweight Materials, Salzburg, Österreich, 2014Search in Google Scholar
[6] Godard, C.; Klingler, A.; Junker, T.; Kerscher, E.: Fortschritte in der Metallographie. Sonderbände der Praktischen Metallographie, Hrsg.: F. Mücklich und G. Petzow, 2014, 46, S. 119–124Search in Google Scholar
[7] Canny, J.: IEEE Trans. Pattern Anal. Mach. Intell.1986, 8, 679–69810.1109/TPAMI.1986.4767851Search in Google Scholar
[8] Britz, D.; Webel, J.; Gola, J.; Mücklich, F.: A Correlative Approach to Capture and Quantify Substructures by Means of Image Registration. Pract Metallogr.2017; 54 (10): 685–696. 10.3139/147.110484Search in Google Scholar
© 2018, Carl Hanser Verlag, München
Articles in the same Issue
- Contents/Inhalt
- Contents
- Editorial
- Editorial
- Technical Contributions/Fachbeiträge
- Microstructural Characterization of Martensitic Q&P Steels – a Comparison of Etching Techniques and Electron Backscatter Diffraction
- Method for the Detection of Grain Boundaries in α Ti-Based Alloys by means of Polarized Light Microscopy and Image Processing in MATLAB
- Investigation of the Precipitation Behavior of H-Carbides in a TiAl Alloy containing Carbon by means of in- and ex-situ Characterization
- Wear and Damage Characterization of Coated Carbide Tools by means of FIB-SEM Microscopy
- Meeting Diary/Veranstaltungskalender
- Meeting Diary
Articles in the same Issue
- Contents/Inhalt
- Contents
- Editorial
- Editorial
- Technical Contributions/Fachbeiträge
- Microstructural Characterization of Martensitic Q&P Steels – a Comparison of Etching Techniques and Electron Backscatter Diffraction
- Method for the Detection of Grain Boundaries in α Ti-Based Alloys by means of Polarized Light Microscopy and Image Processing in MATLAB
- Investigation of the Precipitation Behavior of H-Carbides in a TiAl Alloy containing Carbon by means of in- and ex-situ Characterization
- Wear and Damage Characterization of Coated Carbide Tools by means of FIB-SEM Microscopy
- Meeting Diary/Veranstaltungskalender
- Meeting Diary